Transmission Electron Microscopy of Annealed ZrO2+8 Mol% Sc2O3
The influence of heat treatment (800°C for 200 h) on the micro‐structure of 8 mol% Sc2O3‐ZrO2 was investigated by XRD and TEM. The starting material was initially characterized and found to contain predominantly cubic‐fluorite phase grains, with
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Veröffentlicht in: | Journal of the American Ceramic Society 1983-03, Vol.66 (3), p.213-216 |
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creator | MOGHADAM, FARHAD K. YAMASHITA, TOM SINCLAIR, ROBERT STEVENSON, DAVID A. |
description | The influence of heat treatment (800°C for 200 h) on the micro‐structure of 8 mol% Sc2O3‐ZrO2 was investigated by XRD and TEM. The starting material was initially characterized and found to contain predominantly cubic‐fluorite phase grains, with |
doi_str_mv | 10.1111/j.1151-2916.1983.tb10020.x |
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The starting material was initially characterized and found to contain predominantly cubic‐fluorite phase grains, with <5% of the grain containing the rhombohedral β phase. The β phase was positively identified by the analysis of electron diffraction pattern and by quantitative energy dispersive X‐ray analysis. On aging, the relative amount of β phase was found to increase to about 15 to 20% by XRD measurement; this was confirmed by TEM observation. The orientation relation between the different variants of the β phase within a grain was determined to be (100)r||(010)r, and the geometrical arrangement of these variants within the grain was deduced using a 21/2D imaging electron microscopy technique.</description><identifier>ISSN: 0002-7820</identifier><identifier>EISSN: 1551-2916</identifier><identifier>DOI: 10.1111/j.1151-2916.1983.tb10020.x</identifier><language>eng</language><publisher>Oxford, UK: Blackwell Publishing Ltd</publisher><ispartof>Journal of the American Ceramic Society, 1983-03, Vol.66 (3), p.213-216</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1111%2Fj.1151-2916.1983.tb10020.x$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1111%2Fj.1151-2916.1983.tb10020.x$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,780,784,1416,27868,27923,27924,45573,45574</link.rule.ids></links><search><creatorcontrib>MOGHADAM, FARHAD K.</creatorcontrib><creatorcontrib>YAMASHITA, TOM</creatorcontrib><creatorcontrib>SINCLAIR, ROBERT</creatorcontrib><creatorcontrib>STEVENSON, DAVID A.</creatorcontrib><title>Transmission Electron Microscopy of Annealed ZrO2+8 Mol% Sc2O3</title><title>Journal of the American Ceramic Society</title><description>The influence of heat treatment (800°C for 200 h) on the micro‐structure of 8 mol% Sc2O3‐ZrO2 was investigated by XRD and TEM. 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The starting material was initially characterized and found to contain predominantly cubic‐fluorite phase grains, with <5% of the grain containing the rhombohedral β phase. The β phase was positively identified by the analysis of electron diffraction pattern and by quantitative energy dispersive X‐ray analysis. On aging, the relative amount of β phase was found to increase to about 15 to 20% by XRD measurement; this was confirmed by TEM observation. The orientation relation between the different variants of the β phase within a grain was determined to be (100)r||(010)r, and the geometrical arrangement of these variants within the grain was deduced using a 21/2D imaging electron microscopy technique.</abstract><cop>Oxford, UK</cop><pub>Blackwell Publishing Ltd</pub><doi>10.1111/j.1151-2916.1983.tb10020.x</doi><tpages>4</tpages></addata></record> |
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title | Transmission Electron Microscopy of Annealed ZrO2+8 Mol% Sc2O3 |
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