Synthesis and Properties of Porous Organic Polymers from a Rigid Macrocyclic Building Block
Two rigid macrocyclic CTV-based porous organic polymers, Click-POP-1 and Click-POP-2, have been synthe- sized by Click reaction of a cyclotriveratrylene analogue with alkyne groups and aromatic azides in one pot. FTIR, solid 13C NMR and elemental analysis confirmed the formation of the polymers. Bot...
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| Veröffentlicht in: | Chinese journal of chemistry 2013-05, Vol.31 (5), p.577-581 |
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| container_title | Chinese journal of chemistry |
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| creator | Song, Jingru Huang, Zhitang Zheng, Qiyu |
| description | Two rigid macrocyclic CTV-based porous organic polymers, Click-POP-1 and Click-POP-2, have been synthe- sized by Click reaction of a cyclotriveratrylene analogue with alkyne groups and aromatic azides in one pot. FTIR, solid 13C NMR and elemental analysis confirmed the formation of the polymers. Both of them possess high thermo-stability which is up to 410 and 900 ℃, respectively, and moderate hydrogen storage properties with 0.46 wt% at 77 K. Their nitrogen uptake showed type-I isotherm with BET surface areas up to 342 and 317 m2·g ^-1. |
| doi_str_mv | 10.1002/cjoc.201300138 |
| format | Article |
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FTIR, solid 13C NMR and elemental analysis confirmed the formation of the polymers. Both of them possess high thermo-stability which is up to 410 and 900 ℃, respectively, and moderate hydrogen storage properties with 0.46 wt% at 77 K. Their nitrogen uptake showed type-I isotherm with BET surface areas up to 342 and 317 m2·g ^-1.</description><identifier>ISSN: 1001-604X</identifier><identifier>EISSN: 1614-7065</identifier><identifier>DOI: 10.1002/cjoc.201300138</identifier><language>eng</language><publisher>Weinheim: WILEY-VCH Verlag</publisher><subject>amorphous ; BET比表面积 ; click reaction ; cyclotriveratrylene ; hydrogen uptake ; porous organic polymer ; 储氢性能 ; 刚性 ; 叠氮化物 ; 合成 ; 多孔 ; 大厦 ; 有机聚合物</subject><ispartof>Chinese journal of chemistry, 2013-05, Vol.31 (5), p.577-581</ispartof><rights>Copyright © 2013 SIOC, CAS, Shanghai & WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim</rights><rights>Copyright © 2013 SIOC, CAS, Shanghai & WILEY-VCH Verlag GmbH & Co. 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FTIR, solid 13C NMR and elemental analysis confirmed the formation of the polymers. Both of them possess high thermo-stability which is up to 410 and 900 ℃, respectively, and moderate hydrogen storage properties with 0.46 wt% at 77 K. Their nitrogen uptake showed type-I isotherm with BET surface areas up to 342 and 317 m2·g ^-1.</description><subject>amorphous</subject><subject>BET比表面积</subject><subject>click reaction</subject><subject>cyclotriveratrylene</subject><subject>hydrogen uptake</subject><subject>porous organic polymer</subject><subject>储氢性能</subject><subject>刚性</subject><subject>叠氮化物</subject><subject>合成</subject><subject>多孔</subject><subject>大厦</subject><subject>有机聚合物</subject><issn>1001-604X</issn><issn>1614-7065</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><recordid>eNqFkEtPAjEURidGExHduq5xPdhO23ksBQU0KBMf0cRFUzotFIYptBCdf2_JEOLOxU1vm3Nub74guESwgyCMbsTciE4EEYa-0qOghWJEwgTG9Nj3_jGMIfk8Dc6cm3s-SaK4FXy91tVmJp12gFcFyK1ZSbvR0gGjQG6s2TowtlNeaeGvZb2U1gFlzRJw8KKnugBPXFgjalF6orvVZaGrKeiWRizOgxPFSycv9mc7eO_fv_WG4Wg8eOjdjkKBU5SGQiiScaTSQkUCZxOSciInRKVcQplmsEgTzglBSlKZTCjGBGVFPBERoVHMcYHbwXUzd2XNeivdhs3N1lb-S4YwxSSDlCae6jSUX9c5KxVbWb3ktmYIsl2AbBcgOwTohawRvnUp639o1nsc9_66YeNqt5E_B5fbBYsTnFD28Txg3WHez_EdYgPPX-2Xm5lquvYRHhwSZ4hCjPEvlyePcA</recordid><startdate>201305</startdate><enddate>201305</enddate><creator>Song, Jingru</creator><creator>Huang, Zhitang</creator><creator>Zheng, Qiyu</creator><general>WILEY-VCH Verlag</general><general>WILEY‐VCH Verlag</general><general>Wiley Subscription Services, Inc</general><scope>2RA</scope><scope>92L</scope><scope>CQIGP</scope><scope>~WA</scope><scope>BSCLL</scope><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>201305</creationdate><title>Synthesis and Properties of Porous Organic Polymers from a Rigid Macrocyclic Building Block</title><author>Song, Jingru ; Huang, Zhitang ; Zheng, Qiyu</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3818-ccf49a1f8df2c39b48a4eb4f8ae0e890d87aa441fe5e7b533419d6bc24526a3d3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>amorphous</topic><topic>BET比表面积</topic><topic>click reaction</topic><topic>cyclotriveratrylene</topic><topic>hydrogen uptake</topic><topic>porous organic polymer</topic><topic>储氢性能</topic><topic>刚性</topic><topic>叠氮化物</topic><topic>合成</topic><topic>多孔</topic><topic>大厦</topic><topic>有机聚合物</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Song, Jingru</creatorcontrib><creatorcontrib>Huang, Zhitang</creatorcontrib><creatorcontrib>Zheng, Qiyu</creatorcontrib><collection>中文科技期刊数据库</collection><collection>中文科技期刊数据库-CALIS站点</collection><collection>中文科技期刊数据库-7.0平台</collection><collection>中文科技期刊数据库- 镜像站点</collection><collection>Istex</collection><collection>CrossRef</collection><jtitle>Chinese journal of chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Song, Jingru</au><au>Huang, Zhitang</au><au>Zheng, Qiyu</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and Properties of Porous Organic Polymers from a Rigid Macrocyclic Building Block</atitle><jtitle>Chinese journal of chemistry</jtitle><addtitle>Chinese Journal of Chemistry</addtitle><date>2013-05</date><risdate>2013</risdate><volume>31</volume><issue>5</issue><spage>577</spage><epage>581</epage><pages>577-581</pages><issn>1001-604X</issn><eissn>1614-7065</eissn><abstract>Two rigid macrocyclic CTV-based porous organic polymers, Click-POP-1 and Click-POP-2, have been synthe- sized by Click reaction of a cyclotriveratrylene analogue with alkyne groups and aromatic azides in one pot. 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| ispartof | Chinese journal of chemistry, 2013-05, Vol.31 (5), p.577-581 |
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| language | eng |
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| source | Wiley Online Library Journals Frontfile Complete |
| subjects | amorphous BET比表面积 click reaction cyclotriveratrylene hydrogen uptake porous organic polymer 储氢性能 刚性 叠氮化物 合成 多孔 大厦 有机聚合物 |
| title | Synthesis and Properties of Porous Organic Polymers from a Rigid Macrocyclic Building Block |
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