Cobalt Oxide Nanoflowers for Electrochemical Determination of Glucose
This study reports a simple, economic, and efficient approach for synthesis of cobalt oxide (Co 3 O 4 ) nanostructures by a low-temperature aqueous chemical growth method. The synthesized Co 3 O 4 nanostructures were characterized by various techniques such as x-ray diffraction, x-ray photoelectron...
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| Veröffentlicht in: | Journal of electronic materials 2015-10, Vol.44 (10), p.3724-3732 |
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| creator | Balouch, Quratulain Ibupoto, Zafar Hussain Khaskheli, Ghulam Qadir Soomro, Razium Ali Sirajuddin Samoon, Muhammad Kashif Deewani, Vinod Kumar |
| description | This study reports a simple, economic, and efficient approach for synthesis of cobalt oxide (Co
3
O
4
) nanostructures by a low-temperature aqueous chemical growth method. The synthesized Co
3
O
4
nanostructures were characterized by various techniques such as x-ray diffraction, x-ray photoelectron spectroscopy, and scanning electron microscopy. The synthesized nanostructures exhibited flower-shaped morphology with thickness of each pellet in the range of 200 to 300 nm. The synthesized Co
3
O
4
nanostructures with excellent structural features exhibited high electrocatalytic activity towards the oxidation of glucose in alkaline solution. This enabled development of a highly sensitive (1618.71
µ
A mM
−1
cm
−2
), stable and reproducible non-enzymatic glucose sensor. The developed sensor demonstrated high anti-interference capability against common interferents such as dopamine, ascorbic acid and uric acid. Furthermore, the applicability of the developed sensor for the determination of glucose from human blood serum provides an alternative approach for the routine glucose analysis. |
| doi_str_mv | 10.1007/s11664-015-3860-z |
| format | Article |
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3
O
4
) nanostructures by a low-temperature aqueous chemical growth method. The synthesized Co
3
O
4
nanostructures were characterized by various techniques such as x-ray diffraction, x-ray photoelectron spectroscopy, and scanning electron microscopy. The synthesized nanostructures exhibited flower-shaped morphology with thickness of each pellet in the range of 200 to 300 nm. The synthesized Co
3
O
4
nanostructures with excellent structural features exhibited high electrocatalytic activity towards the oxidation of glucose in alkaline solution. This enabled development of a highly sensitive (1618.71
µ
A mM
−1
cm
−2
), stable and reproducible non-enzymatic glucose sensor. The developed sensor demonstrated high anti-interference capability against common interferents such as dopamine, ascorbic acid and uric acid. Furthermore, the applicability of the developed sensor for the determination of glucose from human blood serum provides an alternative approach for the routine glucose analysis.</description><identifier>ISSN: 0361-5235</identifier><identifier>EISSN: 1543-186X</identifier><identifier>DOI: 10.1007/s11664-015-3860-z</identifier><identifier>CODEN: JECMA5</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Electronics and Microelectronics ; Enzymes ; Glucose ; Instrumentation ; Materials Science ; Nanostructured materials ; Optical and Electronic Materials ; Solid State Physics</subject><ispartof>Journal of electronic materials, 2015-10, Vol.44 (10), p.3724-3732</ispartof><rights>The Minerals, Metals & Materials Society 2015</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c386t-8e803d369b7e84457339513ae664c297131e3effaf5891f458636e2b155766853</citedby><cites>FETCH-LOGICAL-c386t-8e803d369b7e84457339513ae664c297131e3effaf5891f458636e2b155766853</cites><orcidid>0000-0002-1875-8181</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11664-015-3860-z$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11664-015-3860-z$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Balouch, Quratulain</creatorcontrib><creatorcontrib>Ibupoto, Zafar Hussain</creatorcontrib><creatorcontrib>Khaskheli, Ghulam Qadir</creatorcontrib><creatorcontrib>Soomro, Razium Ali</creatorcontrib><creatorcontrib>Sirajuddin</creatorcontrib><creatorcontrib>Samoon, Muhammad Kashif</creatorcontrib><creatorcontrib>Deewani, Vinod Kumar</creatorcontrib><title>Cobalt Oxide Nanoflowers for Electrochemical Determination of Glucose</title><title>Journal of electronic materials</title><addtitle>Journal of Elec Materi</addtitle><description>This study reports a simple, economic, and efficient approach for synthesis of cobalt oxide (Co
