Rapid synthesis and size control of CuInS2 semi-conductor nanoparticles using microwave irradiation
The properties of CuInS 2 semi-conductor nanoparticles make them attractive materials for use in next-generation photovoltaics. We have prepared CuInS 2 nanoparticles from single source precursors via microwave irradiation. Microwave irradiation methods have allowed us to increase the efficiency of...
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| Veröffentlicht in: | Journal of Nanoparticle Research, 10(4):633-641 10(4):633-641, 2008-04, Vol.10 (4), p.633-641 |
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| container_title | Journal of Nanoparticle Research, 10(4):633-641 |
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| creator | Gardner, Joseph S. Shurdha, Endrit Wang, Chongmin Lau, Lisa D. Rodriguez, René G. Pak, Joshua J. |
| description | The properties of CuInS
2
semi-conductor nanoparticles make them attractive materials for use in next-generation photovoltaics. We have prepared CuInS
2
nanoparticles from single source precursors via microwave irradiation. Microwave irradiation methods have allowed us to increase the efficiency of preparation of these materials by providing uniform heating and rapid reaction times. The synergistic effect of varying thiol capping ligand concentrations as well as reaction temperatures and times resulted in fine control of nanoparticle growth in the 3–5 nm size range. Investigation of the photophysical properties of the colloidal nanoparticles were performed using electronic absorption and luminescence emission spectroscopy. Qualitative nanoparticles sizes were determined from the photoluminescence (PLE) data and compared to HRTEM images. |
| doi_str_mv | 10.1007/s11051-007-9294-7 |
| format | Article |
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2
semi-conductor nanoparticles make them attractive materials for use in next-generation photovoltaics. We have prepared CuInS
2
nanoparticles from single source precursors via microwave irradiation. Microwave irradiation methods have allowed us to increase the efficiency of preparation of these materials by providing uniform heating and rapid reaction times. The synergistic effect of varying thiol capping ligand concentrations as well as reaction temperatures and times resulted in fine control of nanoparticle growth in the 3–5 nm size range. Investigation of the photophysical properties of the colloidal nanoparticles were performed using electronic absorption and luminescence emission spectroscopy. Qualitative nanoparticles sizes were determined from the photoluminescence (PLE) data and compared to HRTEM images.</description><identifier>ISSN: 1388-0764</identifier><identifier>EISSN: 1572-896X</identifier><identifier>DOI: 10.1007/s11051-007-9294-7</identifier><language>eng</language><publisher>Dordrecht: Springer Netherlands</publisher><subject>Characterization and Evaluation of Materials ; Chemistry and Materials Science ; CuInS2 ; Emission spectroscopy ; Environmental Molecular Sciences Laboratory ; Inorganic Chemistry ; Irradiation ; Keywords: Microwave Irradiation ; Lasers ; Materials Science ; Nanoparticles ; Nanotechnology ; Optical Devices ; Optics ; Photonics ; Photovoltaics ; Physical Chemistry ; Research Paper ; Size-control ; Studies ; Synergistic effect ; Ternary Nanoparticle, Semi</subject><ispartof>Journal of Nanoparticle Research, 10(4):633-641, 2008-04, Vol.10 (4), p.633-641</ispartof><rights>Springer Science+Business Media B.V. 2007</rights><rights>Springer Science+Business Media B.V. 2008</rights><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c408t-238c8f73a486d540e703e5fefaa0ca45ac014d4d452606d50cd54a37f3cc06a3</citedby><cites>FETCH-LOGICAL-c408t-238c8f73a486d540e703e5fefaa0ca45ac014d4d452606d50cd54a37f3cc06a3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11051-007-9294-7$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11051-007-9294-7$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,885,27923,27924,41487,42556,51318</link.rule.ids><backlink>$$Uhttps://www.osti.gov/biblio/927703$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Gardner, Joseph S.</creatorcontrib><creatorcontrib>Shurdha, Endrit</creatorcontrib><creatorcontrib>Wang, Chongmin</creatorcontrib><creatorcontrib>Lau, Lisa D.</creatorcontrib><creatorcontrib>Rodriguez, René G.</creatorcontrib><creatorcontrib>Pak, Joshua J.</creatorcontrib><creatorcontrib>Pacific Northwest National Laboratory (PNNL), Richland, WA (US), Environmental Molecular Sciences Laboratory (EMSL)</creatorcontrib><title>Rapid synthesis and size control of CuInS2 semi-conductor nanoparticles using microwave irradiation</title><title>Journal of Nanoparticle Research, 10(4):633-641</title><addtitle>J Nanopart Res</addtitle><description>The properties of CuInS
2
