ChemInform Abstract: Scandium‐Substituted Na3Zr2(SiO4)2(PO4) Prepared by a Solution‐Assisted Solid‐State Reaction Method as Sodium‐Ion Conductors

ChemInform Abstract: Scandium‐Substituted Na3Zr2(SiO4)2(PO4) Prepared by a Solution‐Assisted Solid‐State Reaction Method as Sodium‐Ion Conductors

Polycrystalline Na3+xScxZr2‐x(SiO4)2 (PO4) (NSZSPx, x = 0—0.6) are fabricated on a laboratory scale (10 g—1 kg) by precipitation from stoichiometric aqueous solutions of NaNO3, Sc2O3, ZrO(NO3)2, Si(O‐Ac)4, and NH4H2PO4 followed by calcination (800 °C, 3 h), ball milling (2 d), and final sintering (1...

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Veröffentlicht in:ChemInform 2016-09, Vol.47 (39), p.no-no
Hauptverfasser: Ma, Qianli, Guin, Marie, Naqash, Sahir, Tsai, Chih‐Long, Tietz, Frank, Guillon, Olivier
Format: Artikel
Sprache:eng
Schlagworte:
electric properties, superconductors, semiconductors
electrolytes, electrolytic conductivity (inorganic)
phosphorus, P
scandium, Sc
silicon, Si
zirconium, Zr
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Zusammenfassung:Polycrystalline Na3+xScxZr2‐x(SiO4)2 (PO4) (NSZSPx, x = 0—0.6) are fabricated on a laboratory scale (10 g—1 kg) by precipitation from stoichiometric aqueous solutions of NaNO3, Sc2O3, ZrO(NO3)2, Si(O‐Ac)4, and NH4H2PO4 followed by calcination (800 °C, 3 h), ball milling (2 d), and final sintering (1250—1300 °C, 5 h).
ISSN:0931-7597
1522-2667
DOI:10.1002/chin.201639015