Determination of low molecular weight halogenated hydrocarbons by a gas chromatograph with a wide bore capillary column

Determination of low molecular weight halogenated hydrocarbons by a gas chromatograph with a wide bore capillary column

Low molecular weight halogenated hydrocarbons (LMHs) in industrial water and waste water have been determined according to JIS K 0125, in which a packed column has been used as the GC column. In this report, wide bore capillary columns were evaluated as a GC column. DB-624 showed the best separation...

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Veröffentlicht in:Bunseki kagaku 1990-08, Vol.39 (8), p.T113-T116
Hauptverfasser: HATTORI, Yukikazu, YAMAMOTO, Hitoshi, NAGAI, Kanji, HAGINO, Kiyoko, NAKAMOTO, Masao
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container_end_page T116
container_issue 8
container_start_page T113
container_title Bunseki kagaku
container_volume 39
creator HATTORI, Yukikazu
YAMAMOTO, Hitoshi
NAGAI, Kanji
HAGINO, Kiyoko
NAKAMOTO, Masao
description Low molecular weight halogenated hydrocarbons (LMHs) in industrial water and waste water have been determined according to JIS K 0125, in which a packed column has been used as the GC column. In this report, wide bore capillary columns were evaluated as a GC column. DB-624 showed the best separation ability of 5 kinds of column (DB-1, DB-5, DB-17, DB-624, DB-WAX). When hexane solution of LMHs was measured with DB-624, the relative standard deviations (RSD) of response (peak height) and retention time (RT) were 0.82.1% and 0.51.4%, respectively. When the head space method was used, the RSDs of response and RT were 3.45.0% and 0.040.20%, respectively.
doi_str_mv 10.2116/bunsekikagaku.39.8_T113
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title Determination of low molecular weight halogenated hydrocarbons by a gas chromatograph with a wide bore capillary column
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