In situ observations of the rapid solidification for undercooled Al30Si70 alloy melt

Rapid solidification of Al30Si70 alloy was studied via electromagnetic levitation technique. The solidification kinetics and the morphology of the solidification front of the Si phase were analyzed in situ by using a high-speed video camera and subsequent microstructural analysis of as-solidified sa...

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Veröffentlicht in:Journal of materials research 2016-01, Vol.31 (2), p.222-231
Hauptverfasser: Xu, Junfeng, Diao, Long, Yan, Junhui, Dang, Bo, Zhu, Man, Chang, Fange, Jian, Zengyun
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container_end_page 231
container_issue 2
container_start_page 222
container_title Journal of materials research
container_volume 31
creator Xu, Junfeng
Diao, Long
Yan, Junhui
Dang, Bo
Zhu, Man
Chang, Fange
Jian, Zengyun
description Rapid solidification of Al30Si70 alloy was studied via electromagnetic levitation technique. The solidification kinetics and the morphology of the solidification front of the Si phase were analyzed in situ by using a high-speed video camera and subsequent microstructural analysis of as-solidified samples. It shows that solidification of the sample always starts from one point. After that, nucleation continues to proceed at the interface front during growth. The morphology of primary Si transforms from faceted wafer to nonfaceted equiaxed grain and the grain size decreases with increase of undercooling. At small undercooling, the growth velocity of primary Si decreases with time and the floated Si wafers have a trend to agglomerate, while at large undercooling, the nucleation rate decreases with time, which are explained by the fact that silicon content, undercooling and density at the solid–liquid interface change with time in solidification. Finally, the nucleation rate and growth velocity were discussed in combination of classical theory.
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subjects Alloy solidification
Alloys
Analysis
Applied and Technical Physics
Biomaterials
Directional solidification
Experiments
Inorganic Chemistry
Interfaces
Kinetics
Materials Engineering
Materials research
Materials Science
Microscopy
Microstructure
Nanotechnology
Radio frequency
Scanning electron microscopy
Solids
Studies
title In situ observations of the rapid solidification for undercooled Al30Si70 alloy melt
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