Synthesis and characterization of electrospun iron-doped lithium titanate/carbon nanofiber mats
In this paper, nanofibers composed of spinel Li 4 Ti 5−x Fe x O 12 (x = 0 and 0.1)/carbon were synthetized by electrospinning method. Thermal analysis of the prepared fiber was conducted by differential thermal/thermogravimetric analysis, crystal structure was characterized by X-ray diffraction, mor...
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| Veröffentlicht in: | Journal of materials science. Materials in electronics 2015-06, Vol.26 (6), p.4241-4249 |
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| container_title | Journal of materials science. Materials in electronics |
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| creator | Hernandez-Carrillo, Rubi A. Garcia-Gomez, Nora A. Garcia-Gutierrez, Domingo I. Garza-Tovar, Lorena L. Sanchez, Eduardo M. |
| description | In this paper, nanofibers composed of spinel Li
4
Ti
5−x
Fe
x
O
12
(x = 0 and 0.1)/carbon were synthetized by electrospinning method. Thermal analysis of the prepared fiber was conducted by differential thermal/thermogravimetric analysis, crystal structure was characterized by X-ray diffraction, morphology and composition was determined by scanning electron and transmission electron microscopy. The results showed that fibers were composed of nanocrystals of lithium titanate with an average diameter from 17 to 25 nm supported in a carbonaceous matrix. The added Fe played an important role in improving the electronic conductivity and the charge-transfer process of the Li
4
Ti
4.9
Fe
0.1
O
12
/C electrode. Due to the morphological and structural features of these novel nanostructured materials, it can be considered as promising candidates for applications in lithium ion batteries. |
| doi_str_mv | 10.1007/s10854-015-2974-7 |
| format | Article |
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4
Ti
5−x
Fe
x
O
12
(x = 0 and 0.1)/carbon were synthetized by electrospinning method. Thermal analysis of the prepared fiber was conducted by differential thermal/thermogravimetric analysis, crystal structure was characterized by X-ray diffraction, morphology and composition was determined by scanning electron and transmission electron microscopy. The results showed that fibers were composed of nanocrystals of lithium titanate with an average diameter from 17 to 25 nm supported in a carbonaceous matrix. The added Fe played an important role in improving the electronic conductivity and the charge-transfer process of the Li
4
Ti
4.9
Fe
0.1
O
12
/C electrode. Due to the morphological and structural features of these novel nanostructured materials, it can be considered as promising candidates for applications in lithium ion batteries.</description><identifier>ISSN: 0957-4522</identifier><identifier>EISSN: 1573-482X</identifier><identifier>DOI: 10.1007/s10854-015-2974-7</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Materials Science ; Optical and Electronic Materials</subject><ispartof>Journal of materials science. Materials in electronics, 2015-06, Vol.26 (6), p.4241-4249</ispartof><rights>Springer Science+Business Media New York 2015</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c386t-a1c50ba777ae0442b780c3024f1f9aace1ecf65d37d73124523a9f73bf46954f3</citedby><cites>FETCH-LOGICAL-c386t-a1c50ba777ae0442b780c3024f1f9aace1ecf65d37d73124523a9f73bf46954f3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10854-015-2974-7$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10854-015-2974-7$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27903,27904,41467,42536,51298</link.rule.ids></links><search><creatorcontrib>Hernandez-Carrillo, Rubi A.</creatorcontrib><creatorcontrib>Garcia-Gomez, Nora A.</creatorcontrib><creatorcontrib>Garcia-Gutierrez, Domingo I.</creatorcontrib><creatorcontrib>Garza-Tovar, Lorena L.</creatorcontrib><creatorcontrib>Sanchez, Eduardo M.</creatorcontrib><title>Synthesis and characterization of electrospun iron-doped lithium titanate/carbon nanofiber mats</title><title>Journal of materials science. Materials in electronics</title><addtitle>J Mater Sci: Mater Electron</addtitle><description>In this paper, nanofibers composed of spinel Li
4
Ti
5−x
Fe
x
O
12
(x = 0 and 0.1)/carbon were synthetized by electrospinning method. Thermal analysis of the prepared fiber was conducted by differential thermal/thermogravimetric analysis, crystal structure was characterized by X-ray diffraction, morphology and composition was determined by scanning electron and transmission electron microscopy. The results showed that fibers were composed of nanocrystals of lithium titanate with an average diameter from 17 to 25 nm supported in a carbonaceous matrix. The added Fe played an important role in improving the electronic conductivity and the charge-transfer process of the Li
4
Ti
4.9
Fe
0.1
O
12
