Photocatalytic degradation of acetaminophen in modified TiO₂ under visible irradiation
This study investigated the photocatalytic degradation of acetaminophen (ACT) in synthetic titanium dioxide (TiO₂) solution under a visible light (λ >440 nm). The TiO₂ photocatalyst used in this study was synthesized via sol–gel method and doped with potassium aluminum sulfate (KAl(SO₄)₂) and sod...
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| Veröffentlicht in: | Environmental science and pollution research international 2014, Vol.21 (2), p.1208-1216 |
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| creator | Dalida, Maria Lourdes P Amer, Kristine Marfe S Su, Chia-Chi Lu, Ming-Chun |
| description | This study investigated the photocatalytic degradation of acetaminophen (ACT) in synthetic titanium dioxide (TiO₂) solution under a visible light (λ >440 nm). The TiO₂ photocatalyst used in this study was synthesized via sol–gel method and doped with potassium aluminum sulfate (KAl(SO₄)₂) and sodium aluminate (NaAlO₂). The influence of some parameters on the degradation of acetaminophen was examined, such as initial pH, photocatalyst dosage, and initial ACT concentration. The optimal operational conditions were also determined. Results showed that synthetic TiO₂ catalysts presented mainly as anatase phase and no rutile phase was observed. The results of photocatalytic degradation showed that LED alone degraded negligible amount of ACT but with the presence of TiO₂/KAl(SO₄)₂, 95 % removal of 0.10-mM acetaminophen in 540-min irradiation time was achieved. The synthetic TiO₂/KAl(SO₄)₂ presented better photocatalytic degradation of acetaminophen than commercially available Degussa P-25. The weak crystallinity of synthesized TiO₂/NaAlO₂ photocatalyst showed low photocatalytic degradation than TiO₂/KAl(SO₄)₂. The optimal operational conditions were obtained in pH 6.9 with a dose of 1.0 g/L TiO₂/KAl(SO₄)₂ at 30 °C. Kinetic study illustrated that photocatalytic degradation of acetaminophen fits well in the pseudo-first order model. Competitive reactions from intermediates affected the degradation rate of ACT, and were more obvious as the initial ACT concentration increased. |
| doi_str_mv | 10.1007/s11356-013-2003-4 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_1504829234</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>3239469381</sourcerecordid><originalsourceid>FETCH-LOGICAL-c433t-20df00655c7df6ca61fa1b90efbde7008af7941858dd6376288f2969439511c53</originalsourceid><addsrcrecordid>eNp9kMFOGzEQhi1URNKUB-ACljgvzNher32sUEsrRQpSQerNctZ2MErWwd4gceVReZJuuhT1xGkO83__jD5CThAuEKC5LIi8lhUgrxgAr8QBmaJEUTVC609kClqICrkQE_K5lAcABpo1R2TCuFKKCz0lv2_uU59a29v1cx9b6vwqW2f7mDqaArWt7-0mdml77zsaO7pJLoboHb2Ni9eXF7rrnM_0KZa4XHsa8wDHv_QXchjsuvjjtzkjd9-_3V79qOaL659XX-dVKzjvh79dAJB13TYuyNZKDBaXGnxYOt8AKBsaLVDVyjnJG8mUCkxLLbiuEduaz8j52LvN6XHnS28e0i53w0mDNQjFNONiSOGYanMqJftgtjlubH42CGbv0owuzeDS7F2aPXP61rxbbrx7J_7JGwJsDJRh1a18_u_0B61nIxRsMnaVYzF3vxigAIBaNsO3fwCYoYil</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1504829234</pqid></control><display><type>article</type><title>Photocatalytic degradation of acetaminophen in modified TiO₂ under visible irradiation</title><source>MEDLINE</source><source>SpringerLink Journals</source><creator>Dalida, Maria Lourdes P ; Amer, Kristine Marfe S ; Su, Chia-Chi ; Lu, Ming-Chun</creator><creatorcontrib>Dalida, Maria Lourdes P ; Amer, Kristine Marfe S ; Su, Chia-Chi ; Lu, Ming-Chun</creatorcontrib><description>This study investigated the photocatalytic degradation of acetaminophen (ACT) in synthetic titanium dioxide (TiO₂) solution under a visible light (λ >440 nm). The TiO₂ photocatalyst used in this study was synthesized via sol–gel method and doped with potassium aluminum sulfate (KAl(SO₄)₂) and sodium aluminate (NaAlO₂). The influence of some parameters on the degradation of acetaminophen was examined, such as initial pH, photocatalyst dosage, and initial ACT concentration. The optimal operational conditions were also determined. Results showed that synthetic TiO₂ catalysts presented mainly as anatase phase and no rutile phase was observed. The results of photocatalytic degradation showed that LED alone degraded negligible amount of ACT but with the presence of TiO₂/KAl(SO₄)₂, 95 % removal of 0.10-mM acetaminophen in 540-min irradiation time was achieved. The synthetic TiO₂/KAl(SO₄)₂ presented better photocatalytic degradation of acetaminophen than commercially available Degussa P-25. The weak crystallinity of synthesized TiO₂/NaAlO₂ photocatalyst showed low photocatalytic degradation than TiO₂/KAl(SO₄)₂. The optimal operational conditions were obtained in pH 6.9 with a dose of 1.0 g/L TiO₂/KAl(SO₄)₂ at 30 °C. Kinetic study illustrated that photocatalytic degradation of acetaminophen fits well in the pseudo-first order model. Competitive reactions from intermediates affected the degradation rate of ACT, and were more obvious as the initial ACT concentration increased.