X-ray topography contrast from edge dislocations in ZnGeP2 single crystals
X‐ray topography images in the form of contrast rosettes from edge dislocations of the slip system in ZnGeP2 single crystals, obtained under different diffraction conditions, are identified and interpreted. To analyze and model the dislocation images, a semi‐phenomenological theory of contrast is ap...
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Veröffentlicht in: | Journal of applied crystallography 2015-08, Vol.48 (4), p.1228-1233 |
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description | X‐ray topography images in the form of contrast rosettes from edge dislocations of the slip system in ZnGeP2 single crystals, obtained under different diffraction conditions, are identified and interpreted. To analyze and model the dislocation images, a semi‐phenomenological theory of contrast is applied. The simulation of images of edge dislocations under Borrmann effect conditions was carried out in cases when the diffraction vector was parallel or perpendicular to the slip plane of the dislocation. In both cases, the main part of the experimental image is formed because of waveguiding of Bloch waves in the regions of tension and compression of the lattice on either side of the slip plane. Additional image details arise through relaxation of stresses at the exit surface. Since the color of all lobes of the contrast rosette is related to the sign of the deformation, the location of the dislocation half‐plane is unambiguously determined. Thus, from the form of the rosette image, it is possible to obtain the slip plane, the magnitude and sign of the Burger's vector, and the direction of the dislocation line. |
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O. ; Verozubova, G. A.</creator><creatorcontrib>Okunev, A. O. ; Verozubova, G. A.</creatorcontrib><description>X‐ray topography images in the form of contrast rosettes from edge dislocations of the slip system in ZnGeP2 single crystals, obtained under different diffraction conditions, are identified and interpreted. To analyze and model the dislocation images, a semi‐phenomenological theory of contrast is applied. The simulation of images of edge dislocations under Borrmann effect conditions was carried out in cases when the diffraction vector was parallel or perpendicular to the slip plane of the dislocation. In both cases, the main part of the experimental image is formed because of waveguiding of Bloch waves in the regions of tension and compression of the lattice on either side of the slip plane. Additional image details arise through relaxation of stresses at the exit surface. Since the color of all lobes of the contrast rosette is related to the sign of the deformation, the location of the dislocation half‐plane is unambiguously determined. Thus, from the form of the rosette image, it is possible to obtain the slip plane, the magnitude and sign of the Burger's vector, and the direction of the dislocation line.</description><identifier>ISSN: 1600-5767</identifier><identifier>ISSN: 0021-8898</identifier><identifier>EISSN: 1600-5767</identifier><identifier>DOI: 10.1107/S1600576715012571</identifier><language>eng</language><publisher>5 Abbey Square, Chester, Cheshire CH1 2HU, England: International Union of Crystallography</publisher><subject>Borrmann effect ; edge dislocations ; modeling ; Single crystals ; Topography ; X-ray topography ; X-rays</subject><ispartof>Journal of applied crystallography, 2015-08, Vol.48 (4), p.1228-1233</ispartof><rights>International Union of Crystallography, 2015</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1107%2FS1600576715012571$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1107%2FS1600576715012571$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,776,780,1411,27901,27902,45550,45551</link.rule.ids></links><search><creatorcontrib>Okunev, A. O.</creatorcontrib><creatorcontrib>Verozubova, G. A.</creatorcontrib><title>X-ray topography contrast from edge dislocations in ZnGeP2 single crystals</title><title>Journal of applied crystallography</title><addtitle>Jnl Applied Crystallography</addtitle><description>X‐ray topography images in the form of contrast rosettes from edge dislocations of the slip system in ZnGeP2 single crystals, obtained under different diffraction conditions, are identified and interpreted. To analyze and model the dislocation images, a semi‐phenomenological theory of contrast is applied. The simulation of images of edge dislocations under Borrmann effect conditions was carried out in cases when the diffraction vector was parallel or perpendicular to the slip plane of the dislocation. In both cases, the main part of the experimental image is formed because of waveguiding of Bloch waves in the regions of tension and compression of the lattice on either side of the slip plane. Additional image details arise through relaxation of stresses at the exit surface. Since the color of all lobes of the contrast rosette is related to the sign of the deformation, the location of the dislocation half‐plane is unambiguously determined. Thus, from the form of the rosette image, it is possible to obtain the slip plane, the magnitude and sign of the Burger's vector, and the direction of the dislocation line.