/C electrode. Due to the morphological and structural features of these novel nanostructured materials, it can be considered as promising candidates for applications in lithium ion batteries.</description><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Materials Science</subject><subject>Optical and Electronic Materials</subject><issn>0957-4522</issn><issn>1573-482X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2015</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp1kDtPwzAUhS0EEqXwA9gsMZva8SsZUcVLqsQASGzWjWNTV61TbGcov55UYWBhusv5ztX5ELpm9JZRqheZ0VoKQpkkVaMF0SdoxqTmRNTVxyma0UZqImRVnaOLnDeUUiV4PUPm9RDL2uWQMcQO2zUksMWl8A0l9BH3HrutsyX1eT9EHFIfSdfvXYe3oazDsMMlFIhQ3MJCakciQux9aF3COyj5Ep152GZ39Xvn6P3h_m35RFYvj8_LuxWxvFaFALOStqC1BkeFqFpdU8tpJTzzDYB1zFmvZMd1pzmrxiEcGq9564VqpPB8jm6m3n3qvwaXi9n0Q4rjS8NUTRlTiqsxxaaUHffk5LzZp7CDdDCMmqNHM3k0o0dz9Gj0yFQTk8ds_HTpT_O_0A-QfHdI</recordid><startdate>20150601</startdate><enddate>20150601</enddate><creator>Hernandez-Carrillo, Rubi A.</creator><creator>Garcia-Gomez, Nora A.</creator><creator>Garcia-Gutierrez, Domingo I.</creator><creator>Garza-Tovar, Lorena L.</creator><creator>Sanchez, Eduardo M.</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SP</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>ARAPS</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>F28</scope><scope>FR3</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>L7M</scope><scope>P5Z</scope><scope>P62</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>S0W</scope></search><sort><creationdate>20150601</creationdate><title>Synthesis and characterization of electrospun iron-doped lithium titanate/carbon nanofiber mats</title><author>Hernandez-Carrillo, Rubi A. ; Garcia-Gomez, Nora A. ; Garcia-Gutierrez, Domingo I. ; Garza-Tovar, Lorena L. ; Sanchez, Eduardo M.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c386t-a1c50ba777ae0442b780c3024f1f9aace1ecf65d37d73124523a9f73bf46954f3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2015</creationdate><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Materials Science</topic><topic>Optical and Electronic Materials</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Hernandez-Carrillo, Rubi A.</creatorcontrib><creatorcontrib>Garcia-Gomez, Nora A.</creatorcontrib><creatorcontrib>Garcia-Gutierrez, Domingo I.</creatorcontrib><creatorcontrib>Garza-Tovar, Lorena L.</creatorcontrib><creatorcontrib>Sanchez, Eduardo M.</creatorcontrib><collection>CrossRef</collection><collection>Electronics & Communications Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central</collection><collection>Advanced Technologies & Aerospace Database (1962 - current)</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>SciTech Premium Collection (Proquest) (PQ_SDU_P3)</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Advanced Technologies & Aerospace Database</collection><collection>ProQuest Advanced Technologies & Aerospace Collection</collection><collection>Materials science collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>DELNET Engineering & Technology Collection</collection><jtitle>Journal of materials science. Materials in electronics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Hernandez-Carrillo, Rubi A.</au><au>Garcia-Gomez, Nora A.</au><au>Garcia-Gutierrez, Domingo I.</au><au>Garza-Tovar, Lorena L.</au><au>Sanchez, Eduardo M.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and characterization of electrospun iron-doped lithium titanate/carbon nanofiber mats</atitle><jtitle>Journal of materials science. Materials in electronics</jtitle><stitle>J Mater Sci: Mater Electron</stitle><date>2015-06-01</date><risdate>2015</risdate><volume>26</volume><issue>6</issue><spage>4241</spage><epage>4249</epage><pages>4241-4249</pages><issn>0957-4522</issn><eissn>1573-482X</eissn><abstract>In this paper, nanofibers composed of spinel Li
4
Ti
5−x
Fe
x
O
12
(x = 0 and 0.1)/carbon were synthetized by electrospinning method. Thermal analysis of the prepared fiber was conducted by differential thermal/thermogravimetric analysis, crystal structure was characterized by X-ray diffraction, morphology and composition was determined by scanning electron and transmission electron microscopy. The results showed that fibers were composed of nanocrystals of lithium titanate with an average diameter from 17 to 25 nm supported in a carbonaceous matrix. The added Fe played an important role in improving the electronic conductivity and the charge-transfer process of the Li
4
Ti
4.9
Fe
0.1
O
12
/C electrode. Due to the morphological and structural features of these novel nanostructured materials, it can be considered as promising candidates for applications in lithium ion batteries.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10854-015-2974-7</doi><tpages>9</tpages></addata></record> |
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| subjects | Characterization and Evaluation of Materials Chemistry and Materials Science Materials Science Optical and Electronic Materials |
| title | Synthesis and characterization of electrospun iron-doped lithium titanate/carbon nanofiber mats |
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