Synthesis and Characterization of Glucosamide Surfactant
The synthesis and structural analysis of glucosamide surfactants of the general formula C n H 2n+1 NH(CH 2 ) 2 NHCO(CHOH) 4 CH 2 OH ( n = 8, 10, 12) are described, and the surface activity properties of the surfactants are studied. N -alkylethylenediamines were synthesized by the alkylation of the...
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| Veröffentlicht in: | Journal of surfactants and detergents 2013-03, Vol.16 (2), p.155-159 |
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| creator | Han, Fu Deng, Yun-yun Wang, Peng-li Song, Jia Zhou, Ya-wen Xu, Bao-cai |
| description | The synthesis and structural analysis of glucosamide surfactants of the general formula C
n
H
2n+1
NH(CH
2
)
2
NHCO(CHOH)
4
CH
2
OH (
n
= 8, 10, 12) are described, and the surface activity properties of the surfactants are studied.
N
-alkylethylenediamines were synthesized by the alkylation of the ethylenediamine with alkyl bromide. The glucosamide surfactants,
N
-alkyl-
N
′-glucosylethylenediamine (C
n
GA), were prepared by amidation of the precursor diamine with
d
-gluconic acid δ-lactone. They were structurally characterized by IR,
1
H NMR and MS. They reduced the surface tension of water to approximately 26–27 mN m
−1
at concentration levels of (0.5–1.6) × 10
−3
mol L
−1
. |
| doi_str_mv | 10.1007/s11743-012-1392-6 |
| format | Article |
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n
H
2n+1
NH(CH
2
)
2
NHCO(CHOH)
4
CH
2
OH (
n
= 8, 10, 12) are described, and the surface activity properties of the surfactants are studied.
N
-alkylethylenediamines were synthesized by the alkylation of the ethylenediamine with alkyl bromide. The glucosamide surfactants,
N
-alkyl-
N
′-glucosylethylenediamine (C
n
GA), were prepared by amidation of the precursor diamine with
d
-gluconic acid δ-lactone. They were structurally characterized by IR,
1
H NMR and MS. They reduced the surface tension of water to approximately 26–27 mN m
−1
at concentration levels of (0.5–1.6) × 10
−3
mol L
−1
.</description><identifier>ISSN: 1097-3958</identifier><identifier>EISSN: 1558-9293</identifier><identifier>DOI: 10.1007/s11743-012-1392-6</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer-Verlag</publisher><subject>Alkylation ; Amidation ; Aquatic Pollution ; Characterization ; Chemical synthesis ; Chemistry ; Chemistry and Materials Science ; Glucosamide ; Industrial Chemistry/Chemical Engineering ; Original Article ; Physical Chemistry ; Polymer Sciences ; Structural analysis ; Surface chemistry ; Surface tension ; Surfaces and Interfaces ; Surfactants ; Synthesis ; Thin Films ; Waste Water Technology ; Water Management ; Water Pollution Control</subject><ispartof>Journal of surfactants and detergents, 2013-03, Vol.16 (2), p.155-159</ispartof><rights>AOCS 2012</rights><rights>2013 American Oil Chemists' Society (AOCS)</rights><rights>AOCS 2013</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c4345-c82de6c53e7d62eda28ece20acdc1654ecd45552b58449766b6d9232839caad83</citedby><cites>FETCH-LOGICAL-c4345-c82de6c53e7d62eda28ece20acdc1654ecd45552b58449766b6d9232839caad83</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1007%2Fs11743-012-1392-6$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1007%2Fs11743-012-1392-6$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,776,780,1411,27903,27904,45553,45554</link.rule.ids></links><search><creatorcontrib>Han, Fu</creatorcontrib><creatorcontrib>Deng, Yun-yun</creatorcontrib><creatorcontrib>Wang, Peng-li</creatorcontrib><creatorcontrib>Song, Jia</creatorcontrib><creatorcontrib>Zhou, Ya-wen</creatorcontrib><creatorcontrib>Xu, Bao-cai</creatorcontrib><title>Synthesis and Characterization of Glucosamide Surfactant</title><title>Journal of surfactants and detergents</title><addtitle>J Surfact Deterg</addtitle><description>The synthesis and structural analysis of glucosamide surfactants of the general formula C
n
H
2n+1
NH(CH
2
)
2
NHCO(CHOH)
4
CH
2
OH (
n
= 8, 10, 12) are described, and the surface activity properties of the surfactants are studied.