</description><subject>Borrmann effect</subject><subject>edge dislocations</subject><subject>modeling</subject><subject>Single crystals</subject><subject>Topography</subject><subject>X-ray topography</subject><subject>X-rays</subject><issn>1600-5767</issn><issn>0021-8898</issn><issn>1600-5767</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2015</creationdate><recordtype>article</recordtype><recordid>eNplkF9LwzAUxYsoOKcfwLeAz9WbpGnaRylucwz_TGXqS7hrspnZtTXp0H57OyYi-HQOh_O7F04QnFI4pxTkxQONAYSMJRVAmZB0L-hto3Cb7f_xh8GR9ysAGkvGesH4OXTYkqaqq6XD-q0leVU2Dn1DFq5aE6OXhmjriyrHxlalJ7Ykr-XQ3DHibbksDMld6xss_HFwsOjEnPxoP3gaXD1mo3ByO7zOLiehZZLyUOeCRXOIFsi1SFHLJMEEdYTMcGFwzrRAiBeYGJFTLXmSUoaUzbnhUYoR4_3gbHe3dtXHxvhGraqNK7uXikoABhwS6FrprvVpC9Oq2tk1ulZRUNu91L-91DibspepAOAdG-5Y6xvz9cuie1ex5FKo2c1QZfczOk4GmRrxb9TGbqI</recordid><startdate>20150801</startdate><enddate>20150801</enddate><creator>Okunev, A. O.</creator><creator>Verozubova, G. A.</creator><general>International Union of Crystallography</general><general>Blackwell Publishing Ltd</general><scope>BSCLL</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20150801</creationdate><title>X-ray topography contrast from edge dislocations in ZnGeP2 single crystals</title><author>Okunev, A. O. ; Verozubova, G. A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-i2713-dc524b04fa3d59ad788a8ad4a2e35eab2d5a06fa8e5c1d738912a12b3e349a423</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2015</creationdate><topic>Borrmann effect</topic><topic>edge dislocations</topic><topic>modeling</topic><topic>Single crystals</topic><topic>Topography</topic><topic>X-ray topography</topic><topic>X-rays</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Okunev, A. O.</creatorcontrib><creatorcontrib>Verozubova, G. A.</creatorcontrib><collection>Istex</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of applied crystallography</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Okunev, A. O.</au><au>Verozubova, G. A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>X-ray topography contrast from edge dislocations in ZnGeP2 single crystals</atitle><jtitle>Journal of applied crystallography</jtitle><addtitle>Jnl Applied Crystallography</addtitle><date>2015-08-01</date><risdate>2015</risdate><volume>48</volume><issue>4</issue><spage>1228</spage><epage>1233</epage><pages>1228-1233</pages><issn>1600-5767</issn><issn>0021-8898</issn><eissn>1600-5767</eissn><abstract>X‐ray topography images in the form of contrast rosettes from edge dislocations of the slip system in ZnGeP2 single crystals, obtained under different diffraction conditions, are identified and interpreted. To analyze and model the dislocation images, a semi‐phenomenological theory of contrast is applied. The simulation of images of edge dislocations under Borrmann effect conditions was carried out in cases when the diffraction vector was parallel or perpendicular to the slip plane of the dislocation. In both cases, the main part of the experimental image is formed because of waveguiding of Bloch waves in the regions of tension and compression of the lattice on either side of the slip plane. Additional image details arise through relaxation of stresses at the exit surface. Since the color of all lobes of the contrast rosette is related to the sign of the deformation, the location of the dislocation half‐plane is unambiguously determined. Thus, from the form of the rosette image, it is possible to obtain the slip plane, the magnitude and sign of the Burger's vector, and the direction of the dislocation line.</abstract><cop>5 Abbey Square, Chester, Cheshire CH1 2HU, England</cop><pub>International Union of Crystallography</pub><doi>10.1107/S1600576715012571</doi><tpages>6</tpages></addata></record> |
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subjects | Borrmann effect edge dislocations modeling Single crystals Topography X-ray topography X-rays |
title | X-ray topography contrast from edge dislocations in ZnGeP2 single crystals |
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