Synthesis, spectroscopic and luminescent properties of nanosized powders of yttrium phosphates doped with Er^sup 3+^ ions
Here, we report synthesis of pure crystalline nanopowders of yttrium orthophosphate Y^sub 0.95^Er^sub 0.05^PO^sub 4^ with xenotime-type structure and hydrate of yttrium orthophosphate Y^sub 0.95^Er^sub 0.05^PO^sub 4^0.8H2O with rhabdophane-type structure using microwave-hydrothermal treatment of fre...
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| Veröffentlicht in: | Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology 2014-03, Vol.16 (3), p.1 |
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| container_title | Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology |
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| creator | Ryabochkina, Polina A Antoshkina, Svetlana A Vanetsev, Alexander S Sildos, Ilmo Gaitko, Olga M Kyashkin, Vladimir M Ushakov, Sergey N Panov, Andrey A Tabachkova, Natalie Yu Nishchev, Konstantin N |
| description | Here, we report synthesis of pure crystalline nanopowders of yttrium orthophosphate Y^sub 0.95^Er^sub 0.05^PO^sub 4^ with xenotime-type structure and hydrate of yttrium orthophosphate Y^sub 0.95^Er^sub 0.05^PO^sub 4^0.8H2O with rhabdophane-type structure using microwave-hydrothermal treatment of freshly precipitated gels. To establish phase composition of the synthesized nanopowders, we have carried out XRD analysis. Also, we have investigated their morphology by means of TEM and SAXS. We have registered scattered reflection spectra for synthesized Y^sub 0.95^Er^sub 0.05^PO^sub 4^ and Y^sub 0.95^Er^sub 0.05^PO^sub 4^0.8H2O powders. Also, we have obtained luminescent spectra of these nanocrystalline samples for ^sup 4^I^sub 13/2^ [arrow right] ^sup 4^I^sub 15/2^ transition of Er^sup 3+^ ion with excitation of ^sup 4^I^sub 11/2^ level. We have proposed the mode of application of nanocrystalline powders Y^sub 0.95^Er^sub 0.05^PO^sub 4^ and Y^sub 0.95^Er^sub 0.05^PO^sub 4^0.8H2O for the development of composite materials based on polymer capsules that are being used in targeted drug delivery.[PUBLICATION ABSTRACT] |
| doi_str_mv | 10.1007/s11051-014-2326-1 |
| format | Article |
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To establish phase composition of the synthesized nanopowders, we have carried out XRD analysis. Also, we have investigated their morphology by means of TEM and SAXS. We have registered scattered reflection spectra for synthesized Y^sub 0.95^Er^sub 0.05^PO^sub 4^ and Y^sub 0.95^Er^sub 0.05^PO^sub 4^0.8H2O powders. Also, we have obtained luminescent spectra of these nanocrystalline samples for ^sup 4^I^sub 13/2^ [arrow right] ^sup 4^I^sub 15/2^ transition of Er^sup 3+^ ion with excitation of ^sup 4^I^sub 11/2^ level. We have proposed the mode of application of nanocrystalline powders Y^sub 0.95^Er^sub 0.05^PO^sub 4^ and Y^sub 0.95^Er^sub 0.05^PO^sub 4^0.8H2O for the development of composite materials based on polymer capsules that are being used in targeted drug delivery.[PUBLICATION ABSTRACT]</description><identifier>ISSN: 1388-0764</identifier><identifier>EISSN: 1572-896X</identifier><identifier>DOI: 10.1007/s11051-014-2326-1</identifier><language>eng</language><publisher>Dordrecht: Springer Nature B.V</publisher><subject>Composite materials ; Nanoparticles ; Polymers ; Yttrium</subject><ispartof>Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology, 2014-03, Vol.16 (3), p.1</ispartof><rights>Springer Science+Business Media Dordrecht 2014</rights><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids></links><search><creatorcontrib>Ryabochkina, Polina A</creatorcontrib><creatorcontrib>Antoshkina, Svetlana A</creatorcontrib><creatorcontrib>Vanetsev, Alexander