Preparation and characterization of antibacterial Zn2+-exchanged montmorillonites

Zn-montmorillonites(Zn-MMTs) as antibacterial compounds were prepared by an ion-exchange reaction. The reaction time, initial pH value and molar ratios of CEC influencing zinc content in Zn-MMTs were investigated, and Zn-MMTs were characterized by means of EDX, XRD, XPS, and SEM. The results of bact...

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Veröffentlicht in:Journal of Wuhan University of Technology. Materials science edition 2010-10, Vol.25 (5), p.725-729
Hauptverfasser: Shi, Qingshan, Tan, Shaozao, Yang, Qiuhui, Jiao, Zepeng, Ouyang, Yousheng, Chen, Yiben
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container_title Journal of Wuhan University of Technology. Materials science edition
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creator Shi, Qingshan
Tan, Shaozao
Yang, Qiuhui
Jiao, Zepeng
Ouyang, Yousheng
Chen, Yiben
description Zn-montmorillonites(Zn-MMTs) as antibacterial compounds were prepared by an ion-exchange reaction. The reaction time, initial pH value and molar ratios of CEC influencing zinc content in Zn-MMTs were investigated, and Zn-MMTs were characterized by means of EDX, XRD, XPS, and SEM. The results of bacterial growth tests were confirmed by determination of the minimum inhibition concentrations (MICs) and minimum bactericidal concentrations (MBCs). The experimental results show that the zinc is confirmed as bivalent zinc state, the d 001 basal spacing of Zn-MMTs is enlarged with the enhancement of the zinc content, and the particles of Zn-MMTs are formed with irregular shape. Moreover, the antibacterial activity of Zn-MMTs increases with increasing the zinc content, and Zn-MMT-3 containing 6.76 mass% of zinc exhibits optimum antibacterial activity against Escherichia coli and Staphylococcus aureus . The intercalated zinc ions act as very effective antibacterial substances in the long term.
doi_str_mv 10.1007/s11595-010-0080-5
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Materials Science
Studies
title Preparation and characterization of antibacterial Zn2+-exchanged montmorillonites
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