</description><identifier>ISSN: 0944-1344</identifier><identifier>EISSN: 1614-7499</identifier><identifier>DOI: 10.1007/s11356-013-2003-4</identifier><identifier>PMID: 23888349</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer-Verlag</publisher><subject>Acetaminophen ; Acetaminophen - analysis ; Acetaminophen - chemistry ; Aluminum ; Aluminum sulfate ; Analgesics ; Aquatic Pollution ; Atmospheric Protection/Air Quality Control/Air Pollution ; Bioremediation ; Catalysts ; crystal structure ; Degradation ; Earth and Environmental Science ; Ecotoxicology ; Environment ; Environmental Chemistry ; Environmental Health ; Ethanol ; Hydrogen-Ion Concentration ; Intermediates ; Irradiation ; Kinetics ; Lamps ; Light ; Light emitting diodes ; Nonsteroidal anti-inflammatory drugs ; Oxidation ; Pharmaceutical industry ; Photocatalysis ; Photodegradation ; Photolysis ; Potassium ; Radiation ; Research Article ; sodium ; Solutions ; Studies ; Titanium - analysis ; Titanium - chemistry ; Titanium dioxide ; Waste Water Technology ; Water Management ; Water Pollutants, Chemical - analysis ; Water Pollutants, Chemical - chemistry ; Water pollution ; Water Pollution Control</subject><ispartof>Environmental science and pollution research international, 2014, Vol.21 (2), p.1208-1216</ispartof><rights>Springer-Verlag Berlin Heidelberg 2013</rights><rights>Springer-Verlag Berlin Heidelberg 2014</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c433t-20df00655c7df6ca61fa1b90efbde7008af7941858dd6376288f2969439511c53</citedby><cites>FETCH-LOGICAL-c433t-20df00655c7df6ca61fa1b90efbde7008af7941858dd6376288f2969439511c53</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11356-013-2003-4$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11356-013-2003-4$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,4010,27900,27901,27902,41464,42533,51294</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/23888349$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Dalida, Maria Lourdes P</creatorcontrib><creatorcontrib>Amer, Kristine Marfe S</creatorcontrib><creatorcontrib>Su, Chia-Chi</creatorcontrib><creatorcontrib>Lu, Ming-Chun</creatorcontrib><title>Photocatalytic degradation of acetaminophen in modified TiO₂ under visible irradiation</title><title>Environmental science and pollution research international</title><addtitle>Environ Sci Pollut Res</addtitle><addtitle>Environ Sci Pollut Res Int</addtitle><description>This study investigated the photocatalytic degradation of acetaminophen (ACT) in synthetic titanium dioxide (TiO₂) solution under a visible light (λ >440 nm). The TiO₂ photocatalyst used in this study was synthesized via sol–gel method and doped with potassium aluminum sulfate (KAl(SO₄)₂) and sodium aluminate (NaAlO₂). The influence of some parameters on the degradation of acetaminophen was examined, such as initial pH, photocatalyst dosage, and initial ACT concentration. The optimal operational conditions were also determined. Results showed that synthetic TiO₂ catalysts presented mainly as anatase phase and no rutile phase was observed. The results of photocatalytic degradation showed that LED alone degraded negligible amount of ACT but with the presence of TiO₂/KAl(SO₄)₂, 95 % removal of 0.10-mM acetaminophen in 540-min irradiation time was achieved. The synthetic TiO₂/KAl(SO₄)₂ presented better photocatalytic degradation of acetaminophen than commercially available Degussa P-25. The weak crystallinity of synthesized TiO₂/NaAlO₂ photocatalyst showed low photocatalytic degradation than TiO₂/KAl(SO₄)₂. The optimal operational conditions were obtained in pH 6.9 with a dose of 1.0 g/L TiO₂/KAl(SO₄)₂ at 30 °C. Kinetic study illustrated that photocatalytic degradation of acetaminophen fits well in the pseudo-first order model. Competitive reactions from intermediates affected the degradation rate of ACT, and were more obvious as the initial ACT concentration increased.