Preparation, characterization of nano-silica/fluoroacrylate material and the application in stone surface conservation
A series of fluoroacrylate (FPA) and nano-silica/fluoroacrylate were prepared. The properties including physical properties, mechanical behavior and contact angle of FPA were investigated. According to the results, the optimal fluoride content can be screened. The nano-silica/fluoroacrylate (SiO 2 /...
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| Veröffentlicht in: | Journal of polymer research 2016-04, Vol.23 (4), p.1, Article 75 |
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| creator | Zhang, Xiaoying Wen, Wenya Yu, Hanqiang Qiu, Fengxian Chen, Qian Yang, Dongya |
| description | A series of fluoroacrylate (FPA) and nano-silica/fluoroacrylate were prepared. The properties including physical properties, mechanical behavior and contact angle of FPA were investigated. According to the results, the optimal fluoride content can be screened. The nano-silica/fluoroacrylate (SiO
2
/FPA) materials were characterized by fourier transform infrared (FT-IR), thermogravimetric analysis (TGA) and transmission electron microscope (TEM). The surface morphology and mineralogical analysis of the stone samples were characterized by scanning electron microscope (SEM) and X-ray diffraction (XRD), respectively. The prepared coating was selected to protect on the stone surface. Aimed at evaluating the coating performance, the protective performances were also evaluated by artificial aging test. The results indicated that when the content of hexafluoro-butyl methacrylate (HFMA) was 8.0 wt% and the content of SiO
2
was 4.0 wt%, the prepared material has good compatibility and appearance with stone relics. The protective coating material for protection of chosen Jiaoshan Steles Grove (China) is noticeable and it can be widely applied to the protection of stone relics. |
| doi_str_mv | 10.1007/s10965-016-0967-8 |
| format | Article |
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2
/FPA) materials were characterized by fourier transform infrared (FT-IR), thermogravimetric analysis (TGA) and transmission electron microscope (TEM). The surface morphology and mineralogical analysis of the stone samples were characterized by scanning electron microscope (SEM) and X-ray diffraction (XRD), respectively. The prepared coating was selected to protect on the stone surface. Aimed at evaluating the coating performance, the protective performances were also evaluated by artificial aging test. The results indicated that when the content of hexafluoro-butyl methacrylate (HFMA) was 8.0 wt% and the content of SiO
2
was 4.0 wt%, the prepared material has good compatibility and appearance with stone relics. The protective coating material for protection of chosen Jiaoshan Steles Grove (China) is noticeable and it can be widely applied to the protection of stone relics.</description><identifier>ISSN: 1022-9760</identifier><identifier>EISSN: 1572-8935</identifier><identifier>DOI: 10.1007/s10965-016-0967-8</identifier><language>eng</language><publisher>Dordrecht: Springer Netherlands</publisher><subject>Characterization and Evaluation of Materials ; Chemistry ; Chemistry and Materials Science ; Industrial Chemistry/Chemical Engineering ; Original Paper ; Polymer Sciences</subject><ispartof>Journal of polymer research, 2016-04, Vol.23 (4), p.1, Article 75</ispartof><rights>Springer Science+Business Media Dordrecht 2016</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c316t-b8da6a6be986187f3167c15565382999e8346140f35b4cecaa5037c64439e80b3</citedby><cites>FETCH-LOGICAL-c316t-b8da6a6be986187f3167c15565382999e8346140f35b4cecaa5037c64439e80b3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10965-016-0967-8$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10965-016-0967-8$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27923,27924,41487,42556,51318</link.rule.ids></links><search><creatorcontrib>Zhang, Xiaoying</creatorcontrib><creatorcontrib>Wen, Wenya</creatorcontrib><creatorcontrib>Yu, Hanqiang</creatorcontrib><creatorcontrib>Qiu, Fengxian</creatorcontrib><creatorcontrib>Chen, Qian</creatorcontrib><creatorcontrib>Yang, Dongya</creatorcontrib><title>Preparation, characterization of nano-silica/fluoroacrylate material and the application in stone surface conservation</title><title>Journal of polymer research</title><addtitle>J Polym Res</addtitle><description>A series of fluoroacrylate (FPA) and nano-silica/fluoroacrylate were prepared. The properties including physical properties, mechanical behavior and contact angle of FPA were investigated. According to the results, the optimal fluoride content can be screened. The nano-silica/fluoroacrylate (SiO
2
