A facile thermal-treatment route to synthesize ZnO nanosheets and effect of calcination temperature
A facile thermal-treatment route was successfully used to synthesize ZnO nanosheets. Morphological, structural, and optical properties of obtained nanoparticles at different calcination temperatures were studied using various techniques. The FTIR, XRD, EDX, SEM and TEM images confirmed the formation...
Gespeichert in:
| Veröffentlicht in: | PloS one 2014-08, Vol.9 (8), p.e103134 |
|---|---|
| Hauptverfasser: | , , , , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | |
|---|---|
| container_issue | 8 |
| container_start_page | e103134 |
| container_title | PloS one |
| container_volume | 9 |
| creator | Al-Hada, Naif Mohammed Saion, Elias B Shaari, Abdul Halim Kamarudin, Mazliana A Flaifel, Moayad Husein Ahmad, Sahrim Hj Gene, Salahudeen A |
| description | A facile thermal-treatment route was successfully used to synthesize ZnO nanosheets. Morphological, structural, and optical properties of obtained nanoparticles at different calcination temperatures were studied using various techniques. The FTIR, XRD, EDX, SEM and TEM images confirmed the formation of ZnO nanosheets through calcination in the temperature between 500 to 650 °C. The SEM images showed a morphological structure of ZnO nanosheets, which inclined to crumble at higher calcination temperatures. The XRD and FTIR spectra revealed that the samples were amorphous at 30 °C but transformed into a crystalline structure during calcination process. The average particle size and degree of crystallinity increased with increasing calcination temperature. The estimated average particle sizes from TEM images were about 23 and 38 nm for the lowest and highest calcination temperature i.e. 500 and 650 °C, respectively. The optical properties were determined by UV-Vis reflection spectrophotometer and showed a decrease in the band gap with increasing calcination temperature. |
| doi_str_mv | 10.1371/journal.pone.0103134 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_plos_</sourceid><recordid>TN_cdi_plos_journals_2014075822</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><doaj_id>oai_doaj_org_article_c09ecb84e3634731b7e76645249278bd</doaj_id><sourcerecordid>1551819213</sourcerecordid><originalsourceid>FETCH-LOGICAL-c526t-a45d092ed3e4445dd925d437acda55e76ce2ef4340da73f00aa3315cf5ea3ed83</originalsourceid><addsrcrecordid>eNptUstuFDEQHCEQCYE_QGCJC5ddbLc9jwtSFPGIFCkXuHCxeu2e7Kxm7MX2IIWvx8tOogRxcqu7qlzdqqp6LfhaQCM-7MIcPY7rffC05oKDAPWkOhUdyFUtOTx9UJ9UL1Laca6hrevn1YnUvINGy9PKnrMe7TASy1uKE46rHAnzRD6zGOZc-oGlW1-mafhN7Ie_Zh59SFuinBh6x6jvyWYWemZxtIPHPATPMk17ipjnSC-rZz2OiV4t71n1_fOnbxdfV1fXXy4vzq9WVss6r1BpxztJDkipUrtOaqegQetQa2pqS5J6BYo7bKDnHBFAaNtrQiDXwln19qi7H0Myy32SkVwo3uhWyoK4PCJcwJ3Zx2HCeGsCDuZvI8QbgzEPdiRjeUd20yqCGlQDYtMUB7XSUnWyaTeuaH1cfps3EzlbLhZxfCT6eOKHrbkJv4wSxUkNReD9IhDDz5lSNtOQLI0jegpzMkJr0YpOigP03T_Q_2-njigbQ0qR-nszgptDZu5Y5pAZs2Sm0N48XOSedBcS-AOyF8Dk</addsrcrecordid><sourcetype>Open Website</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2014075822</pqid></control><display><type>article</type><title>A facile thermal-treatment route to synthesize ZnO nanosheets and effect of calcination temperature</title><source>MEDLINE</source><source>DOAJ Directory of Open Access Journals</source><source>Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals</source><source>PubMed Central</source><source>Free Full-Text Journals in Chemistry</source><source>Public Library of Science (PLoS)</source><creator>Al-Hada, Naif Mohammed ; Saion, Elias B ; Shaari, Abdul Halim ; Kamarudin, Mazliana A ; Flaifel, Moayad Husein ; Ahmad, Sahrim Hj ; Gene, Salahudeen A</creator><contributor>Kuzyk, Mark G.