</description><subject>Acetaminophen</subject><subject>Acetaminophen - analysis</subject><subject>Acetaminophen - chemistry</subject><subject>Aluminum</subject><subject>Aluminum sulfate</subject><subject>Analgesics</subject><subject>Aquatic Pollution</subject><subject>Atmospheric Protection/Air Quality Control/Air Pollution</subject><subject>Bioremediation</subject><subject>Catalysts</subject><subject>crystal structure</subject><subject>Degradation</subject><subject>Earth and Environmental Science</subject><subject>Ecotoxicology</subject><subject>Environment</subject><subject>Environmental Chemistry</subject><subject>Environmental Health</subject><subject>Ethanol</subject><subject>Hydrogen-Ion Concentration</subject><subject>Intermediates</subject><subject>Irradiation</subject><subject>Kinetics</subject><subject>Lamps</subject><subject>Light</subject><subject>Light emitting diodes</subject><subject>Nonsteroidal anti-inflammatory drugs</subject><subject>Oxidation</subject><subject>Pharmaceutical industry</subject><subject>Photocatalysis</subject><subject>Photodegradation</subject><subject>Photolysis</subject><subject>Potassium</subject><subject>Radiation</subject><subject>Research Article</subject><subject>sodium</subject><subject>Solutions</subject><subject>Studies</subject><subject>Titanium - analysis</subject><subject>Titanium - chemistry</subject><subject>Titanium dioxide</subject><subject>Waste Water Technology</subject><subject>Water Management</subject><subject>Water Pollutants, Chemical - analysis</subject><subject>Water Pollutants, Chemical - chemistry</subject><subject>Water pollution</subject><subject>Water Pollution 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Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Dalida, Maria Lourdes P</au><au>Amer, Kristine Marfe S</au><au>Su, Chia-Chi</au><au>Lu, Ming-Chun</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Photocatalytic degradation of acetaminophen in modified TiO₂ under visible irradiation</atitle><jtitle>Environmental science and pollution research international</jtitle><stitle>Environ Sci Pollut Res</stitle><addtitle>Environ Sci Pollut Res Int</addtitle><date>2014</date><risdate>2014</risdate><volume>21</volume><issue>2</issue><spage>1208</spage><epage>1216</epage><pages>1208-1216</pages><issn>0944-1344</issn><eissn>1614-7499</eissn><abstract>This study investigated the photocatalytic degradation of acetaminophen (ACT) in synthetic titanium dioxide (TiO₂) solution under a visible light (λ >440 nm). The TiO₂ photocatalyst used in this study was synthesized via sol–gel method and doped with potassium aluminum sulfate (KAl(SO₄)₂) and sodium aluminate (NaAlO₂). The influence of some parameters on the degradation of acetaminophen was examined, such as initial pH, photocatalyst dosage, and initial ACT concentration. The optimal operational conditions were also determined. Results showed that synthetic TiO₂ catalysts presented mainly as anatase phase and no rutile phase was observed. The results of photocatalytic degradation showed that LED alone degraded negligible amount of ACT but with the presence of TiO₂/KAl(SO₄)₂, 95 % removal of 0.10-mM acetaminophen in 540-min irradiation time was achieved. The synthetic TiO₂/KAl(SO₄)₂ presented better photocatalytic degradation of acetaminophen than commercially available Degussa P-25. The weak crystallinity of synthesized TiO₂/NaAlO₂ photocatalyst showed low photocatalytic degradation than TiO₂/KAl(SO₄)₂. The optimal operational conditions were obtained in pH 6.9 with a dose of 1.0 g/L TiO₂/KAl(SO₄)₂ at 30 °C. Kinetic study illustrated that photocatalytic degradation of acetaminophen fits well in the pseudo-first order model. Competitive reactions from intermediates affected the degradation rate of ACT, and were more obvious as the initial ACT concentration increased.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer-Verlag</pub><pmid>23888349</pmid><doi>10.1007/s11356-013-2003-4</doi><tpages>9</tpages></addata></record> |
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| subjects | Acetaminophen Acetaminophen - analysis Acetaminophen - chemistry Aluminum Aluminum sulfate Analgesics Aquatic Pollution Atmospheric Protection/Air Quality Control/Air Pollution Bioremediation Catalysts crystal structure Degradation Earth and Environmental Science Ecotoxicology Environment Environmental Chemistry Environmental Health Ethanol Hydrogen-Ion Concentration Intermediates Irradiation Kinetics Lamps Light Light emitting diodes Nonsteroidal anti-inflammatory drugs Oxidation Pharmaceutical industry Photocatalysis Photodegradation Photolysis Potassium Radiation Research Article sodium Solutions Studies Titanium - analysis Titanium - chemistry Titanium dioxide Waste Water Technology Water Management Water Pollutants, Chemical - analysis Water Pollutants, Chemical - chemistry Water pollution Water Pollution Control |
| title | Photocatalytic degradation of acetaminophen in modified TiO₂ under visible irradiation |
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