Development of a monochromator for aberration-corrected scanning transmission electron microscopy

In this article, we report the development of a new 200-kV analytical electron microscope equipped with a monochromator with an integrated double Wien-filter system. It enables us to study the electronic structures of materials in detail using electron energy-loss spectroscopy (EELS) analysis at an...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Journal of electron microscopy 2015-06, Vol.64 (3), p.151
Hauptverfasser: Mukai, Masaki, Okunishi, Eiji, Ashino, Masanori, Omoto, Kazuya, Fukuda, Tomohisa, Ikeda, Akihiro, Somehara, Kazunori, Kaneyama, Toshikatsu, Saitoh, Tomohiro, Hirayama, Tsukasa, Ikuhara, Yuichi
Format: Artikel
Sprache:eng
Schlagworte:
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
container_end_page
container_issue 3
container_start_page 151
container_title Journal of electron microscopy
container_volume 64
creator Mukai, Masaki
Okunishi, Eiji
Ashino, Masanori
Omoto, Kazuya
Fukuda, Tomohisa
Ikeda, Akihiro
Somehara, Kazunori
Kaneyama, Toshikatsu
Saitoh, Tomohiro
Hirayama, Tsukasa
Ikuhara, Yuichi
description In this article, we report the development of a new 200-kV analytical electron microscope equipped with a monochromator with an integrated double Wien-filter system. It enables us to study the electronic structures of materials in detail using electron energy-loss spectroscopy (EELS) analysis at an atomic scale. A highly monochromated and isotropically round electron probe is produced on the specimen plane. The ultimate energy resolutions with 0.1-s acquisition times are measured to be 36 meV at 200 kV and 30 meV at 60 kV. In an EELS mapping experiment performed on SrTiO... with a monochromated electron probe whose energy resolution is 146 meV, an elemental map exhibits atomic resolution. (ProQuest: ... denotes formulae/symbols omitted.)
format Article
fullrecord <record><control><sourceid>proquest</sourceid><recordid>TN_cdi_proquest_journals_1686087473</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>3705623491</sourcerecordid><originalsourceid>FETCH-proquest_journals_16860874733</originalsourceid><addsrcrecordid>eNqNyk0KwjAQBeAgCtafOwRcF6a1mu79wQO4lxinWmkydSYVvL1ZeAAXj_fgeyOVlbCBfGOgGKsMoCxzMFU1VTORJ0BhqgIyZff4xo56jyFqarTVngK5B5O3kVg3KfaKzDa2FHJHzOgi3rQ4G0Ib7jqyDeJbkeQau6Schm8dkzjqPws1aWwnuPz1XK2Oh_PulPdMrwElXp40cEh0Kbb1FmpTmfX6v9cXIjVIRA</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1686087473</pqid></control><display><type>article</type><title>Development of a monochromator for aberration-corrected scanning transmission electron microscopy</title><source>Alma/SFX Local Collection</source><creator>Mukai, Masaki ; Okunishi, Eiji ; Ashino, Masanori ; Omoto, Kazuya ; Fukuda, Tomohisa ; Ikeda, Akihiro ; Somehara, Kazunori ; Kaneyama, Toshikatsu ; Saitoh, Tomohiro ; Hirayama, Tsukasa ; Ikuhara, Yuichi</creator><creatorcontrib>Mukai, Masaki ; Okunishi, Eiji ; Ashino, Masanori ; Omoto, Kazuya ; Fukuda, Tomohisa ; Ikeda, Akihiro ; Somehara, Kazunori ; Kaneyama, Toshikatsu ; Saitoh, Tomohiro ; Hirayama, Tsukasa ; Ikuhara, Yuichi</creatorcontrib><description>In this article, we report the development of a new 200-kV analytical electron microscope equipped with a monochromator with an integrated double Wien-filter system. It enables us to study the electronic structures of materials in detail using electron energy-loss spectroscopy (EELS) analysis at an atomic scale. A highly monochromated and isotropically round electron probe is produced on the specimen plane. The ultimate energy resolutions with 0.1-s acquisition times are measured to be 36 meV at 200 kV and 30 meV at 60 kV. In an EELS mapping experiment performed on SrTiO... with a monochromated electron probe whose energy resolution is 146 meV, an elemental map exhibits atomic resolution. (ProQuest: ... denotes formulae/symbols omitted.)