semi-conductor nanoparticles make them attractive materials for use in next-generation photovoltaics. We have prepared CuInS
2
nanoparticles from single source precursors via microwave irradiation. Microwave irradiation methods have allowed us to increase the efficiency of preparation of these materials by providing uniform heating and rapid reaction times. The synergistic effect of varying thiol capping ligand concentrations as well as reaction temperatures and times resulted in fine control of nanoparticle growth in the 3–5 nm size range. Investigation of the photophysical properties of the colloidal nanoparticles were performed using electronic absorption and luminescence emission spectroscopy. Qualitative nanoparticles sizes were determined from the photoluminescence (PLE) data and compared to HRTEM images.</description><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>CuInS2</subject><subject>Emission spectroscopy</subject><subject>Environmental Molecular Sciences Laboratory</subject><subject>Inorganic Chemistry</subject><subject>Irradiation</subject><subject>Keywords: Microwave Irradiation</subject><subject>Lasers</subject><subject>Materials Science</subject><subject>Nanoparticles</subject><subject>Nanotechnology</subject><subject>Optical Devices</subject><subject>Optics</subject><subject>Photonics</subject><subject>Photovoltaics</subject><subject>Physical Chemistry</subject><subject>Research Paper</subject><subject>Size-control</subject><subject>Studies</subject><subject>Synergistic effect</subject><subject>Ternary Nanoparticle, Semi</subject><issn>1388-0764</issn><issn>1572-896X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2008</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><recordid>eNp1kEtPAyEUhYnRxPr4Ae4wrtELMwzM0jQ-mjQx0S7cEcIwLU0LFRhN_fXSjAs3hgXnku-cXA5CVxRuKYC4S5QCp6RI0rK2JuIITSgXjMi2eT8uupKSgGjqU3SW0hqANqxlE2Re9c51OO19XtnkEta-TO7bYhN8jmGDQ4-nw8y_MZzs1pHy3A0mh4i99mGnY3ZmYxMekvNLvHUmhi_9abGLUXdOZxf8BTrp9SbZy9_7HC0eHxbTZzJ_eZpN7-fE1CAzYZU0sheVrmXT8RqsgMry3vZag9E11wZo3ZXDWQOFAFMoXYm-MgYaXZ2j6zE2pOxUMi5bsyrremuyapkocYW5GZldDB-DTVmtwxB92UpRSpmkEjgvFB2p8pmUou3VLrqtjntFQR3qVmPd6iAPdStRPGz0pML6pY1_kv81_QDEqIOT</recordid><startdate>20080401</startdate><enddate>20080401</enddate><creator>Gardner, Joseph S.</creator><creator>Shurdha, Endrit</creator><creator>Wang, Chongmin</creator><creator>Lau, Lisa 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Nanoparticle Research, 10(4):633-641</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Gardner, Joseph S.</au><au>Shurdha, Endrit</au><au>Wang, Chongmin</au><au>Lau, Lisa D.</au><au>Rodriguez, René G.</au><au>Pak, Joshua J.</au><aucorp>Pacific Northwest National Laboratory (PNNL), Richland, WA (US), Environmental Molecular Sciences Laboratory (EMSL)</aucorp><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Rapid synthesis and size control of CuInS2 semi-conductor nanoparticles using microwave irradiation</atitle><jtitle>Journal of Nanoparticle Research, 10(4):633-641</jtitle><stitle>J Nanopart Res</stitle><date>2008-04-01</date><risdate>2008</risdate><volume>10</volume><issue>4</issue><spage>633</spage><epage>641</epage><pages>633-641</pages><issn>1388-0764</issn><eissn>1572-896X</eissn><abstract>The properties of CuInS
2
semi-conductor nanoparticles make them attractive materials for use in next-generation photovoltaics. We have prepared CuInS
2
nanoparticles from single source precursors via microwave irradiation. Microwave irradiation methods have allowed us to increase the efficiency of preparation of these materials by providing uniform heating and rapid reaction times. The synergistic effect of varying thiol capping ligand concentrations as well as reaction temperatures and times resulted in fine control of nanoparticle growth in the 3–5 nm size range. Investigation of the photophysical properties of the colloidal nanoparticles were performed using electronic absorption and luminescence emission spectroscopy. Qualitative nanoparticles sizes were determined from the photoluminescence (PLE) data and compared to HRTEM images.</abstract><cop>Dordrecht</cop><pub>Springer Netherlands</pub><doi>10.1007/s11051-007-9294-7</doi><tpages>9</tpages></addata></record> |
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| subjects | Characterization and Evaluation of Materials Chemistry and Materials Science CuInS2 Emission spectroscopy Environmental Molecular Sciences Laboratory Inorganic Chemistry Irradiation Keywords: Microwave Irradiation Lasers Materials Science Nanoparticles Nanotechnology Optical Devices Optics Photonics Photovoltaics Physical Chemistry Research Paper Size-control Studies Synergistic effect Ternary Nanoparticle, Semi |
| title | Rapid synthesis and size control of CuInS2 semi-conductor nanoparticles using microwave irradiation |
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