An Efficient One-pot Synthesis of Pyrazolone Derivatives Promoted by Acidic Ionic Liquid

A new class of pyrazolone derivatives has been isolated in good to excellent yields from the 2 : 1 condensation reaction between 3-methyl-1-phenyl-5-pyrazolone and arylaldehydes in the presence of ionic liquid [HMIM]HSO4. The compounds were characterised by their IR, NMR spectra, MS and elemental an...

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Veröffentlicht in:Chinese journal of chemistry 2011-10, Vol.29 (10), p.2202-2204
1. Verfasser: 臧洪俊 苏秋红 郭松 莫颖明 程博闻
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Sprache:eng
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Zusammenfassung:A new class of pyrazolone derivatives has been isolated in good to excellent yields from the 2 : 1 condensation reaction between 3-methyl-1-phenyl-5-pyrazolone and arylaldehydes in the presence of ionic liquid [HMIM]HSO4. The compounds were characterised by their IR, NMR spectra, MS and elemental analyses. The important features of the methodology are a wide application range of substrates, higher yields and shorter reaction time.
ISSN:1001-604X
1614-7065
DOI:10.1002/cjoc.201180381