Low Temperature and Pressure Synthesis of Lithium-Nitride Compound with H2O Addition on Lithium Target for BNCT
Low temperature synthesis of lithium-nitride compound was conducted on the lithium target for BNCT by N2/H2O mixing gas squirt in the ultra high vacuum chamber, and the following results were derived; (1) Lithium-nitride compound was synthesized on the lithium target under 101.3 Pa N2 gas squirt at...
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Veröffentlicht in: | Nihon Kinzoku Gakkai shi (1952) 2014-08, Vol.78 (8), p.317-321 |
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creator | Ishiyama, Shintaro Baba, Yuji Fujii, Ryo Nakamura, Masaru Imahori, Yoshio |
description | Low temperature synthesis of lithium-nitride compound was conducted on the lithium target for BNCT by N2/H2O mixing gas squirt in the ultra high vacuum chamber, and the following results were derived; (1) Lithium-nitride compound was synthesized on the lithium target under 101.3 Pa N2 gas squirt at room temperature and in the ultra high vacuum chamber under the pressure of 1×10-8 Pa. (2)Remarkable contamination by O and C was observed on the lithium-nitride compound synthesized under the squirt pressure of 13.3~80 Pa/1.33~4.7 Pa N2/H2O mixing gas. (3) No contamination and synthesis of Li-N compound was observed under the squirt pressure of 0.013~0.027 Pa/0~0.005 Pa N2/H2O mixing gas. (4) Contamination by O and C was enhanced with excessive addition of H2O at the pressure of over 1.33 Pa. |
doi_str_mv | 10.2320/jinstmet.J2013078 |
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(2)Remarkable contamination by O and C was observed on the lithium-nitride compound synthesized under the squirt pressure of 13.3~80 Pa/1.33~4.7 Pa N2/H2O mixing gas. (3) No contamination and synthesis of Li-N compound was observed under the squirt pressure of 0.013~0.027 Pa/0~0.005 Pa N2/H2O mixing gas. (4) Contamination by O and C was enhanced with excessive addition of H2O at the pressure of over 1.33 Pa.</description><identifier>ISSN: 0021-4876</identifier><identifier>EISSN: 1880-6880</identifier><identifier>DOI: 10.2320/jinstmet.J2013078</identifier><language>eng</language><publisher>Sendai: Japan Science and Technology Agency</publisher><subject>Contamination ; High vacuum ; Lithium ; Low temperature ; Nitrides ; Room temperature ; Synthesis ; Vacuum chambers</subject><ispartof>Nihon Kinzoku Gakkai shi (1952), 2014-08, Vol.78 (8), p.317-321</ispartof><rights>Copyright Japan Science and Technology Agency 2014</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c1138-27e84a291cdf05bb1cd068d6bb41e9919bb5c37bcd4768d5432c88e0b9a615103</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27901,27902</link.rule.ids></links><search><creatorcontrib>Ishiyama, Shintaro</creatorcontrib><creatorcontrib>Baba, Yuji</creatorcontrib><creatorcontrib>Fujii, Ryo</creatorcontrib><creatorcontrib>Nakamura, Masaru</creatorcontrib><creatorcontrib>Imahori, Yoshio</creatorcontrib><title>Low Temperature and Pressure Synthesis of Lithium-Nitride Compound with H2O Addition on Lithium Target for BNCT</title><title>Nihon Kinzoku Gakkai shi (1952)</title><description>Low temperature synthesis of lithium-nitride compound was conducted on the lithium target for BNCT by N2/H2O mixing gas squirt in the ultra high vacuum chamber, and the following results were derived; (1) Lithium-nitride compound was synthesized on the lithium target under 101.3 Pa N2 gas squirt at room temperature and in the ultra high vacuum chamber under the pressure of 1×10-8 Pa. (2)Remarkable contamination by O and C was observed on the lithium-nitride compound synthesized under the squirt pressure of 13.3~80 Pa/1.33~4.7 Pa N2/H2O mixing gas. (3) No contamination and synthesis of Li-N compound was observed under the squirt pressure of 0.013~0.027 Pa/0~0.005 Pa N2/H2O mixing gas. (4) Contamination by O and C was enhanced with excessive addition of H2O at the pressure of over 1.33 Pa.