FLUORESCENCE REACTION OF COMMON EPOXIDES WITH NICOTINAMIDE AND ACETOPHENONE

FLUORESCENCE REACTION OF COMMON EPOXIDES WITH NICOTINAMIDE AND ACETOPHENONE

A spectrofluorometric method for determination of common epoxides based on a fluorescence reaction of the epoxy group with nicotinamide and acetophenone is described. By the method, as little as 10ng order of five aliphatic epoxides could be determined with a coefficient of variation of ca. 3 to 5%....

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:BUNSEKI KAGAKU 1983/04/05, Vol.32(4), pp.E93-E100
Hauptverfasser: SANO, Akira, ASABE, Yoshihiro, SUZUKI, Masao, TAKITANI, Shoji
Format: Artikel
Sprache:eng
Schlagworte:
acetophenone
determination of epoxides
fluorometry
mechanism
naphthyridines
nicotinamide
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
container_end_page E100
container_issue 4
container_start_page E93
container_title BUNSEKI KAGAKU
container_volume 32
creator SANO, Akira
ASABE, Yoshihiro
SUZUKI, Masao
TAKITANI, Shoji
description A spectrofluorometric method for determination of common epoxides based on a fluorescence reaction of the epoxy group with nicotinamide and acetophenone is described. By the method, as little as 10ng order of five aliphatic epoxides could be determined with a coefficient of variation of ca. 3 to 5%. The analysis of the reaction product showed that the fluorophore had a 2, 7-naphthyridine structure.
doi_str_mv 10.2116/bunsekikagaku.32.4_E93
format Article
fullrecord <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_1448933985</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>3119589171</sourcerecordid><originalsourceid>FETCH-LOGICAL-c467t-772da0fdbab56ede0f665a838a02ca03b0ce82ec32555653b9fd0eb66dfbd9ab3</originalsourceid><addsrcrecordid>eNpVkF1PwjAUhnehiYj-BbPEa7Afa9kul1Jkka0ERvSuabcO-RCw3S78906nJFydNyfPc07yet4DBEMEIX3SzcGZ3Wan1mrXDDEaBpJH-MrrAYLIAEYY3ni3zm0BQAQQ2PNeJrOVWPAl4xnj_oLHLE9E5ouJz0SatonPxVsy5kv_NcmnfpYwkSdZnLYrP87Gfsx4LuZTnomM33nXldo7c_83-95qwnM2HczEc8Li2aAI6KgejEaoVKAqtdKEmtKAilKiQhwqgAoFsAaFCZEpMCKEUIJ1VJXAaErLSpeR0rjvPXZ3T_b42RhXy-2xsYf2pYRBEEYYRyFpKdpRhT06Z00lT3bzoeyXhED-lCUvypIYyd-yWjHtxK2r1dqcNWXrTbE3lxqMCOrUf__MFe_KSnPA37XVeis</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1448933985</pqid></control><display><type>article</type><title>FLUORESCENCE REACTION OF COMMON EPOXIDES WITH NICOTINAMIDE AND ACETOPHENONE</title><source>EZB-FREE-00999 freely available EZB journals</source><source>Free Full-Text Journals in Chemistry</source><creator>SANO, Akira ; ASABE, Yoshihiro ; SUZUKI, Masao ; TAKITANI, Shoji</creator><creatorcontrib>SANO, Akira ; ASABE, Yoshihiro ; SUZUKI, Masao ; TAKITANI, Shoji</creatorcontrib><description>A spectrofluorometric method for determination of common epoxides based on a fluorescence reaction of the epoxy group with nicotinamide and acetophenone is described. By the method, as little as 10ng order of five aliphatic epoxides could be determined with a coefficient of variation of ca. 3 to 5%. The analysis of the reaction product showed that the fluorophore had a 2, 7-naphthyridine structure.</description><identifier>ISSN: 0525-1931</identifier><identifier>DOI: 10.2116/bunsekikagaku.32.4_E93</identifier><language>eng</language><publisher>Tokyo: The Japan Society for Analytical Chemistry</publisher><subject>acetophenone ; determination of epoxides ; fluorometry ; mechanism ; naphthyridines ; nicotinamide</subject><ispartof>BUNSEKI KAGAKU, 1983/04/05, Vol.32(4), pp.E93-E100</ispartof><rights>The Japan Society for Analytical Chemistry</rights><rights>Copyright Japan Science and Technology Agency 1983</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c467t-772da0fdbab56ede0f665a838a02ca03b0ce82ec32555653b9fd0eb66dfbd9ab3</citedby></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27923,27924</link.rule.ids></links><search><creatorcontrib>SANO, Akira</creatorcontrib><creatorcontrib>ASABE, Yoshihiro</creatorcontrib><creatorcontrib>SUZUKI, Masao</creatorcontrib><creatorcontrib>TAKITANI, Shoji</creatorcontrib><title>FLUORESCENCE REACTION OF COMMON EPOXIDES WITH NICOTINAMIDE AND ACETOPHENONE</title><title>BUNSEKI KAGAKU</title><addtitle>BUNSEKI KAGAKU</addtitle><description>A spectrofluorometric method for determination of common epoxides based on a fluorescence reaction of the epoxy group with nicotinamide and acetophenone is described. By the method, as little as 10ng order of five aliphatic epoxides could be determined with a coefficient of variation of ca. 3 to 5%. The analysis of the reaction product showed that the fluorophore had a 2, 7-naphthyridine structure.