Recovery of Au(III) ions by Au(III)-imprinted hydrogel
A new Au(III)-imprinted hydrogel (Au(III)-Imp) was prepared by the photopolymerisation of 4-acryloylmorpholine (AcM), 2-hydroxyethyl acrylate (HEA), and poly(ethylene glycol) diacrylate (cross-linking monomer, PEG-DA) in the presence of gold ions. In addition, non-imprinted hydrogel (N-Imp) was simi...
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| Veröffentlicht in: | Chemical papers 2016-06, Vol.70 (6), p.757-768 |
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| creator | Fırlak, Melike Çubuk, Soner Yetimoğlu, Ece Kök Kahraman, Memet V. |
| description | A new Au(III)-imprinted hydrogel (Au(III)-Imp) was prepared by the photopolymerisation of 4-acryloylmorpholine (AcM), 2-hydroxyethyl acrylate (HEA), and poly(ethylene glycol) diacrylate (cross-linking monomer, PEG-DA) in the presence of gold ions. In addition, non-imprinted hydrogel (N-Imp) was similarly prepared without Au(III) ions The Au(III)-Imp hydrogel was characterised by several techniques. To achieve the optimal conditions, effect of pH, time, and initial metal ion concentrations were investigated using a batch system. The pre-concentration factor for Au(III) ions was found to be at least 100. The analytical parameters of the method were determined and the method was also successfully applied to computer circuit board scrap samples. The reusability of the Au(III)-Imp hydrogel was also determined. |
| doi_str_mv | 10.1515/chempap-2016-0019 |
| format | Article |
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In addition, non-imprinted hydrogel (N-Imp) was similarly prepared without Au(III) ions The Au(III)-Imp hydrogel was characterised by several techniques. To achieve the optimal conditions, effect of pH, time, and initial metal ion concentrations were investigated using a batch system. The pre-concentration factor for Au(III) ions was found to be at least 100. The analytical parameters of the method were determined and the method was also successfully applied to computer circuit board scrap samples. The reusability of the Au(III)-Imp hydrogel was also determined.</description><identifier>ISSN: 0366-6352</identifier><identifier>EISSN: 1336-9075</identifier><identifier>DOI: 10.1515/chempap-2016-0019</identifier><language>eng</language><publisher>Cham: Springer International Publishing</publisher><subject>4-acryloylmorpholine ; Biochemistry ; Biotechnology ; Chemistry ; Chemistry and Materials Science ; Chemistry/Food Science ; gold(III) removal ; Industrial Chemistry/Chemical Engineering ; ion imprinted hydrogel ; Materials Science ; Medicinal Chemistry ; Original Paper ; UV curing</subject><ispartof>Chemical papers, 2016-06, Vol.70 (6), p.757-768</ispartof><rights>Institute of Chemistry, Slovak Academy of Sciences 2016</rights><rights>Copyright Walter de Gruyter GmbH 2016</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c409t-a866775f0913b811c557871ae1ad94005716b643c43a4413a1290752f51cb48c3</citedby><cites>FETCH-LOGICAL-c409t-a866775f0913b811c557871ae1ad94005716b643c43a4413a1290752f51cb48c3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1515/chempap-2016-0019$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1515/chempap-2016-0019$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Fırlak, Melike</creatorcontrib><creatorcontrib>Çubuk, Soner</creatorcontrib><creatorcontrib>Yetimoğlu, Ece Kök</creatorcontrib><creatorcontrib>Kahraman, Memet V.</creatorcontrib><title>Recovery of Au(III) ions by Au(III)-imprinted hydrogel</title><title>Chemical papers</title><addtitle>Chem. 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The reusability of the Au(III)-Imp hydrogel was also determined.