</contributor><creatorcontrib>Al-Hada, Naif Mohammed ; Saion, Elias B ; Shaari, Abdul Halim ; Kamarudin, Mazliana A ; Flaifel, Moayad Husein ; Ahmad, Sahrim Hj ; Gene, Salahudeen A ; Kuzyk, Mark G.</creatorcontrib><description>A facile thermal-treatment route was successfully used to synthesize ZnO nanosheets. Morphological, structural, and optical properties of obtained nanoparticles at different calcination temperatures were studied using various techniques. The FTIR, XRD, EDX, SEM and TEM images confirmed the formation of ZnO nanosheets through calcination in the temperature between 500 to 650 °C. The SEM images showed a morphological structure of ZnO nanosheets, which inclined to crumble at higher calcination temperatures. The XRD and FTIR spectra revealed that the samples were amorphous at 30 °C but transformed into a crystalline structure during calcination process. The average particle size and degree of crystallinity increased with increasing calcination temperature. The estimated average particle sizes from TEM images were about 23 and 38 nm for the lowest and highest calcination temperature i.e. 500 and 650 °C, respectively. The optical properties were determined by UV-Vis reflection spectrophotometer and showed a decrease in the band gap with increasing calcination temperature.</description><identifier>ISSN: 1932-6203</identifier><identifier>EISSN: 1932-6203</identifier><identifier>DOI: 10.1371/journal.pone.0103134</identifier><identifier>PMID: 25093752</identifier><language>eng</language><publisher>United States: Public Library of Science</publisher><subject>Applied physics ; Crystal structure ; Crystallinity ; Degree of crystallinity ; Engineering and Technology ; Fourier transforms ; Heat treatment ; Hot Temperature ; Methods ; Microemulsions ; Microscopy, Electron, Scanning ; Microscopy, Electron, Transmission ; Morphology ; Nanoparticles ; Nanosheets ; Nanostructure ; Nanostructures - chemistry ; Nitrates ; Nitrates - chemistry ; Optical properties ; Organic chemicals ; Particle size ; Physical Sciences ; Povidone - chemistry ; Research and Analysis Methods ; Roasting ; Scanning electron microscopy ; Science ; Spectrophotometers ; Spectroscopy, Fourier Transform Infrared ; Surface Properties ; Synthesis ; Temperature ; Temperature effects ; Thermogravimetry ; Water - chemistry ; Zinc Compounds - chemistry ; Zinc oxide ; Zinc Oxide - chemistry ; Zinc oxides</subject><ispartof>PloS one, 2014-08, Vol.9 (8), p.e103134</ispartof><rights>2014 Al-Hada et al. This is an open-access article distributed under the terms of the Creative Commons Attribution License: http://creativecommons.org/licenses/by/4.0/ (the “License”), which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited. Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><rights>2014 Al-Hada et al 2014 Al-Hada et al</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c526t-a45d092ed3e4445dd925d437acda55e76ce2ef4340da73f00aa3315cf5ea3ed83</citedby><cites>FETCH-LOGICAL-c526t-a45d092ed3e4445dd925d437acda55e76ce2ef4340da73f00aa3315cf5ea3ed83</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC4122363/pdf/$$EPDF$$P50$$Gpubmedcentral$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC4122363/$$EHTML$$P50$$Gpubmedcentral$$Hfree_for_read</linktohtml><link.rule.ids>230,314,723,776,780,860,881,2096,2915,23845,27901,27902,53766,53768,79343,79344</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/25093752$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><contributor>Kuzyk, Mark G.