3
O
4
) nanostructures by a low-temperature aqueous chemical growth method. The synthesized Co
3
O
4
nanostructures were characterized by various techniques such as x-ray diffraction, x-ray photoelectron spectroscopy, and scanning electron microscopy. The synthesized nanostructures exhibited flower-shaped morphology with thickness of each pellet in the range of 200 to 300 nm. The synthesized Co
3
O
4
nanostructures with excellent structural features exhibited high electrocatalytic activity towards the oxidation of glucose in alkaline solution. This enabled development of a highly sensitive (1618.71
µ
A mM
−1
cm
−2
), stable and reproducible non-enzymatic glucose sensor. The developed sensor demonstrated high anti-interference capability against common interferents such as dopamine, ascorbic acid and uric acid. Furthermore, the applicability of the developed sensor for the determination of glucose from human blood serum provides an alternative approach for the routine glucose analysis.</description><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Electronics and Microelectronics</subject><subject>Enzymes</subject><subject>Glucose</subject><subject>Instrumentation</subject><subject>Materials Science</subject><subject>Nanostructured materials</subject><subject>Optical and Electronic Materials</subject><subject>Solid State Physics</subject><issn>0361-5235</issn><issn>1543-186X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2015</creationdate><recordtype>article</recordtype><sourceid>8G5</sourceid><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><sourceid>GUQSH</sourceid><sourceid>M2O</sourceid><recordid>eNp1kD1PwzAURS0EEqXwA9gsMRv84vgjIyqlIFV0AYnNctNnSJXGxU4F9NfjKgwsTG85976rQ8gl8GvgXN8kAKVKxkEyYRRn-yMyAlkKBka9HpMRFwqYLIQ8JWcprXkGwcCITCdh6dqeLr6aFdIn1wXfhk-MifoQ6bTFuo-hfsdNU7uW3mGPcdN0rm9CR4Ons3ZXh4Tn5MS7NuHF7x2Tl_vp8-SBzRezx8ntnNV5VM8MGi5WQlVLjaYspRaikiAc5ul1UWkQgAK9d16aCnwpjRIKiyVIqZUyUozJ1dC7jeFjh6m367CLXX5pQXOjTVGWOlMwUHUMKUX0dhubjYvfFrg92LKDLZsl2IMtu8-ZYsikzHZvGP80_xv6AfwXa_U</recordid><startdate>20151001</startdate><enddate>20151001</enddate><creator>Balouch, Quratulain</creator><creator>Ibupoto, Zafar Hussain</creator><creator>Khaskheli, Ghulam Qadir</creator><creator>Soomro, Razium Ali</creator><creator>Sirajuddin</creator><creator>Samoon, Muhammad Kashif</creator><creator>Deewani, Vinod Kumar</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>7XB</scope><scope>88I</scope><scope>8AF</scope><scope>8AO</scope><scope>8FE</scope><scope>8FG</scope><scope>8FK</scope><scope>8G5</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>ARAPS</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>GNUQQ</scope><scope>GUQSH</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>L6V</scope><scope>M2O</scope><scope>M2P</scope><scope>M7S</scope><scope>MBDVC</scope><scope>P5Z</scope><scope>P62</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope><scope>Q9U</scope><scope>S0X</scope><orcidid>https://orcid.org/0000-0002-1875-8181</orcidid></search><sort><creationdate>20151001</creationdate><title>Cobalt Oxide Nanoflowers for Electrochemical Determination of Glucose</title><author>Balouch, Quratulain ; Ibupoto, Zafar Hussain ; Khaskheli, Ghulam Qadir ; Soomro, Razium Ali ; Sirajuddin ; Samoon, Muhammad Kashif ; Deewani, Vinod Kumar</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c386t-8e803d369b7e84457339513ae664c297131e3effaf5891f458636e2b155766853</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2015</creationdate><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Electronics and Microelectronics</topic><topic>Enzymes</topic><topic>Glucose</topic><topic>Instrumentation</topic><topic>Materials