N
-alkylethylenediamines were synthesized by the alkylation of the ethylenediamine with alkyl bromide. The glucosamide surfactants,
N
-alkyl-
N
′-glucosylethylenediamine (C
n
GA), were prepared by amidation of the precursor diamine with
d
-gluconic acid δ-lactone. They were structurally characterized by IR,
1
H NMR and MS. They reduced the surface tension of water to approximately 26–27 mN m
−1
at concentration levels of (0.5–1.6) × 10
−3
mol L
−1
.</description><subject>Alkylation</subject><subject>Amidation</subject><subject>Aquatic Pollution</subject><subject>Characterization</subject><subject>Chemical synthesis</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Glucosamide</subject><subject>Industrial Chemistry/Chemical Engineering</subject><subject>Original Article</subject><subject>Physical Chemistry</subject><subject>Polymer Sciences</subject><subject>Structural analysis</subject><subject>Surface chemistry</subject><subject>Surface tension</subject><subject>Surfaces and Interfaces</subject><subject>Surfactants</subject><subject>Synthesis</subject><subject>Thin Films</subject><subject>Waste Water Technology</subject><subject>Water Management</subject><subject>Water Pollution Control</subject><issn>1097-3958</issn><issn>1558-9293</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><recordid>eNqFkEtLAzEQgIMoWKs_wNuC52gem9dRaq1KwUP1HNJk1m5pd2uyi9Rf35T14EVkDjMw880MH0LXlNxSQtRdolSVHBPKMOWGYXmCRlQIjQ0z_DTXxCjMjdDn6CKlNSGMlkKMkF7sm24FqU6Fa0IxWbnofAex_nZd3TZFWxWzTe_b5LZ1gGLRxyr3XdNdorPKbRJc_eQxen-cvk2e8Px19jy5n2Nf8lJgr1kA6QUHFSSD4JgGD4w4HzyVogQf8h-CLYUuS6OkXMpgGGeaG-9c0HyMboa9u9h-9pA6u2772OSTljKtchB6nKLDlI9tShEqu4v11sW9pcQeBdlBkM2C7FGQlZlRA_NVb2D_P2BfFg9TkqVmkg1kylDzAfHXT3-eOwC_QnhY</recordid><startdate>201303</startdate><enddate>201303</enddate><creator>Han, Fu</creator><creator>Deng, Yun-yun</creator><creator>Wang, Peng-li</creator><creator>Song, Jia</creator><creator>Zhou, Ya-wen</creator><creator>Xu, Bao-cai</creator><general>Springer-Verlag</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>4T-</scope><scope>7QH</scope><scope>7UA</scope><scope>7XB</scope><scope>88I</scope><scope>8AO</scope><scope>8FE</scope><scope>8FG</scope><scope>8FK</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AEUYN</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>BHPHI</scope><scope>BKSAR</scope><scope>C1K</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>F1W</scope><scope>GNUQQ</scope><scope>H97</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>L.G</scope><scope>M2P</scope><scope>PCBAR</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>Q9U</scope></search><sort><creationdate>201303</creationdate><title>Synthesis and Characterization of Glucosamide Surfactant</title><author>Han, Fu ; Deng, Yun-yun ; Wang, Peng-li ; Song, Jia ; Zhou, Ya-wen ; Xu, Bao-cai</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4345-c82de6c53e7d62eda28ece20acdc1654ecd45552b58449766b6d9232839caad83</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>Alkylation</topic><topic>Amidation</topic><topic>Aquatic Pollution</topic><topic>Characterization</topic><topic>Chemical synthesis</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Glucosamide</topic><topic>Industrial Chemistry/Chemical Engineering</topic><topic>Original Article</topic><topic>Physical Chemistry</topic><topic>Polymer Sciences</topic><topic>Structural analysis</topic><topic>Surface chemistry</topic><topic>Surface tension</topic><topic>Surfaces and Interfaces</topic><topic>Surfactants</topic><topic>Synthesis</topic><topic>Thin Films</topic><topic>Waste Water Technology</topic><topic>Water Management</topic><topic>Water Pollution