</contributor><creatorcontrib>Al-Hada, Naif Mohammed</creatorcontrib><creatorcontrib>Saion, Elias B</creatorcontrib><creatorcontrib>Shaari, Abdul Halim</creatorcontrib><creatorcontrib>Kamarudin, Mazliana A</creatorcontrib><creatorcontrib>Flaifel, Moayad Husein</creatorcontrib><creatorcontrib>Ahmad, Sahrim Hj</creatorcontrib><creatorcontrib>Gene, Salahudeen A</creatorcontrib><title>A facile thermal-treatment route to synthesize ZnO nanosheets and effect of calcination temperature</title><title>PloS one</title><addtitle>PLoS One</addtitle><description>A facile thermal-treatment route was successfully used to synthesize ZnO nanosheets. Morphological, structural, and optical properties of obtained nanoparticles at different calcination temperatures were studied using various techniques. The FTIR, XRD, EDX, SEM and TEM images confirmed the formation of ZnO nanosheets through calcination in the temperature between 500 to 650 °C. The SEM images showed a morphological structure of ZnO nanosheets, which inclined to crumble at higher calcination temperatures. The XRD and FTIR spectra revealed that the samples were amorphous at 30 °C but transformed into a crystalline structure during calcination process. The average particle size and degree of crystallinity increased with increasing calcination temperature. The estimated average particle sizes from TEM images were about 23 and 38 nm for the lowest and highest calcination temperature i.e. 500 and 650 °C, respectively. The optical properties were determined by UV-Vis reflection spectrophotometer and showed a decrease in the band gap with increasing calcination temperature.</description><subject>Applied physics</subject><subject>Crystal structure</subject><subject>Crystallinity</subject><subject>Degree of crystallinity</subject><subject>Engineering and Technology</subject><subject>Fourier transforms</subject><subject>Heat treatment</subject><subject>Hot Temperature</subject><subject>Methods</subject><subject>Microemulsions</subject><subject>Microscopy, Electron, Scanning</subject><subject>Microscopy, Electron, Transmission</subject><subject>Morphology</subject><subject>Nanoparticles</subject><subject>Nanosheets</subject><subject>Nanostructure</subject><subject>Nanostructures - chemistry</subject><subject>Nitrates</subject><subject>Nitrates - chemistry</subject><subject>Optical properties</subject><subject>Organic chemicals</subject><subject>Particle size</subject><subject>Physical Sciences</subject><subject>Povidone - chemistry</subject><subject>Research and Analysis Methods</subject><subject>Roasting</subject><subject>Scanning electron microscopy</subject><subject>Science</subject><subject>Spectrophotometers</subject><subject>Spectroscopy, Fourier Transform Infrared</subject><subject>Surface Properties</subject><subject>Synthesis</subject><subject>Temperature</subject><subject>Temperature effects</subject><subject>Thermogravimetry</subject><subject>Water - chemistry</subject><subject>Zinc Compounds - chemistry</subject><subject>Zinc oxide</subject><subject>Zinc Oxide - chemistry</subject><subject>Zinc oxides</subject><issn>1932-6203</issn><issn>1932-6203</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><sourceid>BENPR</sourceid><sourceid>DOA</sourceid><recordid>eNptUstuFDEQHCEQCYE_QGCJC5ddbLc9jwtSFPGIFCkXuHCxeu2e7Kxm7MX2IIWvx8tOogRxcqu7qlzdqqp6LfhaQCM-7MIcPY7rffC05oKDAPWkOhUdyFUtOTx9UJ9UL1Laca6hrevn1YnUvINGy9PKnrMe7TASy1uKE46rHAnzRD6zGOZc-oGlW1-mafhN7Ie_Zh59SFuinBh6x6jvyWYWemZxtIPHPATPMk17ipjnSC-rZz2OiV4t71n1_fOnbxdfV1fXXy4vzq9WVss6r1BpxztJDkipUrtOaqegQetQa2pqS5J6BYo7bKDnHBFAaNtrQiDXwln19qi7H0Myy32SkVwo3uhWyoK4PCJcwJ3Zx2HCeGsCDuZvI8QbgzEPdiRjeUd20yqCGlQDYtMUB7XSUnWyaTeuaH1cfps3EzlbLhZxfCT6eOKHrbkJv4wSxUkNReD9IhDDz5lSNtOQLI0jegpzMkJr0YpOigP03T_Q_2-njigbQ0qR-nszgptDZu5Y5pAZs2Sm0N48XOSedBcS-AOyF8Dk</recordid><startdate>20140805</startdate><enddate>20140805</enddate><creator>Al-Hada, Naif Mohammed</creator><creator>Saion, Elias B</creator><creator>Shaari, Abdul Halim</creator><creator>Kamarudin, Mazliana