1H and 13C NMR analysis of brassinosteroids
The 1H and 13C NMR spectra of the two phytohormones, brassinolide and 24‐epi‐brassinolide, and the two synthetic analogues 22,23,24‐trisepi‐brassinolide and (22S,23S)‐28‐homo‐brassinolide, were assigned using 1D and 2D NMR techniques. Independent assignment strategies are presented for the 1H and 13...
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| Veröffentlicht in: | Magnetic resonance in chemistry 1992-07, Vol.30 (7), p.651-657 |
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| container_end_page | 657 |
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| container_issue | 7 |
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| container_title | Magnetic resonance in chemistry |
| container_volume | 30 |
| creator | Porzel, Andrea Marquardt, Volker Adam, Günter Massiot, Georges Zeigan, Dieter |
| description | The 1H and 13C NMR spectra of the two phytohormones, brassinolide and 24‐epi‐brassinolide, and the two synthetic analogues 22,23,24‐trisepi‐brassinolide and (22S,23S)‐28‐homo‐brassinolide, were assigned using 1D and 2D NMR techniques. Independent assignment strategies are presented for the 1H and 13C chemical shifts of the steroidal side‐chain. |
| doi_str_mv | 10.1002/mrc.1260300714 |
| format | Article |
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Independent assignment strategies are presented for the 1H and 13C chemical shifts of the steroidal side‐chain.</description><identifier>ISSN: 0749-1581</identifier><identifier>EISSN: 1097-458X</identifier><identifier>DOI: 10.1002/mrc.1260300714</identifier><identifier>CODEN: MRCHEG</identifier><language>eng</language><publisher>Chichester, UK: John Wiley & Sons, Ltd</publisher><subject>1H and 13C chemical shift assignment ; 1H COSY ; Atomic and molecular physics ; Brassinosteroids ; Exact sciences and technology ; HMBC ; HMQC ; Molecular properties and interactions with photons ; Nuclear resonance and relaxation ; Partially relaxed ; Physics ; Relayed COSY ; XHCORRD</subject><ispartof>Magnetic resonance in chemistry, 1992-07, Vol.30 (7), p.651-657</ispartof><rights>Copyright © 1992 John Wiley & Sons, Ltd.</rights><rights>1993 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fmrc.1260300714$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fmrc.1260300714$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,776,780,1411,27901,27902,45550,45551</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=4352051$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Porzel, Andrea</creatorcontrib><creatorcontrib>Marquardt, Volker</creatorcontrib><creatorcontrib>Adam, Günter</creatorcontrib><creatorcontrib>Massiot, Georges</creatorcontrib><creatorcontrib>Zeigan, Dieter</creatorcontrib><title>1H and 13C NMR analysis of brassinosteroids</title><title>Magnetic resonance in chemistry</title><addtitle>Magn. Reson. Chem</addtitle><description>The 1H and 13C NMR spectra of the two phytohormones, brassinolide and 24‐epi‐brassinolide, and the two synthetic analogues 22,23,24‐trisepi‐brassinolide and (22S,23S)‐28‐homo‐brassinolide, were assigned using 1D and 2D NMR techniques. 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| ispartof | Magnetic resonance in chemistry, 1992-07, Vol.30 (7), p.651-657 |
| issn | 0749-1581 1097-458X |
| language | eng |
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| source | Wiley Online Library Journals Frontfile Complete |
| subjects | 1H and 13C chemical shift assignment 1H COSY Atomic and molecular physics Brassinosteroids Exact sciences and technology HMBC HMQC Molecular properties and interactions with photons Nuclear resonance and relaxation Partially relaxed Physics Relayed COSY XHCORRD |
| title | 1H and 13C NMR analysis of brassinosteroids |
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