Control</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Han, Fu</creatorcontrib><creatorcontrib>Deng, Yun-yun</creatorcontrib><creatorcontrib>Wang, Peng-li</creatorcontrib><creatorcontrib>Song, Jia</creatorcontrib><creatorcontrib>Zhou, Ya-wen</creatorcontrib><creatorcontrib>Xu, Bao-cai</creatorcontrib><collection>CrossRef</collection><collection>ProQuest Central (Corporate)</collection><collection>Docstoc</collection><collection>Aqualine</collection><collection>Water Resources Abstracts</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>Science Database (Alumni Edition)</collection><collection>ProQuest Pharma Collection</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest One Sustainability</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>Natural Science Collection</collection><collection>Earth, Atmospheric & Aquatic Science Collection</collection><collection>Environmental Sciences and Pollution Management</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>ASFA: Aquatic Sciences and Fisheries Abstracts</collection><collection>ProQuest Central Student</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) 3: Aquatic Pollution & Environmental Quality</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) Professional</collection><collection>Science Database</collection><collection>Earth, Atmospheric & Aquatic Science Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central Basic</collection><jtitle>Journal of surfactants and detergents</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Han, Fu</au><au>Deng, Yun-yun</au><au>Wang, Peng-li</au><au>Song, Jia</au><au>Zhou, Ya-wen</au><au>Xu, Bao-cai</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and Characterization of Glucosamide Surfactant</atitle><jtitle>Journal of surfactants and detergents</jtitle><stitle>J Surfact Deterg</stitle><date>2013-03</date><risdate>2013</risdate><volume>16</volume><issue>2</issue><spage>155</spage><epage>159</epage><pages>155-159</pages><issn>1097-3958</issn><eissn>1558-9293</eissn><abstract>The synthesis and structural analysis of glucosamide surfactants of the general formula C
n
H
2n+1
NH(CH
2
)
2
NHCO(CHOH)
4
CH
2
OH (
n
= 8, 10, 12) are described, and the surface activity properties of the surfactants are studied.
N
-alkylethylenediamines were synthesized by the alkylation of the ethylenediamine with alkyl bromide. The glucosamide surfactants,
N
-alkyl-
N
′-glucosylethylenediamine (C
n
GA), were prepared by amidation of the precursor diamine with
d
-gluconic acid δ-lactone. They were structurally characterized by IR,
1
H NMR and MS. They reduced the surface tension of water to approximately 26–27 mN m
−1
at concentration levels of (0.5–1.6) × 10
−3
mol L
−1
.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer-Verlag</pub><doi>10.1007/s11743-012-1392-6</doi><tpages>5</tpages></addata></record> |
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| ispartof | Journal of surfactants and detergents, 2013-03, Vol.16 (2), p.155-159 |
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| language | eng |
| recordid | cdi_proquest_journals_1287878018 |
| source | Wiley Online Library Journals Frontfile Complete |
| subjects | Alkylation Amidation Aquatic Pollution Characterization Chemical synthesis Chemistry Chemistry and Materials Science Glucosamide Industrial Chemistry/Chemical Engineering Original Article Physical Chemistry Polymer Sciences Structural analysis Surface chemistry Surface tension Surfaces and Interfaces Surfactants Synthesis Thin Films Waste Water Technology Water Management Water Pollution Control |
| title | Synthesis and Characterization of Glucosamide Surfactant |
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