A</creator><creator>Flaifel, Moayad Husein</creator><creator>Ahmad, Sahrim Hj</creator><creator>Gene, Salahudeen A</creator><general>Public Library of Science</general><general>Public Library of Science (PLoS)</general><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>7QG</scope><scope>7QL</scope><scope>7QO</scope><scope>7RV</scope><scope>7SN</scope><scope>7SS</scope><scope>7T5</scope><scope>7TG</scope><scope>7TM</scope><scope>7U9</scope><scope>7X2</scope><scope>7X7</scope><scope>7XB</scope><scope>88E</scope><scope>8AO</scope><scope>8C1</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>8FH</scope><scope>8FI</scope><scope>8FJ</scope><scope>8FK</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AEUYN</scope><scope>AFKRA</scope><scope>ARAPS</scope><scope>ATCPS</scope><scope>AZQEC</scope><scope>BBNVY</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>BHPHI</scope><scope>C1K</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>FR3</scope><scope>FYUFA</scope><scope>GHDGH</scope><scope>GNUQQ</scope><scope>H94</scope><scope>HCIFZ</scope><scope>K9.</scope><scope>KB.</scope><scope>KB0</scope><scope>KL.</scope><scope>L6V</scope><scope>LK8</scope><scope>M0K</scope><scope>M0S</scope><scope>M1P</scope><scope>M7N</scope><scope>M7P</scope><scope>M7S</scope><scope>NAPCQ</scope><scope>P5Z</scope><scope>P62</scope><scope>P64</scope><scope>PATMY</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope><scope>PYCSY</scope><scope>RC3</scope><scope>7X8</scope><scope>5PM</scope><scope>DOA</scope></search><sort><creationdate>20140805</creationdate><title>A facile thermal-treatment route to synthesize ZnO nanosheets and effect of calcination temperature</title><author>Al-Hada, Naif Mohammed ; Saion, Elias B ; Shaari, Abdul Halim ; Kamarudin, Mazliana A ; Flaifel, Moayad Husein ; Ahmad, Sahrim Hj ; Gene, Salahudeen A</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c526t-a45d092ed3e4445dd925d437acda55e76ce2ef4340da73f00aa3315cf5ea3ed83</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Applied physics</topic><topic>Crystal structure</topic><topic>Crystallinity</topic><topic>Degree of crystallinity</topic><topic>Engineering and Technology</topic><topic>Fourier transforms</topic><topic>Heat treatment</topic><topic>Hot Temperature</topic><topic>Methods</topic><topic>Microemulsions</topic><topic>Microscopy, Electron, Scanning</topic><topic>Microscopy, Electron, Transmission</topic><topic>Morphology</topic><topic>Nanoparticles</topic><topic>Nanosheets</topic><topic>Nanostructure</topic><topic>Nanostructures - chemistry</topic><topic>Nitrates</topic><topic>Nitrates - chemistry</topic><topic>Optical properties</topic><topic>Organic chemicals</topic><topic>Particle size</topic><topic>Physical Sciences</topic><topic>Povidone - chemistry</topic><topic>Research and Analysis Methods</topic><topic>Roasting</topic><topic>Scanning electron microscopy</topic><topic>Science</topic><topic>Spectrophotometers</topic><topic>Spectroscopy, Fourier Transform Infrared</topic><topic>Surface Properties</topic><topic>Synthesis</topic><topic>Temperature</topic><topic>Temperature effects</topic><topic>Thermogravimetry</topic><topic>Water - chemistry</topic><topic>Zinc Compounds - chemistry</topic><topic>Zinc oxide</topic><topic>Zinc Oxide - chemistry</topic><topic>Zinc oxides</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Al-Hada, Naif Mohammed</creatorcontrib><creatorcontrib>Saion, Elias B</creatorcontrib><creatorcontrib>Shaari, Abdul Halim</creatorcontrib><creatorcontrib>Kamarudin, Mazliana A</creatorcontrib><creatorcontrib>Flaifel, Moayad Husein</creatorcontrib><creatorcontrib>Ahmad, Sahrim Hj</creatorcontrib><creatorcontrib>Gene, Salahudeen A</creatorcontrib><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>ProQuest