The structure of Dimethylaminomethanediphosphonic Acid, C3H11NO6P2
Mr = 218.9, monoclinic, P 21/c, a = 6.870(1), b = 10.824(2), c = 11.337(2) Å, β = = 94.59(2)0, Z = 4, V = 840.5(3) Å3, Dx = 1.73 Mgm−3. Final R = 0.033 for 2648 independent reflections, excluding those with |F0| < 3σ(F0). Intensities were measured with an automatic diffractometer. This organophos...
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| Veröffentlicht in: | Crystal research and technology (1979) 1984, Vol.19 (5), p.669-674 |
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| container_title | Crystal research and technology (1979) |
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| creator | Kulpe, S. Seidel, I. Szulzewsky, K. |
| description | Mr = 218.9, monoclinic, P 21/c, a = 6.870(1), b = 10.824(2), c = 11.337(2) Å, β = = 94.59(2)0, Z = 4, V = 840.5(3) Å3, Dx = 1.73 Mgm−3. Final R = 0.033 for 2648 independent reflections, excluding those with |F0| < 3σ(F0). Intensities were measured with an automatic diffractometer. This organophosphorous compound is characterized by two PC bonds. Four symmetrically independent intermolecular hydrogen bonds determine the threedimensional packing of the molecules and the unique chemical properties of the campound.
Mr = 218,9, monoklin, P 21/c, a = 6,870(1), b = 10,824(2), c = 11,337(2) Å, β = = 94,59(2)0, Z = 4, V = 840,5(3) Å3, Dx = 1,730(1) Mg m−3. Abschließender R = 0,033 für 2648 unabhängige Reflexe, ausschließlich derjenigen mit |F0| < 3 σ(F0). Intensitäten wurden mit einem automatischen Diffraktometer gemessen. Diese phosphororganische Verbindung ist durch zwei PC‐Bindungen charakterisiert. Vier symmetrieunabhängige intermolekulare Wasserstoffbrückenbindungen bestimmen die dreidimensionale Packung der Moleküle und die besonderen chemischen Eigenschaften der Verbindung. |
| doi_str_mv | 10.1002/crat.2170190518 |
| format | Article |
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Mr = 218,9, monoklin, P 21/c, a = 6,870(1), b = 10,824(2), c = 11,337(2) Å, β = = 94,59(2)0, Z = 4, V = 840,5(3) Å3, Dx = 1,730(1) Mg m−3. Abschließender R = 0,033 für 2648 unabhängige Reflexe, ausschließlich derjenigen mit |F0| < 3 σ(F0). Intensitäten wurden mit einem automatischen Diffraktometer gemessen. Diese phosphororganische Verbindung ist durch zwei PC‐Bindungen charakterisiert. Vier symmetrieunabhängige intermolekulare Wasserstoffbrückenbindungen bestimmen die dreidimensionale Packung der Moleküle und die besonderen chemischen Eigenschaften der Verbindung.</description><identifier>ISSN: 0232-1300</identifier><identifier>EISSN: 1521-4079</identifier><identifier>DOI: 10.1002/crat.2170190518</identifier><identifier>CODEN: CRTEDF</identifier><language>eng</language><publisher>Berlin: WILEY-VCH Verlag</publisher><subject>Condensed matter: structure, mechanical and thermal properties ; Exact sciences and technology ; Organic compounds ; Organometalloidal and organometallic compounds ; Physics ; Structure of solids and liquids; crystallography ; Structure of specific crystalline solids</subject><ispartof>Crystal research and technology (1979), 1984, Vol.19 (5), p.669-674</ispartof><rights>Copyright © 1984 WILEY‐VCH Verlag GmbH & Co. KGaA</rights><rights>1985 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fcrat.2170190518$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fcrat.2170190518$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,776,780,1411,4009,27902,27903,27904,45553,45554</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=8853810$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Kulpe, S.</creatorcontrib><creatorcontrib>Seidel, I.</creatorcontrib><creatorcontrib>Szulzewsky, K.</creatorcontrib><title>The structure of Dimethylaminomethanediphosphonic Acid, C3H11NO6P2</title><title>Crystal research and technology (1979)</title><addtitle>Cryst. Res. Technol</addtitle><description>Mr = 218.9, monoclinic, P 21/c, a = 6.870(1), b = 10.824(2), c = 11.337(2) Å, β = = 94.59(2)0, Z = 4, V = 840.5(3) Å3, Dx = 1.73 Mgm−3. Final R = 0.033 for 2648 independent reflections, excluding those with |F0| < 3σ(F0). Intensities were measured with an automatic diffractometer. This organophosphorous compound is characterized by two PC bonds. Four symmetrically independent intermolecular hydrogen bonds determine the threedimensional packing of the molecules and the unique chemical properties of the campound.
