SSynthesis, characterisation and antimicrobial-activity of 3-thio-1,5-dihydro-2,4,3-benzodioxaphosphepin-3-amino acid esters

SSynthesis, characterisation and antimicrobial-activity of 3-thio-1,5-dihydro-2,4,3-benzodioxaphosphepin-3-amino acid esters

A new series of 3-thio-1,5-dihydro-2,4,3-benzodioxaphosphepin-3-amino acid esters (4a-k) were synthesized by treating different amino acid ester hydrochlorides (3a-k) with phosphorus monochloride intermediate (2) which was previously formed in situ from 1,2-phenylenedimethanol (1) and thiophosphoryl...

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Veröffentlicht in:Organic communications 2011-07, Vol.4 (3), p.67
Hauptverfasser: Chinthaparthi, Radha Rani, Gangireddy Chandra Sekhar Reddy, Chereddy, Syama Sundar, Kunda Uma Maheswara Rao, Krishnammagari, Suresh Kumar, Cirandur Suresh Reddy
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container_issue 3
container_start_page 67
container_title Organic communications
container_volume 4
creator Chinthaparthi, Radha Rani
Gangireddy Chandra Sekhar Reddy
Chereddy, Syama Sundar
Kunda Uma Maheswara Rao
Krishnammagari, Suresh Kumar
Cirandur Suresh Reddy
description A new series of 3-thio-1,5-dihydro-2,4,3-benzodioxaphosphepin-3-amino acid esters (4a-k) were synthesized by treating different amino acid ester hydrochlorides (3a-k) with phosphorus monochloride intermediate (2) which was previously formed in situ from 1,2-phenylenedimethanol (1) and thiophosphoryl chloride in the presence of triethylamine in dry tetrahydrofuran (THF) at 0-5 ºC to room temperature. The structures of the title compounds (4a-k) were established by analytical, IR, NMR (1H, 13C and 31P) and mass spectra, and they have been screened for their antimicrobial activity. They exhibited significant antibacterial, and antifungal activity.
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title SSynthesis, characterisation and antimicrobial-activity of 3-thio-1,5-dihydro-2,4,3-benzodioxaphosphepin-3-amino acid esters
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