</description><subject>Contamination</subject><subject>High vacuum</subject><subject>Lithium</subject><subject>Low temperature</subject><subject>Nitrides</subject><subject>Room temperature</subject><subject>Synthesis</subject><subject>Vacuum chambers</subject><issn>0021-4876</issn><issn>1880-6880</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><recordid>eNo1kNFLwzAQxoMoOHR_gG8Bnztzadqkj7OoU8omWJ9L06YuwzY1SRn7783YBsd9fHc_7uBD6AHIgsaUPO304Hyv_OKDEogJF1doBkKQKA3tGs0IoRAxwdNbNHdOy-CZYCzlM2QKs8el6kdlaz9ZheuhxZ9WOXc0X4fBb5XTDpsOF9pv9dRHa-2tbhXOTT-aKeD7sMArusHLttVemwGHOtO4rO2P8rgzFj-v8_Ie3XT1r1Pzs96h79eXMl9FxebtPV8WUQMQi4hyJVhNM2jajiRSBiWpaFMpGagsg0zKpIm5bFrGwzxhMW2EUERmdQoJkPgOPZ7ujtb8Tcr5amcmO4SXFfAkIRkjwAMFJ6qxxjmrumq0uq_toQJSHaOtLtFWl2jjfzqrboA</recordid><startdate>20140801</startdate><enddate>20140801</enddate><creator>Ishiyama, Shintaro</creator><creator>Baba, Yuji</creator><creator>Fujii, Ryo</creator><creator>Nakamura, Masaru</creator><creator>Imahori, Yoshio</creator><general>Japan Science and Technology Agency</general><scope>AAYXX</scope><scope>CITATION</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20140801</creationdate><title>Low Temperature and Pressure Synthesis of Lithium-Nitride Compound with H2O Addition on Lithium Target for BNCT</title><author>Ishiyama, Shintaro ; Baba, Yuji ; Fujii, Ryo ; Nakamura, Masaru ; Imahori, Yoshio</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c1138-27e84a291cdf05bb1cd068d6bb41e9919bb5c37bcd4768d5432c88e0b9a615103</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Contamination</topic><topic>High vacuum</topic><topic>Lithium</topic><topic>Low temperature</topic><topic>Nitrides</topic><topic>Room temperature</topic><topic>Synthesis</topic><topic>Vacuum chambers</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Ishiyama, Shintaro</creatorcontrib><creatorcontrib>Baba, Yuji</creatorcontrib><creatorcontrib>Fujii, Ryo</creatorcontrib><creatorcontrib>Nakamura, Masaru</creatorcontrib><creatorcontrib>Imahori, Yoshio</creatorcontrib><collection>CrossRef</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Nihon Kinzoku Gakkai shi (1952)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Ishiyama, Shintaro</au><au>Baba, Yuji</au><au>Fujii, Ryo</au><au>Nakamura, Masaru</au><au>Imahori, Yoshio</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Low Temperature and Pressure Synthesis of Lithium-Nitride Compound with H2O Addition on Lithium Target for BNCT</atitle><jtitle>Nihon Kinzoku Gakkai shi (1952)</jtitle><date>2014-08-01</date><risdate>2014</risdate><volume>78</volume><issue>8</issue><spage>317</spage><epage>321</epage><pages>317-321</pages><issn>0021-4876</issn><eissn>1880-6880</eissn><abstract>Low temperature synthesis of lithium-nitride compound was conducted on the lithium target for BNCT by N2/H2O mixing gas squirt in the ultra high vacuum chamber, and the following results were derived; (1) Lithium-nitride compound was synthesized on the lithium target under 101.3 Pa N2 gas squirt at room temperature and in the ultra high vacuum chamber under the pressure of 1×10-8 Pa. (2)Remarkable contamination by O and C was observed on the lithium-nitride compound synthesized under the squirt pressure of 13.3~80 Pa/1.33~4.7 Pa N2/H2O mixing gas. (3) No contamination and synthesis of Li-N compound was observed under the squirt pressure of 0.013~0.027 Pa/0~0.005 Pa N2/H2O mixing gas. (4) Contamination by O and C was enhanced with excessive addition of H2O at the pressure of over 1.33 Pa.</abstract><cop>Sendai</cop><pub>Japan Science and Technology Agency</pub><doi>10.2320/jinstmet.J2013078</doi><tpages>5</tpages><oa>free_for_read</oa></addata></record> |
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source | Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals |
subjects | Contamination High vacuum Lithium Low temperature Nitrides Room temperature Synthesis Vacuum chambers |
title | Low Temperature and Pressure Synthesis of Lithium-Nitride Compound with H2O Addition on Lithium Target for BNCT |
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