</description><subject>4-acryloylmorpholine</subject><subject>Biochemistry</subject><subject>Biotechnology</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chemistry/Food Science</subject><subject>gold(III) removal</subject><subject>Industrial Chemistry/Chemical Engineering</subject><subject>ion imprinted hydrogel</subject><subject>Materials Science</subject><subject>Medicinal Chemistry</subject><subject>Original Paper</subject><subject>UV curing</subject><issn>0366-6352</issn><issn>1336-9075</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><sourceid>BENPR</sourceid><recordid>eNqNkEtLxEAQhAdRcF39Ad4CXvQw2p15JSdZFh-BBUH0PEwmk32wu4kziZJ_b0JW8CJ46m6oqi4-Qi4RblGguLMrt6tNTWNASQEwPSITZEzSFJQ4JhNgUlLJRHxKzkLYAHAOAiZEvjpbfTrfRVUZzdrrLMtuonW1D1He_dx0vav9et-4Ilp1ha-WbntOTkqzDe7iMKfk_fHhbf5MFy9P2Xy2oJZD2lCTSKmUKCFFlieIVgiVKDQOTZFyAKFQ5pIzy5nhHJnBeOgblwJtzhPLpuRqzK199dG60OhN1fp9_1KjStIkYalkvQpHlfVVCN6Vuu-7M77TCHrAow949IBHD3h6z_3o-TLbxvnCLX3b9cuvB395FUglVJ8QjwlhoLP8l5V9Axx3e6A</recordid><startdate>20160601</startdate><enddate>20160601</enddate><creator>Fırlak, Melike</creator><creator>Çubuk, Soner</creator><creator>Yetimoğlu, Ece Kök</creator><creator>Kahraman, Memet V.</creator><general>Springer International Publishing</general><general>De Gruyter</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>L6V</scope><scope>L7M</scope><scope>M7S</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope></search><sort><creationdate>20160601</creationdate><title>Recovery of Au(III) ions by Au(III)-imprinted hydrogel</title><author>Fırlak, Melike ; Çubuk, Soner ; Yetimoğlu, Ece Kök ; Kahraman, Memet V.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c409t-a866775f0913b811c557871ae1ad94005716b643c43a4413a1290752f51cb48c3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2016</creationdate><topic>4-acryloylmorpholine</topic><topic>Biochemistry</topic><topic>Biotechnology</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Chemistry/Food Science</topic><topic>gold(III) removal</topic><topic>Industrial Chemistry/Chemical Engineering</topic><topic>ion imprinted hydrogel</topic><topic>Materials Science</topic><topic>Medicinal Chemistry</topic><topic>Original Paper</topic><topic>UV curing</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Fırlak, Melike</creatorcontrib><creatorcontrib>Çubuk, Soner</creatorcontrib><creatorcontrib>Yetimoğlu, Ece Kök</creatorcontrib><creatorcontrib>Kahraman, Memet V.</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>ProQuest Engineering Collection</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Engineering Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>Engineering Collection</collection><jtitle>Chemical papers</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Fırlak, Melike</au><au>Çubuk, Soner</au><au>Yetimoğlu, Ece Kök</au><au>Kahraman, Memet V.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Recovery of Au(III) ions by Au(III)-imprinted hydrogel</atitle><jtitle>Chemical papers</jtitle><stitle>Chem. Pap</stitle><date>2016-06-01</date><risdate>2016</risdate><volume>70</volume><issue>6</issue><spage>757</spage><epage>768</epage><pages>757-768</pages><issn>0366-6352</issn><eissn>1336-9075</eissn><abstract>A new Au(III)-imprinted hydrogel (Au(III)-Imp) was prepared by the photopolymerisation of 4-acryloylmorpholine (AcM), 2-hydroxyethyl acrylate (HEA), and poly(ethylene glycol) diacrylate (cross-linking monomer, PEG-DA) in the presence of gold ions. In addition, non-imprinted hydrogel (N-Imp) was similarly prepared without Au(III) ions The Au(III)-Imp hydrogel was characterised by several techniques. To achieve the optimal conditions, effect of pH, time, and initial metal ion concentrations were investigated using a batch system. The pre-concentration factor for Au(III) ions was found to be at least 100. The analytical parameters of the method were determined and the method was also successfully applied to computer circuit board scrap samples. 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| language | eng |
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| source | Springer Nature - Complete Springer Journals |
| subjects | 4-acryloylmorpholine Biochemistry Biotechnology Chemistry Chemistry and Materials Science Chemistry/Food Science gold(III) removal Industrial Chemistry/Chemical Engineering ion imprinted hydrogel Materials Science Medicinal Chemistry Original Paper UV curing |
| title | Recovery of Au(III) ions by Au(III)-imprinted hydrogel |
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