Preparation and Selectivity Characteristics of FluorocarbonaceousBonded Stationary Phase for Reverse-Phase H igh-PerformanceLiquid Chromatography

Preparation and Selectivity Characteristics of FluorocarbonaceousBonded Stationary Phase for Reverse-Phase H igh-PerformanceLiquid Chromatography

1H, 1H, 2H, 2H, 3H, 3H-Tridecafluoro (4, 4-dimethylheptyl)silanes [3a-3c] were prepared from the corresponding polyfluoroalkene [1] and silanes HSiXY2 {2a; X=Y =C1, 2b X=C1, Y=CH3, 2c; X=Y=OCH3} in the presence of hexachloroplatinic(IV) acid in good yields (71-90%; Scheme 1 and Table 1). The product...

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Veröffentlicht in:Nippon Kagakukai shi (1972) 1991-12, Vol.1991 (12), p.1638
Hauptverfasser: KONAKAHARA, Takeo, OKADA, Shin-ichiro, MONDE, Takashi, NAKAYAMA, Nobuyuki, FURUHASHI, Jun, SUGAYA, Jun-ichi
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container_issue 12
container_start_page 1638
container_title Nippon Kagakukai shi (1972)
container_volume 1991
creator KONAKAHARA, Takeo
OKADA, Shin-ichiro
MONDE, Takashi
NAKAYAMA, Nobuyuki
FURUHASHI, Jun
SUGAYA, Jun-ichi
description 1H, 1H, 2H, 2H, 3H, 3H-Tridecafluoro (4, 4-dimethylheptyl)silanes [3a-3c] were prepared from the corresponding polyfluoroalkene [1] and silanes HSiXY2 {2a; X=Y =C1, 2b X=C1, Y=CH3, 2c; X=Y=OCH3} in the presence of hexachloroplatinic(IV) acid in good yields (71-90%; Scheme 1 and Table 1). The product silanes [3a, 3b] and Dimethyl(1H, 1H, 2H, 2H-tridecafluorooctyl)-chlorosilane [4] were used to prepare the corresponding new-type branched- and straight-fluorocarbonaceous bonded stationary phase (PES) for reverse-phase high-performance liquid chromatography (RP-HPLC).
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The product silanes [3a, 3b] and Dimethyl(1H, 1H, 2H, 2H-tridecafluorooctyl)-chlorosilane [4] were used to prepare the corresponding new-type branched- and straight-fluorocarbonaceous bonded stationary phase (PES) for reverse-phase high-performance liquid chromatography (RP-HPLC).</description><identifier>ISSN: 0369-4577</identifier><language>eng</language><publisher>Tokyo: Japan Science and Technology Agency</publisher><ispartof>Nippon Kagakukai shi (1972), 1991-12, Vol.1991 (12), p.1638</ispartof><rights>Copyright Japan Science and Technology Agency 1991</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784</link.rule.ids></links><search><creatorcontrib>KONAKAHARA, Takeo</creatorcontrib><creatorcontrib>OKADA, Shin-ichiro</creatorcontrib><creatorcontrib>MONDE, Takashi</creatorcontrib><creatorcontrib>NAKAYAMA, Nobuyuki</creatorcontrib><creatorcontrib>FURUHASHI, Jun</creatorcontrib><creatorcontrib>SUGAYA, Jun-ichi</creatorcontrib><title>Preparation and Selectivity Characteristics of FluorocarbonaceousBonded Stationary Phase for Reverse-Phase H igh-PerformanceLiquid Chromatography</title><title>Nippon Kagakukai shi (1972)</title><description>1H, 1H, 2H, 2H, 3H, 3H-Tridecafluoro (4, 4-dimethylheptyl)silanes [3a-3c] were prepared from the corresponding polyfluoroalkene [1] and silanes HSiXY2 {2a; X=Y =C1, 2b X=C1, Y=CH3, 2c; X=Y=OCH3} in the presence of hexachloroplatinic(IV) acid in good yields (71-90%; Scheme 1 and Table 1). 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title Preparation and Selectivity Characteristics of FluorocarbonaceousBonded Stationary Phase for Reverse-Phase H igh-PerformanceLiquid Chromatography
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