/FPA) materials were characterized by fourier transform infrared (FT-IR), thermogravimetric analysis (TGA) and transmission electron microscope (TEM). The surface morphology and mineralogical analysis of the stone samples were characterized by scanning electron microscope (SEM) and X-ray diffraction (XRD), respectively. The prepared coating was selected to protect on the stone surface. Aimed at evaluating the coating performance, the protective performances were also evaluated by artificial aging test. The results indicated that when the content of hexafluoro-butyl methacrylate (HFMA) was 8.0 wt% and the content of SiO
2
was 4.0 wt%, the prepared material has good compatibility and appearance with stone relics. The protective coating material for protection of chosen Jiaoshan Steles Grove (China) is noticeable and it can be widely applied to the protection of stone relics.</description><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Industrial Chemistry/Chemical Engineering</subject><subject>Original Paper</subject><subject>Polymer Sciences</subject><issn>1022-9760</issn><issn>1572-8935</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp1kEtPwzAQhC0EEqXwA7hZ4oqpncSPHFHFS6oEBzhbG9ehqVI72Eml8utxGg5cOO1o55tdaRC6ZvSOUSoXkdFScEKZIElIok7QjHGZEVXm_DRpmmWklIKeo4sYt5RyLoWaof1bsB0E6BvvbrHZJGl6G5rv4wb7GjtwnsSmbQws6nbwwYMJhxZ6i3cwotBicGvcbyyGrhu5Y7RxOPbeWRyHUIOx2HgXbdgf3Ut0VkMb7dXvnKOPx4f35TNZvT69LO9XxORM9KRSaxAgKlsqwZSs01IaxrngucrKsrQqLwQraJ3zqjDWAHCaSyOKIk8erfI5upnudsF_DTb2euuH4NJLzaTkkhUZZYliE2WCjzHYWneh2UE4aEb1WK-e6tWpXj3Wq1XKZFMmJtZ92vDn8r-hHxXPfyw</recordid><startdate>20160401</startdate><enddate>20160401</enddate><creator>Zhang, Xiaoying</creator><creator>Wen, Wenya</creator><creator>Yu, Hanqiang</creator><creator>Qiu, Fengxian</creator><creator>Chen, Qian</creator><creator>Yang, Dongya</creator><general>Springer Netherlands</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope></search><sort><creationdate>20160401</creationdate><title>Preparation, characterization of nano-silica/fluoroacrylate material and the application in stone surface conservation</title><author>Zhang, Xiaoying ; Wen, Wenya ; Yu, Hanqiang ; Qiu, Fengxian ; Chen, Qian ; Yang, Dongya</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c316t-b8da6a6be986187f3167c15565382999e8346140f35b4cecaa5037c64439e80b3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2016</creationdate><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Industrial Chemistry/Chemical Engineering</topic><topic>Original Paper</topic><topic>Polymer Sciences</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Zhang, Xiaoying</creatorcontrib><creatorcontrib>Wen, Wenya</creatorcontrib><creatorcontrib>Yu, Hanqiang</creatorcontrib><creatorcontrib>Qiu, Fengxian</creatorcontrib><creatorcontrib>Chen, Qian</creatorcontrib><creatorcontrib>Yang, Dongya</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><jtitle>Journal of polymer research</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Zhang, Xiaoying</au><au>Wen, Wenya</au><au>Yu, Hanqiang</au><au>Qiu, Fengxian</au><au>Chen, Qian</au><au>Yang, Dongya</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Preparation, characterization of nano-silica/fluoroacrylate material and the application in stone surface conservation</atitle><jtitle>Journal of polymer research</jtitle><stitle>J Polym Res</stitle><date>2016-04-01</date><risdate>2016</risdate><volume>23</volume><issue>4</issue><spage>1</spage><pages>1-</pages><artnum>75</artnum><issn>1022-9760</issn><eissn>1572-8935</eissn><abstract>A series of fluoroacrylate (FPA) and nano-silica/fluoroacrylate were prepared. The properties including physical properties, mechanical behavior and contact angle of FPA were investigated. According to the results, the optimal fluoride content can be screened. The nano-silica/fluoroacrylate (SiO
2
/FPA) materials were characterized by fourier transform infrared (FT-IR), thermogravimetric analysis (TGA) and transmission electron microscope (TEM). The surface morphology and mineralogical analysis of the stone samples were characterized by scanning electron microscope (SEM) and X-ray diffraction (XRD), respectively. The prepared coating was selected to protect on the stone surface. Aimed at evaluating the coating performance, the protective performances were also evaluated by artificial aging test. The results indicated that when the content of hexafluoro-butyl methacrylate (HFMA) was 8.0 wt% and the content of SiO
2
was 4.0 wt%, the prepared material has good compatibility and appearance with stone relics. The protective coating material for protection of chosen Jiaoshan Steles Grove (China) is noticeable and it can be widely applied to the protection of stone relics.</abstract><cop>Dordrecht</cop><pub>Springer Netherlands</pub><doi>10.1007/s10965-016-0967-8</doi></addata></record> |
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| subjects | Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Industrial Chemistry/Chemical Engineering Original Paper Polymer Sciences |
| title | Preparation, characterization of nano-silica/fluoroacrylate material and the application in stone surface conservation |
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