S</creatorcontrib><creatorcontrib>Sildos, Ilmo</creatorcontrib><creatorcontrib>Gaitko, Olga M</creatorcontrib><creatorcontrib>Kyashkin, Vladimir M</creatorcontrib><creatorcontrib>Ushakov, Sergey N</creatorcontrib><creatorcontrib>Panov, Andrey A</creatorcontrib><creatorcontrib>Tabachkova, Natalie Yu</creatorcontrib><creatorcontrib>Nishchev, Konstantin N</creatorcontrib><title>Synthesis, spectroscopic and luminescent properties of nanosized powders of yttrium phosphates doped with Er^sup 3+^ ions</title><title>Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology</title><description>Here, we report synthesis of pure crystalline nanopowders of yttrium orthophosphate Y^sub 0.95^Er^sub 0.05^PO^sub 4^ with xenotime-type structure and hydrate of yttrium orthophosphate Y^sub 0.95^Er^sub 0.05^PO^sub 4^0.8H2O with rhabdophane-type structure using microwave-hydrothermal treatment of freshly precipitated gels. To establish phase composition of the synthesized nanopowders, we have carried out XRD analysis. Also, we have investigated their morphology by means of TEM and SAXS. We have registered scattered reflection spectra for synthesized Y^sub 0.95^Er^sub 0.05^PO^sub 4^ and Y^sub 0.95^Er^sub 0.05^PO^sub 4^0.8H2O powders. Also, we have obtained luminescent spectra of these nanocrystalline samples for ^sup 4^I^sub 13/2^ [arrow right] ^sup 4^I^sub 15/2^ transition of Er^sup 3+^ ion with excitation of ^sup 4^I^sub 11/2^ level. We have proposed the mode of application of nanocrystalline powders Y^sub 0.95^Er^sub 0.05^PO^sub 4^ and Y^sub 0.95^Er^sub 0.05^PO^sub 4^0.8H2O for the development of composite materials based on polymer capsules that are being used in targeted drug delivery.[PUBLICATION ABSTRACT]</description><subject>Composite 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properties of nanosized powders of yttrium phosphates doped with Er^sup 3+^ ions</atitle><jtitle>Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology</jtitle><date>2014-03-01</date><risdate>2014</risdate><volume>16</volume><issue>3</issue><spage>1</spage><pages>1-</pages><issn>1388-0764</issn><eissn>1572-896X</eissn><abstract>Here, we report synthesis of pure crystalline nanopowders of yttrium orthophosphate Y^sub 0.95^Er^sub 0.05^PO^sub 4^ with xenotime-type structure and hydrate of yttrium orthophosphate Y^sub 0.95^Er^sub 0.05^PO^sub 4^0.8H2O with rhabdophane-type structure using microwave-hydrothermal treatment of freshly precipitated gels. To establish phase composition of the synthesized nanopowders, we have carried out XRD analysis. Also, we have investigated their morphology by means of TEM and SAXS. We have registered scattered reflection spectra for synthesized Y^sub 0.95^Er^sub 0.05^PO^sub 4^ and Y^sub 0.95^Er^sub 0.05^PO^sub 4^0.8H2O powders. Also, we have obtained luminescent spectra of these nanocrystalline samples for ^sup 4^I^sub 13/2^ [arrow right] ^sup 4^I^sub 15/2^ transition of Er^sup 3+^ ion with excitation of ^sup 4^I^sub 11/2^ level. We have proposed the mode of application of nanocrystalline powders Y^sub 0.95^Er^sub 0.05^PO^sub 4^ and Y^sub 0.95^Er^sub 0.05^PO^sub 4^0.8H2O for the development of composite materials based on polymer capsules that are being used in targeted drug delivery.[PUBLICATION ABSTRACT]</abstract><cop>Dordrecht</cop><pub>Springer Nature B.V</pub><doi>10.1007/s11051-014-2326-1</doi></addata></record> |
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| language | eng |
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| subjects | Composite materials Nanoparticles Polymers Yttrium |
| title | Synthesis, spectroscopic and luminescent properties of nanosized powders of yttrium phosphates doped with Er^sup 3+^ ions |
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