</description><subject>acetophenone</subject><subject>determination of epoxides</subject><subject>fluorometry</subject><subject>mechanism</subject><subject>naphthyridines</subject><subject>nicotinamide</subject><issn>0525-1931</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1983</creationdate><recordtype>article</recordtype><recordid>eNpVkF1PwjAUhnehiYj-BbPEa7Afa9kul1Jkka0ERvSuabcO-RCw3S78906nJFydNyfPc07yet4DBEMEIX3SzcGZ3Wan1mrXDDEaBpJH-MrrAYLIAEYY3ni3zm0BQAQQ2PNeJrOVWPAl4xnj_oLHLE9E5ouJz0SatonPxVsy5kv_NcmnfpYwkSdZnLYrP87Gfsx4LuZTnomM33nXldo7c_83-95qwnM2HczEc8Li2aAI6KgejEaoVKAqtdKEmtKAilKiQhwqgAoFsAaFCZEpMCKEUIJ1VJXAaErLSpeR0rjvPXZ3T_b42RhXy-2xsYf2pYRBEEYYRyFpKdpRhT06Z00lT3bzoeyXhED-lCUvypIYyd-yWjHtxK2r1dqcNWXrTbE3lxqMCOrUf__MFe_KSnPA37XVeis</recordid><startdate>19830101</startdate><enddate>19830101</enddate><creator>SANO, Akira</creator><creator>ASABE, Yoshihiro</creator><creator>SUZUKI, Masao</creator><creator>TAKITANI, Shoji</creator><general>The Japan Society for Analytical Chemistry</general><general>Japan Science and Technology Agency</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope></search><sort><creationdate>19830101</creationdate><title>FLUORESCENCE REACTION OF COMMON EPOXIDES WITH NICOTINAMIDE AND ACETOPHENONE</title><author>SANO, Akira ; ASABE, Yoshihiro ; SUZUKI, Masao ; TAKITANI, Shoji</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c467t-772da0fdbab56ede0f665a838a02ca03b0ce82ec32555653b9fd0eb66dfbd9ab3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1983</creationdate><topic>acetophenone</topic><topic>determination of epoxides</topic><topic>fluorometry</topic><topic>mechanism</topic><topic>naphthyridines</topic><topic>nicotinamide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>SANO, Akira</creatorcontrib><creatorcontrib>ASABE, Yoshihiro</creatorcontrib><creatorcontrib>SUZUKI, Masao</creatorcontrib><creatorcontrib>TAKITANI, Shoji</creatorcontrib><collection>CrossRef</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>BUNSEKI KAGAKU</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>SANO, Akira</au><au>ASABE, Yoshihiro</au><au>SUZUKI, Masao</au><au>TAKITANI, Shoji</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>FLUORESCENCE REACTION OF COMMON EPOXIDES WITH NICOTINAMIDE AND ACETOPHENONE</atitle><jtitle>BUNSEKI KAGAKU</jtitle><addtitle>BUNSEKI KAGAKU</addtitle><date>1983-01-01</date><risdate>1983</risdate><volume>32</volume><issue>4</issue><spage>E93</spage><epage>E100</epage><pages>E93-E100</pages><issn>0525-1931</issn><abstract>A spectrofluorometric method for determination of common epoxides based on a fluorescence reaction of the epoxy group with nicotinamide and acetophenone is described. By the method, as little as 10ng order of five aliphatic epoxides could be determined with a coefficient of variation of ca. 3 to 5%. The analysis of the reaction product showed that the fluorophore had a 2, 7-naphthyridine structure.</abstract><cop>Tokyo</cop><pub>The Japan Society for Analytical Chemistry</pub><doi>10.2116/bunsekikagaku.32.4_E93</doi><oa>free_for_read</oa></addata></record>
fulltext fulltext
identifier ISSN: 0525-1931
ispartof BUNSEKI KAGAKU, 1983/04/05, Vol.32(4), pp.E93-E100
issn 0525-1931
language eng
recordid cdi_proquest_journals_1448933985
source EZB-FREE-00999 freely available EZB journals; Free Full-Text Journals in Chemistry
subjects acetophenone
determination of epoxides
fluorometry
mechanism
naphthyridines
nicotinamide
title FLUORESCENCE REACTION OF COMMON EPOXIDES WITH NICOTINAMIDE AND ACETOPHENONE
url https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-10T11%3A29%3A04IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=FLUORESCENCE%20REACTION%20OF%20COMMON%20EPOXIDES%20WITH%20NICOTINAMIDE%20AND%20ACETOPHENONE&rft.jtitle=BUNSEKI%20KAGAKU&rft.au=SANO,%20Akira&rft.date=1983-01-01&rft.volume=32&rft.issue=4&rft.spage=E93&rft.epage=E100&rft.pages=E93-E100&rft.issn=0525-1931&rft_id=info:doi/10.2116/bunsekikagaku.32.4_E93&rft_dat=%3Cproquest_cross%3E3119589171%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=1448933985&rft_id=info:pmid/&rfr_iscdi=true