Central (Corporate)</collection><collection>Animal Behavior Abstracts</collection><collection>Bacteriology Abstracts (Microbiology B)</collection><collection>Biotechnology Research Abstracts</collection><collection>Nursing & Allied Health Database</collection><collection>Ecology Abstracts</collection><collection>Entomology Abstracts (Full archive)</collection><collection>Immunology Abstracts</collection><collection>Meteorological & Geoastrophysical Abstracts</collection><collection>Nucleic Acids Abstracts</collection><collection>Virology and AIDS Abstracts</collection><collection>Agricultural Science Collection</collection><collection>Health & Medical Collection</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>Medical Database (Alumni Edition)</collection><collection>ProQuest Pharma Collection</collection><collection>Public Health Database</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>ProQuest Natural Science Collection</collection><collection>Hospital Premium Collection</collection><collection>Hospital Premium Collection (Alumni Edition)</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest One Sustainability</collection><collection>ProQuest Central UK/Ireland</collection><collection>Advanced Technologies & Aerospace Collection</collection><collection>Agricultural & Environmental Science Collection</collection><collection>ProQuest Central Essentials</collection><collection>Biological Science Collection</collection><collection>ProQuest Central</collection><collection>Technology Collection (ProQuest)</collection><collection>Natural Science Collection</collection><collection>Environmental Sciences and Pollution Management</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>Engineering Research Database</collection><collection>Health Research Premium Collection</collection><collection>Health Research Premium Collection (Alumni)</collection><collection>ProQuest Central Student</collection><collection>AIDS and Cancer Research Abstracts</collection><collection>SciTech Premium Collection</collection><collection>ProQuest Health & Medical Complete (Alumni)</collection><collection>Materials Science Database</collection><collection>Nursing & Allied Health Database (Alumni Edition)</collection><collection>Meteorological & Geoastrophysical Abstracts - Academic</collection><collection>ProQuest Engineering Collection</collection><collection>ProQuest Biological Science Collection</collection><collection>Agricultural Science Database</collection><collection>Health & Medical Collection (Alumni Edition)</collection><collection>Medical Database</collection><collection>Algology Mycology and Protozoology Abstracts (Microbiology C)</collection><collection>Biological Science Database</collection><collection>Engineering Database</collection><collection>Nursing & Allied Health Premium</collection><collection>Advanced Technologies & Aerospace Database</collection><collection>ProQuest Advanced Technologies & Aerospace Collection</collection><collection>Biotechnology and BioEngineering Abstracts</collection><collection>Environmental Science Database</collection><collection>Materials Science Collection</collection><collection>Publicly Available Content Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>Engineering Collection</collection><collection>Environmental Science Collection</collection><collection>Genetics Abstracts</collection><collection>MEDLINE - Academic</collection><collection>PubMed Central (Full Participant titles)</collection><collection>DOAJ Directory of Open Access Journals</collection><jtitle>PloS one</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Al-Hada, Naif Mohammed</au><au>Saion, Elias B</au><au>Shaari, Abdul Halim</au><au>Kamarudin, Mazliana A</au><au>Flaifel, Moayad Husein</au><au>Ahmad, Sahrim Hj</au><au>Gene, Salahudeen A</au><au>Kuzyk, Mark G.