Preparation and crystal structure of garnet-type calcium zirconium germanate Ca4ZrGe3O12
A polycrystalline sample of Ca4ZrGe3O12 was synthesized using the nitrate–citrate method and heated at 850–1100 °C. Structural refinement based on X-ray powder diffraction data showed that the crystal structure is of the garnet type with a cubic unit-cell parameter [a = 12.71299(3) Å] and the space...
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| Veröffentlicht in: | Powder diffraction 2016-12, Vol.31 (4), p.292-294 |
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| container_title | Powder diffraction |
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| creator | Zhuravlev, V. D. Tyutyunnik, A. P. Lobachevskaya, N. I. |
| description | A polycrystalline sample of Ca4ZrGe3O12 was synthesized using the nitrate–citrate method and heated at 850–1100 °C. Structural refinement based on X-ray powder diffraction data showed that the crystal structure is of the garnet type with a cubic unit-cell parameter [a = 12.71299(3) Å] and the space group Ia
$\bar 3$
d. The structural formula is presented as Ca3[CaZr]octa[Ge]tetraO12. |
| doi_str_mv | 10.1017/S0885715616000506 |
| format | Article |
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$\bar 3$
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$\bar 3$
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| source | Cambridge University Press Journals Complete |
| subjects | New Diffraction Data |
| title | Preparation and crystal structure of garnet-type calcium zirconium germanate Ca4ZrGe3O12 |
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