Effect of epoxy value on the rheological properties and microcosmic mechanism of WER emulsified asphalt
Waterborne epoxy resin (WER), a cleaning material with exceptional high-temperature resistance, has attracted much attention to modify emulsified asphalt in the pavement material field. Epoxy value is the critical characteristic index of WER. In this research, three WER with the epoxy values of 0.20...
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| description | Waterborne epoxy resin (WER), a cleaning material with exceptional high-temperature resistance, has attracted much attention to modify emulsified asphalt in the pavement material field. Epoxy value is the critical characteristic index of WER. In this research, three WER with the epoxy values of 0.20 eq/100g, 0.44 eq/100g, and 0.51 eq/100g were utilized as asphalt modifiers. The influence of epoxy value on WER-EA was investigated by comparing the rheological properties of three kinds of WER emulsified asphalt (WER-EA). The modification mechanism of WER-EA has been analyzed using FTIR and SEM. The results demonstrate that different WER-EA resulted in significantly different rheological properties. WER-EA with the epoxy value of 0.20 eq/100g (E20) performed best at high temperatures, with a maximum increase of 17477% in G*/sinδ compared to the neat asphalt and a maximum increase of 66.3% in G*/sinδ compared to the other two WER-EA. WER-EA with 0.44 eq/100g epoxy value (E44) performed best at low temperatures, with a maximum increase in m value of 39.4% and a maximum decrease in S value of 33.3% compared to the other two WER-EA. In addition, the interpenetrating polymer network (IPN) in E20 was observed to be more solid and stable, and IPN in E44 was more uniform. To summarize, lower epoxy value led to a higher degree of WER reaction and higher content of rigid groups, which is more conducive to optimizing the high-temperature property of WER-EA. WER with moderate epoxy value resulted in a low content of polar bonds and thus high content of flexible segments, which helps emulsified asphalt to form a more uniform IPN. |
| doi_str_mv | 10.1371/journal.pone.0296202 |
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Epoxy value is the critical characteristic index of WER. In this research, three WER with the epoxy values of 0.20 eq/100g, 0.44 eq/100g, and 0.51 eq/100g were utilized as asphalt modifiers. The influence of epoxy value on WER-EA was investigated by comparing the rheological properties of three kinds of WER emulsified asphalt (WER-EA). The modification mechanism of WER-EA has been analyzed using FTIR and SEM. The results demonstrate that different WER-EA resulted in significantly different rheological properties. WER-EA with the epoxy value of 0.20 eq/100g (E20) performed best at high temperatures, with a maximum increase of 17477% in G*/sinδ compared to the neat asphalt and a maximum increase of 66.3% in G*/sinδ compared to the other two WER-EA. WER-EA with 0.44 eq/100g epoxy value (E44) performed best at low temperatures, with a maximum increase in m value of 39.4% and a maximum decrease in S value of 33.3% compared to the other two WER-EA. In addition, the interpenetrating polymer network (IPN) in E20 was observed to be more solid and stable, and IPN in E44 was more uniform. To summarize, lower epoxy value led to a higher degree of WER reaction and higher content of rigid groups, which is more conducive to optimizing the high-temperature property of WER-EA. WER with moderate epoxy value resulted in a low content of polar bonds and thus high content of flexible segments, which helps emulsified asphalt to form a more uniform IPN.</description><identifier>ISSN: 1932-6203</identifier><identifier>EISSN: 1932-6203</identifier><identifier>DOI: 10.1371/journal.pone.0296202</identifier><identifier>PMID: 38277357</identifier><language>eng</language><publisher>United States: Public Library of Science</publisher><subject>Addition polymerization ; Analysis ; Asphalt ; Asphalt cement ; Asphalt pavements ; Cold Temperature ; Composition ; Curing ; Ductility ; Epoxy Resins ; Fourier transforms ; Heat resistance ; High temperature ; Hydrocarbons ; Interpenetrating networks ; Low temperature ; Materials ; Molecular weight ; Pavement materials ; Performance evaluation ; Physical properties ; Polymers ; Properties ; Rheological properties ; Rheology ; Scanning electron microscopy ; Temperature ; Test methods ; Viscosity</subject><ispartof>PloS one, 2024-01, Vol.19 (1), p.e0296202-e0296202</ispartof><rights>Copyright: © 2024 Huang et al. This is an open access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited.</rights><rights>COPYRIGHT 2024 Public Library of Science</rights><rights>2024 Huang et al. This is an open access article distributed under the terms of the Creative Commons Attribution License: http://creativecommons.org/licenses/by/4.0/ (the “License”), which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited. Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><rights>2024 Huang et al. This is an open access article distributed under the terms of the Creative Commons Attribution License: http://creativecommons.org/licenses/by/4.0/ (the “License”), which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited. Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c586t-3952f1a9b09959cb58e86d6e819e7778b6ec122f82547bf1ce6b11907df772ca3</cites><orcidid>0009-0001-7199-786X</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://journals.plos.org/plosone/article/file?id=10.1371/journal.pone.0296202&type=printable$$EPDF$$P50$$Gplos$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://journals.plos.org/plosone/article?id=10.1371/journal.pone.0296202$$EHTML$$P50$$Gplos$$Hfree_for_read</linktohtml><link.rule.ids>314,776,780,860,2096,2915,23845,27901,27902,79342,79343</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/38277357$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Huang, Dongqing</creatorcontrib><creatorcontrib>Shi, Junyi</creatorcontrib><creatorcontrib>Ouyang, Zongyan</creatorcontrib><title>Effect of epoxy value on the rheological properties and microcosmic mechanism of WER emulsified asphalt</title><title>PloS one</title><addtitle>PLoS One</addtitle><description>Waterborne epoxy resin (WER), a cleaning material with exceptional high-temperature resistance, has attracted much attention to modify emulsified asphalt in the pavement material field. Epoxy value is the critical characteristic index of WER. In this research, three WER with the epoxy values of 0.20 eq/100g, 0.44 eq/100g, and 0.51 eq/100g were utilized as asphalt modifiers. The influence of epoxy value on WER-EA was investigated by comparing the rheological properties of three kinds of WER emulsified asphalt (WER-EA). The modification mechanism of WER-EA has been analyzed using FTIR and SEM. The results demonstrate that different WER-EA resulted in significantly different rheological properties. WER-EA with the epoxy value of 0.20 eq/100g (E20) performed best at high temperatures, with a maximum increase of 17477% in G*/sinδ compared to the neat asphalt and a maximum increase of 66.3% in G*/sinδ compared to the other two WER-EA. WER-EA with 0.44 eq/100g epoxy value (E44) performed best at low temperatures, with a maximum increase in m value of 39.4% and a maximum decrease in S value of 33.3% compared to the other two WER-EA. In addition, the interpenetrating polymer network (IPN) in E20 was observed to be more solid and stable, and IPN in E44 was more uniform. To summarize, lower epoxy value led to a higher degree of WER reaction and higher content of rigid groups, which is more conducive to optimizing the high-temperature property of WER-EA. WER with moderate epoxy value resulted in a low content of polar bonds and thus high content of flexible segments, which helps emulsified asphalt to form a more uniform IPN.</description><subject>Addition polymerization</subject><subject>Analysis</subject><subject>Asphalt</subject><subject>Asphalt cement</subject><subject>Asphalt pavements</subject><subject>Cold Temperature</subject><subject>Composition</subject><subject>Curing</subject><subject>Ductility</subject><subject>Epoxy Resins</subject><subject>Fourier transforms</subject><subject>Heat resistance</subject><subject>High temperature</subject><subject>Hydrocarbons</subject><subject>Interpenetrating networks</subject><subject>Low temperature</subject><subject>Materials</subject><subject>Molecular weight</subject><subject>Pavement materials</subject><subject>Performance evaluation</subject><subject>Physical properties</subject><subject>Polymers</subject><subject>Properties</subject><subject>Rheological properties</subject><subject>Rheology</subject><subject>Scanning electron microscopy</subject><subject>Temperature</subject><subject>Test 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Academic</collection><collection>DOAJ Directory of Open Access Journals</collection><jtitle>PloS one</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Huang, Dongqing</au><au>Shi, Junyi</au><au>Ouyang, Zongyan</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Effect of epoxy value on the rheological properties and microcosmic mechanism of WER emulsified asphalt</atitle><jtitle>PloS one</jtitle><addtitle>PLoS One</addtitle><date>2024-01-26</date><risdate>2024</risdate><volume>19</volume><issue>1</issue><spage>e0296202</spage><epage>e0296202</epage><pages>e0296202-e0296202</pages><issn>1932-6203</issn><eissn>1932-6203</eissn><abstract>Waterborne epoxy resin (WER), a cleaning material with exceptional high-temperature resistance, has attracted much attention to modify emulsified asphalt in the pavement material field. Epoxy value is the critical characteristic index of WER. In this research, three WER with the epoxy values of 0.20 eq/100g, 0.44 eq/100g, and 0.51 eq/100g were utilized as asphalt modifiers. The influence of epoxy value on WER-EA was investigated by comparing the rheological properties of three kinds of WER emulsified asphalt (WER-EA). The modification mechanism of WER-EA has been analyzed using FTIR and SEM. The results demonstrate that different WER-EA resulted in significantly different rheological properties. WER-EA with the epoxy value of 0.20 eq/100g (E20) performed best at high temperatures, with a maximum increase of 17477% in G*/sinδ compared to the neat asphalt and a maximum increase of 66.3% in G*/sinδ compared to the other two WER-EA. WER-EA with 0.44 eq/100g epoxy value (E44) performed best at low temperatures, with a maximum increase in m value of 39.4% and a maximum decrease in S value of 33.3% compared to the other two WER-EA. In addition, the interpenetrating polymer network (IPN) in E20 was observed to be more solid and stable, and IPN in E44 was more uniform. To summarize, lower epoxy value led to a higher degree of WER reaction and higher content of rigid groups, which is more conducive to optimizing the high-temperature property of WER-EA. WER with moderate epoxy value resulted in a low content of polar bonds and thus high content of flexible segments, which helps emulsified asphalt to form a more uniform IPN.</abstract><cop>United States</cop><pub>Public Library of Science</pub><pmid>38277357</pmid><doi>10.1371/journal.pone.0296202</doi><tpages>e0296202</tpages><orcidid>https://orcid.org/0009-0001-7199-786X</orcidid><oa>free_for_read</oa></addata></record> |
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| subjects | Addition polymerization Analysis Asphalt Asphalt cement Asphalt pavements Cold Temperature Composition Curing Ductility Epoxy Resins Fourier transforms Heat resistance High temperature Hydrocarbons Interpenetrating networks Low temperature Materials Molecular weight Pavement materials Performance evaluation Physical properties Polymers Properties Rheological properties Rheology Scanning electron microscopy Temperature Test methods Viscosity |
| title | Effect of epoxy value on the rheological properties and microcosmic mechanism of WER emulsified asphalt |
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