Changes in Volatile Compounds of Black Cumin (Nigella Sativa L.) Seed Oil During Thermal Oxidation
This study examined the oxidation stability and volatile compounds in samples of black cumin seed oil at 60 and 100°C. Oxidative changes of black cumin oils followed by periodic determination of its conjugated dienes and trienes during accelerated conditions (60 and 100°C). Black cumin oil showed hi...
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Veröffentlicht in: | International journal of food properties 2014-08, Vol.17 (7), p.1482-1489 |
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description | This study examined the oxidation stability and volatile compounds in samples of black cumin seed oil at 60 and 100°C. Oxidative changes of black cumin oils followed by periodic determination of its conjugated dienes and trienes during accelerated conditions (60 and 100°C). Black cumin oil showed high resistance to oxidation during thermal oxidation (60 and 100°C). In addition to oxidative stability, volatile compounds in the oil were determined by headspace solid phase microextraction with gas chromatography-mass spectrometry analysis technique. The major componenent of the oil was p-cymene (44.77%) followed by thymoquinone (28.62%). Some volatile compounds were lost rapidly during thermal oxidation at the end of storage. Levels of thymoquinone, 4-terpineol, α-longipinene, carvacrol, and isolongifolene reduced slowly and remained more stable during storage at two temperatures (60 and 100°C). |
doi_str_mv | 10.1080/10942912.2012.723231 |
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Levels of thymoquinone, 4-terpineol, α-longipinene, carvacrol, and isolongifolene reduced slowly and remained more stable during storage at two temperatures (60 and 100°C).</description><identifier>ISSN: 1532-2386</identifier><identifier>ISSN: 1094-2912</identifier><identifier>EISSN: 1532-2386</identifier><identifier>DOI: 10.1080/10942912.2012.723231</identifier><language>eng</language><publisher>Abingdon: Taylor & Francis</publisher><subject>Black cumin oil ; carvacrol ; Chromatography ; food quality ; Food science ; gas-chromatography-mass spectrometry ; headspace analysis ; Mass spectrometry ; Nigella sativa ; Nigella sativa L ; Oils & fats ; Oxidation ; oxidative stability ; P-cymene ; seed oils ; solid phase microextraction ; temperature ; Thymoquinone ; VOCs ; volatile compounds ; Volatile organic compounds</subject><ispartof>International journal of food properties, 2014-08, Vol.17 (7), p.1482-1489</ispartof><rights>Copyright © Taylor & Francis Group, LLC</rights><rights>Copyright Taylor & Francis Ltd. 2014</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c359t-c54eaef54c7efe136f5f5cf6188946fd253a6b88d86794aa80186a93a698df413</citedby><cites>FETCH-LOGICAL-c359t-c54eaef54c7efe136f5f5cf6188946fd253a6b88d86794aa80186a93a698df413</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids></links><search><creatorcontrib>Kiralan, Mustafa</creatorcontrib><title>Changes in Volatile Compounds of Black Cumin (Nigella Sativa L.) Seed Oil During Thermal Oxidation</title><title>International journal of food properties</title><description>This study examined the oxidation stability and volatile compounds in samples of black cumin seed oil at 60 and 100°C. Oxidative changes of black cumin oils followed by periodic determination of its conjugated dienes and trienes during accelerated conditions (60 and 100°C). Black cumin oil showed high resistance to oxidation during thermal oxidation (60 and 100°C). In addition to oxidative stability, volatile compounds in the oil were determined by headspace solid phase microextraction with gas chromatography-mass spectrometry analysis technique. The major componenent of the oil was p-cymene (44.77%) followed by thymoquinone (28.62%). Some volatile compounds were lost rapidly during thermal oxidation at the end of storage. Levels of thymoquinone, 4-terpineol, α-longipinene, carvacrol, and isolongifolene reduced slowly and remained more stable during storage at two temperatures (60 and 100°C).