</description><identifier>ISSN: 0022-0744</identifier><identifier>EISSN: 2050-5701</identifier><language>eng</language><publisher>Oxford: Oxford Publishing Limited (England)</publisher><subject>Electrons ; Molecular structure ; Optics ; Scanning electron microscopy ; Spectrum analysis ; Transmission electron microscopy</subject><ispartof>Journal of electron microscopy, 2015-06, Vol.64 (3), p.151</ispartof><rights>Copyright Oxford Publishing Limited(England) Jun 2015</rights><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784</link.rule.ids></links><search><creatorcontrib>Mukai, Masaki</creatorcontrib><creatorcontrib>Okunishi, Eiji</creatorcontrib><creatorcontrib>Ashino, Masanori</creatorcontrib><creatorcontrib>Omoto, Kazuya</creatorcontrib><creatorcontrib>Fukuda, Tomohisa</creatorcontrib><creatorcontrib>Ikeda, Akihiro</creatorcontrib><creatorcontrib>Somehara, Kazunori</creatorcontrib><creatorcontrib>Kaneyama, Toshikatsu</creatorcontrib><creatorcontrib>Saitoh, Tomohiro</creatorcontrib><creatorcontrib>Hirayama, Tsukasa</creatorcontrib><creatorcontrib>Ikuhara, Yuichi</creatorcontrib><title>Development of a monochromator for aberration-corrected scanning transmission electron microscopy</title><title>Journal of electron microscopy</title><description>In this article, we report the development of a new 200-kV analytical electron microscope equipped with a monochromator with an integrated double Wien-filter system. It enables us to study the electronic structures of materials in detail using electron energy-loss spectroscopy (EELS) analysis at an atomic scale. A highly monochromated and isotropically round electron probe is produced on the specimen plane. The ultimate energy resolutions with 0.1-s acquisition times are measured to be 36 meV at 200 kV and 30 meV at 60 kV. In an EELS mapping experiment performed on SrTiO... with a monochromated electron probe whose energy resolution is 146 meV, an elemental map exhibits atomic resolution. (ProQuest: ... denotes formulae/symbols omitted.)</description><subject>Electrons</subject><subject>Molecular structure</subject><subject>Optics</subject><subject>Scanning electron microscopy</subject><subject>Spectrum analysis</subject><subject>Transmission electron microscopy</subject><issn>0022-0744</issn><issn>2050-5701</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2015</creationdate><recordtype>article</recordtype><recordid>eNqNyk0KwjAQBeAgCtafOwRcF6a1mu79wQO4lxinWmkydSYVvL1ZeAAXj_fgeyOVlbCBfGOgGKsMoCxzMFU1VTORJ0BhqgIyZff4xo56jyFqarTVngK5B5O3kVg3KfaKzDa2FHJHzOgi3rQ4G0Ib7jqyDeJbkeQau6Schm8dkzjqPws1aWwnuPz1XK2Oh_PulPdMrwElXp40cEh0Kbb1FmpTmfX6v9cXIjVIRA</recordid><startdate>20150601</startdate><enddate>20150601</enddate><creator>Mukai, Masaki</creator><creator>Okunishi, Eiji</creator><creator>Ashino, Masanori</creator><creator>Omoto, Kazuya</creator><creator>Fukuda, Tomohisa</creator><creator>Ikeda, Akihiro</creator><creator>Somehara, Kazunori</creator><creator>Kaneyama, Toshikatsu</creator><creator>Saitoh, Tomohiro</creator><creator>Hirayama, Tsukasa</creator><creator>Ikuhara, Yuichi</creator><general>Oxford Publishing Limited (England)</general><scope>7QF</scope><scope>7QO</scope><scope>7QQ</scope><scope>7SC</scope><scope>7SE</scope><scope>7SP</scope><scope>7SR</scope><scope>7TA</scope><scope>7TB</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>F28</scope><scope>FR3</scope><scope>H8D</scope><scope>H8G</scope><scope>JG9</scope><scope>JQ2</scope><scope>K9.</scope><scope>KR7</scope><scope>L7M</scope><scope>L~C</scope><scope>L~D</scope><scope>NAPCQ</scope><scope>P64</scope></search><sort><creationdate>20150601</creationdate><title>Development of a monochromator for aberration-corrected scanning transmission electron microscopy</title><author>Mukai, Masaki ; Okunishi, Eiji ; Ashino, Masanori ; Omoto, Kazuya ; Fukuda, Tomohisa ; Ikeda, Akihiro ; Somehara, Kazunori ; Kaneyama, Toshikatsu ; Saitoh, Tomohiro ; Hirayama, Tsukasa ; Ikuhara, Yuichi</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-proquest_journals_16860874733</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2015</creationdate><topic>Electrons</topic><topic>Molecular structure</topic><topic>Optics</topic><topic>Scanning electron microscopy</topic><topic>Spectrum analysis</topic><topic>Transmission electron