Phase, microstructure and service character of as-deposited and short-time heat-treated Ni-Mo alloys with mixed state
Considering the amorphous and nano-crystalline cluster structure and their activity, on the basis of the mixed structure Ni-Mo alloys, the crystallization kinetics of the alloys and the performance of the alloys after heat treatment with different mixed structure were studied. The phase structure an...
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| Veröffentlicht in: | PloS one 2021-05, Vol.16 (5), p.e0249875-e0249875 |
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| creator | Xu, Hong Li, Ning Zhuo, Qinghua Lu, Lirong Chen, Weizeng |
| description | Considering the amorphous and nano-crystalline cluster structure and their activity, on the basis of the mixed structure Ni-Mo alloys, the crystallization kinetics of the alloys and the performance of the alloys after heat treatment with different mixed structure were studied. The phase structure and composition were determined by X-ray powder diffraction. The crystallization activation energy of the mixed structure was obtained by differential scanning calorimetry. The electrochemical activity of the mixed structure alloy was determined by electrochemical analysis. The experimental results show that the structural stability of the mixed-structure alloy is better, but the crystallization activation energy is much lower than that of the amorphous alloy. The crystallization process consists of a meta-stable structure transition and a new phase formation. The electrochemical properties of the alloy indicated that the alloy with the mixed structure has higher electrochemical activity, with higher hardness and better corrosion resistance, which results from the large true contact surface and the large number of active centers in this material structure. |
| doi_str_mv | 10.1371/journal.pone.0249875 |
| format | Article |
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The phase structure and composition were determined by X-ray powder diffraction. The crystallization activation energy of the mixed structure was obtained by differential scanning calorimetry. The electrochemical activity of the mixed structure alloy was determined by electrochemical analysis. The experimental results show that the structural stability of the mixed-structure alloy is better, but the crystallization activation energy is much lower than that of the amorphous alloy. The crystallization process consists of a meta-stable structure transition and a new phase formation. The electrochemical properties of the alloy indicated that the alloy with the mixed structure has higher electrochemical activity, with higher hardness and better corrosion resistance, which results from the large true contact surface and the large number of active centers in this material structure.</description><identifier>ISSN: 1932-6203</identifier><identifier>EISSN: 1932-6203</identifier><identifier>DOI: 10.1371/journal.pone.0249875</identifier><identifier>PMID: 34019559</identifier><language>eng</language><publisher>San Francisco: Public Library of Science</publisher><subject>Alloys ; Ammonia ; Ammonium ; Amorphous alloys ; Amorphous materials ; Amorphous structure ; Analysis ; Cathodic dissolution ; Corrosion resistance ; Crystallization ; Crystals ; Dissolution ; Electrodes ; Electroplating ; Engineering ; Engineering and Technology ; Engineering schools ; Ethylenediaminetetraacetic acids ; Experimental methods ; Heat ; Heat treatment ; Heat treatments ; Heating rate ; Low carbon steels ; Metallic glasses ; Molybdenum ; Nanocrystals ; Nickel base alloys ; Nitric acid ; Phase composition ; Physical Sciences ; Physicochemical properties ; Protective coatings ; Structure ; Thermal analysis ; Urea</subject><ispartof>PloS one, 2021-05, Vol.16 (5), p.e0249875-e0249875</ispartof><rights>COPYRIGHT 2021 Public Library of Science</rights><rights>2021 Xu et al. This is an open access article distributed under the terms of the Creative Commons Attribution License: http://creativecommons.org/licenses/by/4.0/ (the “License”), which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited. Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><rights>2021 Xu et al 2021 Xu et al</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c669t-2c51d81d8b2ae54bc8758a3e7e899f18abcff08a9e97f5d60758e1438f4a8fe03</citedby><cites>FETCH-LOGICAL-c669t-2c51d81d8b2ae54bc8758a3e7e899f18abcff08a9e97f5d60758e1438f4a8fe03</cites><orcidid>0000-0003-0294-1747</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC8139472/pdf/$$EPDF$$P50$$Gpubmedcentral$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC8139472/$$EHTML$$P50$$Gpubmedcentral$$Hfree_for_read</linktohtml><link.rule.ids>230,314,727,780,784,864,885,2102,2928,23866,27924,27925,53791,53793,79600,79601</link.rule.ids></links><search><contributor>Bakhsheshi-Rad, Hamid