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A facile thermal-treatment route to synthesize ZnO nanosheets and effect of calcination temperature</atitle><jtitle>PloS one</jtitle><addtitle>PLoS One</addtitle><date>2014-08-05</date><risdate>2014</risdate><volume>9</volume><issue>8</issue><spage>e103134</spage><pages>e103134-</pages><issn>1932-6203</issn><eissn>1932-6203</eissn><abstract>A facile thermal-treatment route was successfully used to synthesize ZnO nanosheets. Morphological, structural, and optical properties of obtained nanoparticles at different calcination temperatures were studied using various techniques. The FTIR, XRD, EDX, SEM and TEM images confirmed the formation of ZnO nanosheets through calcination in the temperature between 500 to 650 °C. The SEM images showed a morphological structure of ZnO nanosheets, which inclined to crumble at higher calcination temperatures. The XRD and FTIR spectra revealed that the samples were amorphous at 30 °C but transformed into a crystalline structure during calcination process. The average particle size and degree of crystallinity increased with increasing calcination temperature. The estimated average particle sizes from TEM images were about 23 and 38 nm for the lowest and highest calcination temperature i.e. 500 and 650 °C, respectively. The optical properties were determined by UV-Vis reflection spectrophotometer and showed a decrease in the band gap with increasing calcination temperature.</abstract><cop>United States</cop><pub>Public Library of Science</pub><pmid>25093752</pmid><doi>10.1371/journal.pone.0103134</doi><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1932-6203 |
| ispartof | PloS one, 2014-08, Vol.9 (8), p.e103134 |
| issn | 1932-6203 1932-6203 |
| language | eng |
| recordid | cdi_plos_journals_2014075822 |
| source | MEDLINE; DOAJ Directory of Open Access Journals; Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals; PubMed Central; Free Full-Text Journals in Chemistry; Public Library of Science (PLoS) |
| subjects | Applied physics Crystal structure Crystallinity Degree of crystallinity Engineering and Technology Fourier transforms Heat treatment Hot Temperature Methods Microemulsions Microscopy, Electron, Scanning Microscopy, Electron, Transmission Morphology Nanoparticles Nanosheets Nanostructure Nanostructures - chemistry Nitrates Nitrates - chemistry Optical properties Organic chemicals Particle size Physical Sciences Povidone - chemistry Research and Analysis Methods Roasting Scanning electron microscopy Science Spectrophotometers Spectroscopy, Fourier Transform Infrared Surface Properties Synthesis Temperature Temperature effects Thermogravimetry Water - chemistry Zinc Compounds - chemistry Zinc oxide Zinc Oxide - chemistry Zinc oxides |
| title | A facile thermal-treatment route to synthesize ZnO nanosheets and effect of calcination temperature |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-31T13%3A23%3A45IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_plos_&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=A%20facile%20thermal-treatment%20route%20to%20synthesize%20ZnO%20nanosheets%20and%20effect%20of%20calcination%20temperature&rft.jtitle=PloS%20one&rft.au=Al-Hada,%20Naif%20Mohammed&rft.date=2014-08-05&rft.volume=9&rft.issue=8&rft.spage=e103134&rft.pages=e103134-&rft.issn=1932-6203&rft.eissn=1932-6203&rft_id=info:doi/10.1371/journal.pone.0103134&rft_dat=%3Cproquest_plos_%3E1551819213%3C/proquest_plos_%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2014075822&rft_id=info:pmid/25093752&rft_doaj_id=oai_doaj_org_article_c09ecb84e3634731b7e76645249278bd&rfr_iscdi=true |