microscopy</topic><toplevel>online_resources</toplevel><creatorcontrib>Mukai, Masaki</creatorcontrib><creatorcontrib>Okunishi, Eiji</creatorcontrib><creatorcontrib>Ashino, Masanori</creatorcontrib><creatorcontrib>Omoto, Kazuya</creatorcontrib><creatorcontrib>Fukuda, Tomohisa</creatorcontrib><creatorcontrib>Ikeda, Akihiro</creatorcontrib><creatorcontrib>Somehara, Kazunori</creatorcontrib><creatorcontrib>Kaneyama, Toshikatsu</creatorcontrib><creatorcontrib>Saitoh, Tomohiro</creatorcontrib><creatorcontrib>Hirayama, Tsukasa</creatorcontrib><creatorcontrib>Ikuhara, Yuichi</creatorcontrib><collection>Aluminium Industry Abstracts</collection><collection>Biotechnology Research Abstracts</collection><collection>Ceramic Abstracts</collection><collection>Computer and Information Systems Abstracts</collection><collection>Corrosion Abstracts</collection><collection>Electronics &amp; Communications Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Materials Business File</collection><collection>Mechanical &amp; Transportation Engineering Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ANTE: Abstracts in New Technology &amp; Engineering</collection><collection>Engineering Research Database</collection><collection>Aerospace Database</collection><collection>Copper Technical Reference Library</collection><collection>Materials Research Database</collection><collection>ProQuest Computer Science Collection</collection><collection>ProQuest Health &amp; Medical Complete (Alumni)</collection><collection>Civil Engineering Abstracts</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Computer and Information Systems Abstracts – Academic</collection><collection>Computer and Information Systems Abstracts Professional</collection><collection>Nursing &amp; Allied Health Premium</collection><collection>Biotechnology and BioEngineering Abstracts</collection><jtitle>Journal of electron microscopy</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Mukai, Masaki</au><au>Okunishi, Eiji</au><au>Ashino, Masanori</au><au>Omoto, Kazuya</au><au>Fukuda, Tomohisa</au><au>Ikeda, Akihiro</au><au>Somehara, Kazunori</au><au>Kaneyama, Toshikatsu</au><au>Saitoh, Tomohiro</au><au>Hirayama, Tsukasa</au><au>Ikuhara, Yuichi</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Development of a monochromator for aberration-corrected scanning transmission electron microscopy</atitle><jtitle>Journal of electron microscopy</jtitle><date>2015-06-01</date><risdate>2015</risdate><volume>64</volume><issue>3</issue><spage>151</spage><pages>151-</pages><issn>0022-0744</issn><eissn>2050-5701</eissn><abstract>In this article, we report the development of a new 200-kV analytical electron microscope equipped with a monochromator with an integrated double Wien-filter system. It enables us to study the electronic structures of materials in detail using electron energy-loss spectroscopy (EELS) analysis at an atomic scale. A highly monochromated and isotropically round electron probe is produced on the specimen plane. The ultimate energy resolutions with 0.1-s acquisition times are measured to be 36 meV at 200 kV and 30 meV at 60 kV. In an EELS mapping experiment performed on SrTiO... with a monochromated electron probe whose energy resolution is 146 meV, an elemental map exhibits atomic resolution. (ProQuest: ... denotes formulae/symbols omitted.)</abstract><cop>Oxford</cop><pub>Oxford Publishing Limited (England)</pub></addata></record>
fulltext fulltext
identifier ISSN: 0022-0744
ispartof Journal of electron microscopy, 2015-06, Vol.64 (3), p.151
issn 0022-0744
2050-5701
language eng
recordid cdi_proquest_journals_1686087473
source Alma/SFX Local Collection
subjects Electrons
Molecular structure
Optics
Scanning electron microscopy
Spectrum analysis
Transmission electron microscopy
title Development of a monochromator for aberration-corrected scanning transmission electron microscopy
url https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-12-28T11%3A33%3A30IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Development%20of%20a%20monochromator%20for%20aberration-corrected%20scanning%20transmission%20electron%20microscopy&rft.jtitle=Journal%20of%20electron%20microscopy&rft.au=Mukai,%20Masaki&rft.date=2015-06-01&rft.volume=64&rft.issue=3&rft.spage=151&rft.pages=151-&rft.issn=0022-0744&rft.eissn=2050-5701&rft_id=info:doi/&rft_dat=%3Cproquest%3E3705623491%3C/proquest%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=1686087473&rft_id=info:pmid/&rfr_iscdi=true