Science</topic><topic>Nanostructured materials</topic><topic>Optical and Electronic Materials</topic><topic>Solid State Physics</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Balouch, Quratulain</creatorcontrib><creatorcontrib>Ibupoto, Zafar Hussain</creatorcontrib><creatorcontrib>Khaskheli, Ghulam Qadir</creatorcontrib><creatorcontrib>Soomro, Razium Ali</creatorcontrib><creatorcontrib>Sirajuddin</creatorcontrib><creatorcontrib>Samoon, Muhammad Kashif</creatorcontrib><creatorcontrib>Deewani, Vinod Kumar</creatorcontrib><collection>CrossRef</collection><collection>ProQuest Central (Corporate)</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>Science Database (Alumni Edition)</collection><collection>STEM Database</collection><collection>ProQuest Pharma Collection</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>Research Library (Alumni Edition)</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>Advanced Technologies & Aerospace Collection</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>ProQuest Central Student</collection><collection>Research Library Prep</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>ProQuest Engineering Collection</collection><collection>Research Library</collection><collection>Science Database</collection><collection>Engineering Database</collection><collection>Research Library (Corporate)</collection><collection>Advanced Technologies & Aerospace Database</collection><collection>ProQuest Advanced Technologies & Aerospace Collection</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>Engineering Collection</collection><collection>ProQuest Central Basic</collection><collection>SIRS Editorial</collection><jtitle>Journal of electronic materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Balouch, Quratulain</au><au>Ibupoto, Zafar Hussain</au><au>Khaskheli, Ghulam Qadir</au><au>Soomro, Razium Ali</au><au>Sirajuddin</au><au>Samoon, Muhammad Kashif</au><au>Deewani, Vinod Kumar</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Cobalt Oxide Nanoflowers for Electrochemical Determination of Glucose</atitle><jtitle>Journal of electronic materials</jtitle><stitle>Journal of Elec Materi</stitle><date>2015-10-01</date><risdate>2015</risdate><volume>44</volume><issue>10</issue><spage>3724</spage><epage>3732</epage><pages>3724-3732</pages><issn>0361-5235</issn><eissn>1543-186X</eissn><coden>JECMA5</coden><abstract>This study reports a simple, economic, and efficient approach for synthesis of cobalt oxide (Co
3
O
4
) nanostructures by a low-temperature aqueous chemical growth method. The synthesized Co
3
O
4
nanostructures were characterized by various techniques such as x-ray diffraction, x-ray photoelectron spectroscopy, and scanning electron microscopy. The synthesized nanostructures exhibited flower-shaped morphology with thickness of each pellet in the range of 200 to 300 nm. The synthesized Co
3
O
4
nanostructures with excellent structural features exhibited high electrocatalytic activity towards the oxidation of glucose in alkaline solution. This enabled development of a highly sensitive (1618.71
µ
A mM
−1
cm
−2
), stable and reproducible non-enzymatic glucose sensor. The developed sensor demonstrated high anti-interference capability against common interferents such as dopamine, ascorbic acid and uric acid. Furthermore, the applicability of the developed sensor for the determination of glucose from human blood serum provides an alternative approach for the routine glucose analysis.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s11664-015-3860-z</doi><tpages>9</tpages><orcidid>https://orcid.org/0000-0002-1875-8181</orcidid></addata></record> |
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| subjects | Characterization and Evaluation of Materials Chemistry and Materials Science Electronics and Microelectronics Enzymes Glucose Instrumentation Materials Science Nanostructured materials Optical and Electronic Materials Solid State Physics |
| title | Cobalt Oxide Nanoflowers for Electrochemical Determination of Glucose |
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