Crystal Structure of Bis[O,O′-di(p-tolyl)thiophosphoryl]disulfide, [(p-MeC6H4O)2PS2]2

Crystal Structure of Bis[O,O′-di(p-tolyl)thiophosphoryl]disulfide, [(p-MeC6H4O)2PS2]2

Bis[O,O′-di(p-tolyl)thiophosphoryl]disulfide crystallizes in the space group P21/c with a = 11.145(2)Å, b = 7.965(7)Å, c = 17.065(2)Å, β = 90.300(1)° and Z = 2. Both distorted tetrahedrally coordinated phosphorus atoms have two p-MeC6H4O groups, which are oriented in such a way that each is centro s...

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Veröffentlicht in:Analytical Sciences ; X-ray Structure and Analysis Online 2008, Vol.24, pp.x197-x198
Hauptverfasser: GURNANI, Chitra, MAHESHWARI, Seema, RATNANI, Raju, DRAKE, John. E.
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description Bis[O,O′-di(p-tolyl)thiophosphoryl]disulfide crystallizes in the space group P21/c with a = 11.145(2)Å, b = 7.965(7)Å, c = 17.065(2)Å, β = 90.300(1)° and Z = 2. Both distorted tetrahedrally coordinated phosphorus atoms have two p-MeC6H4O groups, which are oriented in such a way that each is centro symmetrically related to the mid point of the S-S bond, resulting in the equivalent p-MeC6H4O groups being co-planar and a P-S-S-P torsion angle of 179.02(4)°.
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title Crystal Structure of Bis[O,O′-di(p-tolyl)thiophosphoryl]disulfide, [(p-MeC6H4O)2PS2]2
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