Reza</contributor><creatorcontrib>Xu, Hong</creatorcontrib><creatorcontrib>Li, Ning</creatorcontrib><creatorcontrib>Zhuo, Qinghua</creatorcontrib><creatorcontrib>Lu, Lirong</creatorcontrib><creatorcontrib>Chen, Weizeng</creatorcontrib><title>Phase, microstructure and service character of as-deposited and short-time heat-treated Ni-Mo alloys with mixed state</title><title>PloS one</title><description>Considering the amorphous and nano-crystalline cluster structure and their activity, on the basis of the mixed structure Ni-Mo alloys, the crystallization kinetics of the alloys and the performance of the alloys after heat treatment with different mixed structure were studied. The phase structure and composition were determined by X-ray powder diffraction. The crystallization activation energy of the mixed structure was obtained by differential scanning calorimetry. The electrochemical activity of the mixed structure alloy was determined by electrochemical analysis. The experimental results show that the structural stability of the mixed-structure alloy is better, but the crystallization activation energy is much lower than that of the amorphous alloy. The crystallization process consists of a meta-stable structure transition and a new phase formation. The electrochemical properties of the alloy indicated that the alloy with the mixed structure has higher electrochemical activity, with higher hardness and better corrosion resistance, which results from the large true contact surface and the large number of active centers in this material structure.</description><subject>Alloys</subject><subject>Ammonia</subject><subject>Ammonium</subject><subject>Amorphous alloys</subject><subject>Amorphous materials</subject><subject>Amorphous structure</subject><subject>Analysis</subject><subject>Cathodic dissolution</subject><subject>Corrosion resistance</subject><subject>Crystallization</subject><subject>Crystals</subject><subject>Dissolution</subject><subject>Electrodes</subject><subject>Electroplating</subject><subject>Engineering</subject><subject>Engineering and Technology</subject><subject>Engineering schools</subject><subject>Ethylenediaminetetraacetic acids</subject><subject>Experimental methods</subject><subject>Heat</subject><subject>Heat treatment</subject><subject>Heat treatments</subject><subject>Heating rate</subject><subject>Low carbon steels</subject><subject>Metallic glasses</subject><subject>Molybdenum</subject><subject>Nanocrystals</subject><subject>Nickel base alloys</subject><subject>Nitric acid</subject><subject>Phase composition</subject><subject>Physical Sciences</subject><subject>Physicochemical properties</subject><subject>Protective coatings</subject><subject>Structure</subject><subject>Thermal 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cluster structure and their activity, on the basis of the mixed structure Ni-Mo alloys, the crystallization kinetics of the alloys and the performance of the alloys after heat treatment with different mixed structure were studied. The phase structure and composition were determined by X-ray powder diffraction. The crystallization activation energy of the mixed structure was obtained by differential scanning calorimetry. The electrochemical activity of the mixed structure alloy was determined by electrochemical analysis. The experimental results show that the structural stability of the mixed-structure alloy is better, but the crystallization activation energy is much lower than that of the amorphous alloy. The crystallization process consists of a meta-stable structure transition and a new phase formation. The electrochemical properties of the alloy indicated that the alloy with the mixed structure has higher electrochemical activity, with higher hardness and better corrosion resistance, which results from the large true contact surface and the large number of active centers in this material structure.</abstract><cop>San Francisco</cop><pub>Public Library of Science</pub><pmid>34019559</pmid><doi>10.1371/journal.pone.0249875</doi><tpages>e0249875</tpages><orcidid>https://orcid.org/0000-0003-0294-1747</orcidid><oa>free_for_read</oa></addata></record> |
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| subjects | Alloys Ammonia Ammonium Amorphous alloys Amorphous materials Amorphous structure Analysis Cathodic dissolution Corrosion resistance Crystallization Crystals Dissolution Electrodes Electroplating Engineering Engineering and Technology Engineering schools Ethylenediaminetetraacetic acids Experimental methods Heat Heat treatment Heat treatments Heating rate Low carbon steels Metallic glasses Molybdenum Nanocrystals Nickel base alloys Nitric acid Phase composition Physical Sciences Physicochemical properties Protective coatings Structure Thermal analysis Urea |
| title | Phase, microstructure and service character of as-deposited and short-time heat-treated Ni-Mo alloys with mixed state |
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