</description><subject>Black cumin oil</subject><subject>carvacrol</subject><subject>Chromatography</subject><subject>food quality</subject><subject>Food science</subject><subject>gas-chromatography-mass spectrometry</subject><subject>headspace analysis</subject><subject>Mass spectrometry</subject><subject>Nigella sativa</subject><subject>Nigella sativa L</subject><subject>Oils & fats</subject><subject>Oxidation</subject><subject>oxidative stability</subject><subject>P-cymene</subject><subject>seed oils</subject><subject>solid phase microextraction</subject><subject>temperature</subject><subject>Thymoquinone</subject><subject>VOCs</subject><subject>volatile compounds</subject><subject>Volatile organic compounds</subject><issn>1532-2386</issn><issn>1094-2912</issn><issn>1532-2386</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><recordid>eNqFkc1OAyEUhSdGE7X6BiaSuNFFKwwDAyuj42_S2EWtW3KdgYrSoUJH7duLGU3cuQFy851zcw5ZdkDwiGCBTwmWRS5JPspxOsqc5pRsZDuE0XyYU8E3_7y3s90YXzAmghK8kz1Vz9DOdUS2RY_ewco6jSq_WPqubSLyBl04qF9R1S0ScXxv59o5QNMEvgMaj07QVOsGTaxDl12w7Rw9POuwAIcmn7ZJlG_3si0DLur9n3uQza6vHqrb4Xhyc1edj4c1ZXI1rFmhQRtW1KU2mlBumGG14UQIWXDT5IwCfxKiEbyUBYBIETjINJSiMQWhg-yo910G_9bpuFIvvgttWqkII4TJkpY8UUVP1cHHGLRRy2AXENaKYPXdpvptU323qfo2k-ysl9nW-JTvwwfXqBWsnQ8mQFvbqOg_Doe9gwGvYB6SYDZNAEt_wbiQjH4BEoiCvw</recordid><startdate>20140809</startdate><enddate>20140809</enddate><creator>Kiralan, Mustafa</creator><general>Taylor & Francis</general><general>Taylor & Francis Ltd</general><scope>FBQ</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7QR</scope><scope>8FD</scope><scope>FR3</scope><scope>P64</scope></search><sort><creationdate>20140809</creationdate><title>Changes in Volatile Compounds of Black Cumin (Nigella Sativa L.) 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Seed Oil During Thermal Oxidation</atitle><jtitle>International journal of food properties</jtitle><date>2014-08-09</date><risdate>2014</risdate><volume>17</volume><issue>7</issue><spage>1482</spage><epage>1489</epage><pages>1482-1489</pages><issn>1532-2386</issn><issn>1094-2912</issn><eissn>1532-2386</eissn><abstract>This study examined the oxidation stability and volatile compounds in samples of black cumin seed oil at 60 and 100°C. Oxidative changes of black cumin oils followed by periodic determination of its conjugated dienes and trienes during accelerated conditions (60 and 100°C). Black cumin oil showed high resistance to oxidation during thermal oxidation (60 and 100°C). In addition to oxidative stability, volatile compounds in the oil were determined by headspace solid phase microextraction with gas chromatography-mass spectrometry analysis technique. The major componenent of the oil was p-cymene (44.77%) followed by thymoquinone (28.62%). Some volatile compounds were lost rapidly during thermal oxidation at the end of storage. Levels of thymoquinone, 4-terpineol, α-longipinene, carvacrol, and isolongifolene reduced slowly and remained more stable during storage at two temperatures (60 and 100°C).</abstract><cop>Abingdon</cop><pub>Taylor & Francis</pub><doi>10.1080/10942912.2012.723231</doi><tpages>8</tpages></addata></record> |
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subjects | Black cumin oil carvacrol Chromatography food quality Food science gas-chromatography-mass spectrometry headspace analysis Mass spectrometry Nigella sativa Nigella sativa L Oils & fats Oxidation oxidative stability P-cymene seed oils solid phase microextraction temperature Thymoquinone VOCs volatile compounds Volatile organic compounds |
title | Changes in Volatile Compounds of Black Cumin (Nigella Sativa L.) Seed Oil During Thermal Oxidation |
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