Determination of Carboxybetaine Amphoteric Surfactants in Household and Cosmetic Products by High Performance Liquid Chromatography with Prelabeling
A high performance liquid chromatographic (HPLC) method is described for the determination of carboxybetaine amphoteric surfactants in commercial household and cosmetic products. The surfactants are prelabeled with 4-bromomethyl-7-methoxycoumarin and then are separated by reversed phase HPLC with a...
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| Veröffentlicht in: | Analytical Sciences 1986/10/10, Vol.2(5), pp.467-471 |
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| container_title | Analytical Sciences |
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| creator | KONDOH, Yukihiro TAKANO, Satoshi |
| description | A high performance liquid chromatographic (HPLC) method is described for the determination of carboxybetaine amphoteric surfactants in commercial household and cosmetic products. The surfactants are prelabeled with 4-bromomethyl-7-methoxycoumarin and then are separated by reversed phase HPLC with a gradient elution. The determination of carboxybetaines in shampoos was carried out by an internal standard method. The calibration curve was linear in the range from 0.007 to 4.6nmol. The relative standard deviation was found to be 1.0% for 0.46nmol injection. By using the proposed method, carboxybetaines in commercial household and cosmetic products were determined with high sensitivity and high selectivity. |
| doi_str_mv | 10.2116/analsci.2.467 |
| format | Article |
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The surfactants are prelabeled with 4-bromomethyl-7-methoxycoumarin and then are separated by reversed phase HPLC with a gradient elution. The determination of carboxybetaines in shampoos was carried out by an internal standard method. The calibration curve was linear in the range from 0.007 to 4.6nmol. The relative standard deviation was found to be 1.0% for 0.46nmol injection. By using the proposed method, carboxybetaines in commercial household and cosmetic products were determined with high sensitivity and high selectivity.</description><identifier>ISSN: 0910-6340</identifier><identifier>EISSN: 1348-2246</identifier><identifier>DOI: 10.2116/analsci.2.467</identifier><identifier>CODEN: ANSCEN</identifier><language>eng</language><publisher>Tokyo: The Japan Society for Analytical Chemistry</publisher><subject>4-bromomethyl-7-methoxycoumarin ; Applied sciences ; carboxybetaine amphoteric surfactants ; Chemical industry and chemicals ; Cosmetics, toiletries ; Exact sciences and technology ; High performance liquid chromatography ; prelabeling ; shampoo ; Washing products. Cosmetics and toiletries. Perfumes</subject><ispartof>Analytical Sciences, 1986/10/10, Vol.2(5), pp.467-471</ispartof><rights>The Japan Society for Analytical Chemistry</rights><rights>1987 INIST-CNRS</rights><rights>Copyright Japan Science and Technology Agency 1986</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c3767-20399de9436400443e2a35368d5f3ec59951a2a8d47f2afefe087d1e1c78b7e03</citedby><cites>FETCH-LOGICAL-c3767-20399de9436400443e2a35368d5f3ec59951a2a8d47f2afefe087d1e1c78b7e03</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,1877,4010,27900,27901,27902</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=8041680$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>KONDOH, Yukihiro</creatorcontrib><creatorcontrib>TAKANO, Satoshi</creatorcontrib><title>Determination of Carboxybetaine Amphoteric Surfactants in Household and Cosmetic Products by High Performance Liquid Chromatography with Prelabeling</title><title>Analytical Sciences</title><description>A high performance liquid chromatographic (HPLC) method is described for the determination of carboxybetaine amphoteric surfactants in commercial household and cosmetic products. The surfactants are prelabeled with 4-bromomethyl-7-methoxycoumarin and then are separated by reversed phase HPLC with a gradient elution. The determination of carboxybetaines in shampoos was carried out by an internal standard method. The calibration curve was linear in the range from 0.007 to 4.6nmol. The relative standard deviation was found to be 1.0% for 0.46nmol injection. By using the proposed method, carboxybetaines in commercial household and cosmetic products were determined with high sensitivity and high selectivity.