Mr = 218,9, monoklin, P 21/c, a = 6,870(1), b = 10,824(2), c = 11,337(2) Å, β = = 94,59(2)0, Z = 4, V = 840,5(3) Å3, Dx = 1,730(1) Mg m−3. Abschließender R = 0,033 für 2648 unabhängige Reflexe, ausschließlich derjenigen mit |F0| < 3 σ(F0). Intensitäten wurden mit einem automatischen Diffraktometer gemessen. Diese phosphororganische Verbindung ist durch zwei PC‐Bindungen charakterisiert. Vier symmetrieunabhängige intermolekulare Wasserstoffbrückenbindungen bestimmen die dreidimensionale Packung der Moleküle und die besonderen chemischen Eigenschaften der Verbindung.</description><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Exact sciences and technology</subject><subject>Organic compounds</subject><subject>Organometalloidal and organometallic compounds</subject><subject>Physics</subject><subject>Structure of solids and liquids; crystallography</subject><subject>Structure of specific crystalline solids</subject><issn>0232-1300</issn><issn>1521-4079</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1984</creationdate><recordtype>article</recordtype><recordid>eNpFkEFPwzAMhSMEEmNw5toDRzpsp21ScRoDNqRqQzDEMUrTVAt03dR0gv17Og1tB8u2_J5lf4xdIwwQgO5Mo9sBoQBMIUZ5wnoYE4YRiPSU9YA4hcgBztmF918AkCYR9djDfGED3zYb024aG6zK4NEtbbvYVnrp6tWu1LUt3Hqx8l3UzgRD44rbYMQniNNZ8kqX7KzUlbdX_7nPPp6f5qNJmM3GL6NhFjqUqQyJG4JcdKflhgRRAlwLbQqRg8nR2IggEUApiihOdJKT1GWRQk5xKrsnYt5nN_u9a-2NrspG18Z5tW7cUjdbJWXMJUInu9_Lflxlt4cxgtphUjtM6ohJjd6G82PbucO92_nW_h7cuvlWieAiVp_TsYr4NHvPpFQP_A-9n2tZ</recordid><startdate>1984</startdate><enddate>1984</enddate><creator>Kulpe, S.</creator><creator>Seidel, I.</creator><creator>Szulzewsky, K.</creator><general>WILEY-VCH Verlag</general><general>WILEY‐VCH Verlag</general><general>Wiley-VCH</general><scope>BSCLL</scope><scope>IQODW</scope></search><sort><creationdate>1984</creationdate><title>The structure of Dimethylaminomethanediphosphonic Acid, C3H11NO6P2</title><author>Kulpe, S. ; Seidel, I. ; Szulzewsky, K.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-i1898-23c20b7518bc2722603a7acd7b0cb1ce4206702917456a6b28afd90b259840753</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1984</creationdate><topic>Condensed matter: structure, mechanical and thermal properties</topic><topic>Exact sciences and technology</topic><topic>Organic compounds</topic><topic>Organometalloidal and organometallic compounds</topic><topic>Physics</topic><topic>Structure of solids and liquids; crystallography</topic><topic>Structure of specific crystalline solids</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Kulpe, S.</creatorcontrib><creatorcontrib>Seidel, I.</creatorcontrib><creatorcontrib>Szulzewsky, K.</creatorcontrib><collection>Istex</collection><collection>Pascal-Francis</collection><jtitle>Crystal research and technology (1979)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Kulpe, S.</au><au>Seidel, I.</au><au>Szulzewsky, K.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>The structure of Dimethylaminomethanediphosphonic Acid, C3H11NO6P2</atitle><jtitle>Crystal research and technology (1979)</jtitle><addtitle>Cryst. Res. Technol</addtitle><date>1984</date><risdate>1984</risdate><volume>19</volume><issue>5</issue><spage>669</spage><epage>674</epage><pages>669-674</pages><issn>0232-1300</issn><eissn>1521-4079</eissn><coden>CRTEDF</coden><abstract>Mr = 218.9, monoclinic, P 21/c, a = 6.870(1), b = 10.824(2), c = 11.337(2) Å, β = = 94.59(2)0, Z = 4, V = 840.5(3) Å3, Dx = 1.73 Mgm−3. Final R = 0.033 for 2648 independent reflections, excluding those with |F0| < 3σ(F0). Intensities were measured with an automatic diffractometer. This organophosphorous compound is characterized by two PC bonds. Four symmetrically independent intermolecular hydrogen bonds determine the threedimensional packing of the molecules and the unique chemical properties of the campound.
Mr = 218,9, monoklin, P 21/c, a = 6,870(1), b = 10,824(2), c = 11,337(2) Å, β = = 94,59(2)0, Z = 4, V = 840,5(3) Å3, Dx = 1,730(1) Mg m−3. Abschließender R = 0,033 für 2648 unabhängige Reflexe, ausschließlich derjenigen mit |F0| < 3 σ(F0). Intensitäten wurden mit einem automatischen Diffraktometer gemessen. Diese phosphororganische Verbindung ist durch zwei PC‐Bindungen charakterisiert. Vier symmetrieunabhängige intermolekulare Wasserstoffbrückenbindungen bestimmen die dreidimensionale Packung der Moleküle und die besonderen chemischen Eigenschaften der Verbindung.</abstract><cop>Berlin</cop><pub>WILEY-VCH Verlag</pub><doi>10.1002/crat.2170190518</doi><tpages>6</tpages></addata></record> |
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| source | Wiley-Blackwell Journals |
| subjects | Condensed matter: structure, mechanical and thermal properties Exact sciences and technology Organic compounds Organometalloidal and organometallic compounds Physics Structure of solids and liquids crystallography Structure of specific crystalline solids |
| title | The structure of Dimethylaminomethanediphosphonic Acid, C3H11NO6P2 |
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