</description><subject>4-bromomethyl-7-methoxycoumarin</subject><subject>Applied sciences</subject><subject>carboxybetaine amphoteric surfactants</subject><subject>Chemical industry and chemicals</subject><subject>Cosmetics, toiletries</subject><subject>Exact sciences and technology</subject><subject>High performance liquid chromatography</subject><subject>prelabeling</subject><subject>shampoo</subject><subject>Washing products. Cosmetics and toiletries. Perfumes</subject><issn>0910-6340</issn><issn>1348-2246</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1986</creationdate><recordtype>article</recordtype><recordid>eNo9kE2P0zAQQCMEEmXhyN0SXFP8lcQ5rspCkSrtSsA5mjjjxlVid21H0P_BD8ZVuz1YPszzs-YVxUdG15yx-gs4mKK2a76WdfOqWDEhVcm5rF8XK9oyWtZC0rfFuxgPlDKuOF8V_75iwjBbB8l6R7whGwi9_3vqMYF1SO7n4-gzYjX5uQQDOoFLkVhHtn6JOPppIOAGsvFxxpSpp-CHRWekP5Gt3Y_kCYPxYQankezs82IzPAY_Q_L7AMfxRP7YlLGAE_Q4Wbd_X7wxeRX8cL3vit_fHn5ttuXu8fuPzf2u1KKpm5JT0bYDtlLUklIpBXIQlajVUBmBumrbigEHNcjGcDBokKpmYMh0o_oGqbgrPl28x-CfF4ypO_glnCt2TEolJa25ylR5oXTwMQY03THYGcKpY7Q7h--u4Tve5fCZ_3y1QtQwmZA3t_H2SFHJanX-_OGCHWKCPd7mEHLFCV-krFVVFl9O1t_meoTQoRP_AVKioFs</recordid><startdate>1986</startdate><enddate>1986</enddate><creator>KONDOH, Yukihiro</creator><creator>TAKANO, Satoshi</creator><general>The Japan Society for Analytical Chemistry</general><general>Japan Society for Analytical Chemistry</general><general>Japan Science and Technology Agency</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7QF</scope><scope>7QO</scope><scope>7QQ</scope><scope>7SE</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>FR3</scope><scope>H8G</scope><scope>JG9</scope><scope>L7M</scope><scope>P64</scope></search><sort><creationdate>1986</creationdate><title>Determination of Carboxybetaine Amphoteric Surfactants in Household and Cosmetic Products by High Performance Liquid Chromatography with Prelabeling</title><author>KONDOH, Yukihiro ; TAKANO, Satoshi</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3767-20399de9436400443e2a35368d5f3ec59951a2a8d47f2afefe087d1e1c78b7e03</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1986</creationdate><topic>4-bromomethyl-7-methoxycoumarin</topic><topic>Applied sciences</topic><topic>carboxybetaine amphoteric surfactants</topic><topic>Chemical industry and chemicals</topic><topic>Cosmetics, toiletries</topic><topic>Exact sciences and technology</topic><topic>High performance liquid chromatography</topic><topic>prelabeling</topic><topic>shampoo</topic><topic>Washing products. Cosmetics and toiletries. Perfumes</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>KONDOH, Yukihiro</creatorcontrib><creatorcontrib>TAKANO, Satoshi</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Aluminium Industry Abstracts</collection><collection>Biotechnology Research Abstracts</collection><collection>Ceramic Abstracts</collection><collection>Corrosion Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Engineering Research Database</collection><collection>Copper Technical Reference Library</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Biotechnology and BioEngineering Abstracts</collection><jtitle>Analytical Sciences</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>KONDOH, Yukihiro</au><au>TAKANO, Satoshi</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Determination of Carboxybetaine Amphoteric Surfactants in Household and Cosmetic Products by High Performance Liquid Chromatography with Prelabeling</atitle><jtitle>Analytical Sciences</jtitle><date>1986</date><risdate>1986</risdate><volume>2</volume><issue>5</issue><spage>467</spage><epage>471</epage><pages>467-471</pages><issn>0910-6340</issn><eissn>1348-2246</eissn><coden>ANSCEN</coden><abstract>A high performance liquid chromatographic (HPLC) method is described for the determination of carboxybetaine amphoteric surfactants in commercial household and cosmetic products. The surfactants are prelabeled with 4-bromomethyl-7-methoxycoumarin and then are separated by reversed phase HPLC with a gradient elution. The determination of carboxybetaines in shampoos was carried out by an internal standard method. The calibration curve was linear in the range from 0.007 to 4.6nmol. The relative standard deviation was found to be 1.0% for 0.46nmol injection. By using the proposed method, carboxybetaines in commercial household and cosmetic products were determined with high sensitivity and high selectivity.</abstract><cop>Tokyo</cop><pub>The Japan Society for Analytical Chemistry</pub><doi>10.2116/analsci.2.467</doi><tpages>5</tpages><oa>free_for_read</oa></addata></record> |
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| identifier | ISSN: 0910-6340 |
| ispartof | Analytical Sciences, 1986/10/10, Vol.2(5), pp.467-471 |
| issn | 0910-6340 1348-2246 |
| language | eng |
| recordid | cdi_proquest_journals_1448440628 |
| source | J-STAGE (Japan Science & Technology Information Aggregator, Electronic) Freely Available Titles - Japanese; Open Access Titles of Japan; Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals; Free Full-Text Journals in Chemistry |
| subjects | 4-bromomethyl-7-methoxycoumarin Applied sciences carboxybetaine amphoteric surfactants Chemical industry and chemicals Cosmetics, toiletries Exact sciences and technology High performance liquid chromatography prelabeling shampoo Washing products. Cosmetics and toiletries. Perfumes |
| title | Determination of Carboxybetaine Amphoteric Surfactants in Household and Cosmetic Products by High Performance Liquid Chromatography with Prelabeling |
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