Determination of Glyoxal, Methylglyoxal, Diacethyl, and 2, 3-Pentanedione in Fermented Foods by High-Performance Liquid Chromatography with Fluorescence Detection
A highly sensitive and rapid high-performance liquid chromatographic method for the determination of glyoxal, methylglyoxaJ. diacethyl, and 2, 3-pentanedione in fermented foods is described. After extraction of the compounds with methanol, the compounds in the extract are converted into the correspo...
Gespeichert in:
| Veröffentlicht in: | Journal of liquid chromatography 1994-01, Vol.17 (1), p.203-211 |
|---|---|
| Hauptverfasser: | , , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 211 |
|---|---|
| container_issue | 1 |
| container_start_page | 203 |
| container_title | Journal of liquid chromatography |
| container_volume | 17 |
| creator | Yamaguchi, M. Ishida, J. Xuan, Z. X. Nakamura, A. Yoshitake, T. |
| description | A highly sensitive and rapid high-performance liquid chromatographic method for the determination of glyoxal, methylglyoxaJ. diacethyl, and 2, 3-pentanedione in fermented foods is described. After extraction of the compounds with methanol, the compounds in the extract are converted into the corresponding fluorescent derivatives by reaction with 1.2-diamino-4.5-methylenedioxybenzene. a fluorogenic reagent for α-dicarbonyl compounds. The derivatives are separated on a reversed-phase column (L-column ODS) with isocratic elution using acetonitrile −0.5M ammonium acetate, and are detected fluorimetrically. The detection limits are 11.6-13.8 fmol per 10-μl injection for all the compounds at a signal to noise ratio of 3. |
| doi_str_mv | 10.1080/10826079408013445 |
| format | Article |
| fullrecord | <record><control><sourceid>pascalfrancis_infor</sourceid><recordid>TN_cdi_pascalfrancis_primary_4071388</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>4071388</sourcerecordid><originalsourceid>FETCH-LOGICAL-c325t-c903f9050b9cf171684339ed71ff77e24877c02714152d6dc6833db85b9266513</originalsourceid><addsrcrecordid>eNp1kL9OwzAQxi0EEhX0Adg8MDZgx07sSCyoJS1SEQwwR67_NEZpXOxUJa_Dk-K2lAVxg093-n535w-AK4xuMOLoNj5pjlhBY4EJpdkJGKSE4ARRTE7BAGHKE1Lg4hwMQ3hHMTLKaM4H4GuiO-1XthWddS10Bk6b3n2KZgSfdFf3zfJYTqyQ-84IilbBdARJ8qLbTrRaRVRD28IyjootrWDpnApw0cOZXdZR543zK9FKDef2Y2MVHNferUTnll6s6x5ubVfDstk4r4PUO93uMLk76hKcGdEEPfzJF-CtfHgdz5L58_RxfD9PJEmzLpEFIqZAGVoU0mCGc04JKbRi2BjGdEo5YxKlDFOcpSpXMueEqAXPFkWa5xkmFwAf5krvQvDaVGtvV8L3FUbVzufqj8-RuT4waxGkaIyPX7ThF6SIYcJ5lN0dZLbd-7B1vlFVJ_rG-SND_t_yDXvfkIM</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype></control><display><type>article</type><title>Determination of Glyoxal, Methylglyoxal, Diacethyl, and 2, 3-Pentanedione in Fermented Foods by High-Performance Liquid Chromatography with Fluorescence Detection</title><source>Taylor & Francis Journals Complete</source><creator>Yamaguchi, M. ; Ishida, J. ; Xuan, Z. X. ; Nakamura, A. ; Yoshitake, T.</creator><creatorcontrib>Yamaguchi, M. ; Ishida, J. ; Xuan, Z. X. ; Nakamura, A. ; Yoshitake, T.</creatorcontrib><description>A highly sensitive and rapid high-performance liquid chromatographic method for the determination of glyoxal, methylglyoxaJ. diacethyl, and 2, 3-pentanedione in fermented foods is described. After extraction of the compounds with methanol, the compounds in the extract are converted into the corresponding fluorescent derivatives by reaction with 1.2-diamino-4.5-methylenedioxybenzene. a fluorogenic reagent for α-dicarbonyl compounds. The derivatives are separated on a reversed-phase column (L-column ODS) with isocratic elution using acetonitrile −0.5M ammonium acetate, and are detected fluorimetrically. The detection limits are 11.6-13.8 fmol per 10-μl injection for all the compounds at a signal to noise ratio of 3.</description><identifier>ISSN: 0148-3919</identifier><identifier>EISSN: 2331-0413</identifier><identifier>DOI: 10.1080/10826079408013445</identifier><identifier>CODEN: JLCHD8</identifier><language>eng</language><publisher>New York, NY: Taylor & Francis Group</publisher><subject>Biological and medical sciences ; Fermented food industries ; Food industries ; Fundamental and applied biological sciences. Psychology ; Other fermented food industries</subject><ispartof>Journal of liquid chromatography, 1994-01, Vol.17 (1), p.203-211</ispartof><rights>Copyright Taylor & Francis Group, LLC 1994</rights><rights>1994 INIST-CNRS</rights><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c325t-c903f9050b9cf171684339ed71ff77e24877c02714152d6dc6833db85b9266513</citedby><cites>FETCH-LOGICAL-c325t-c903f9050b9cf171684339ed71ff77e24877c02714152d6dc6833db85b9266513</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.tandfonline.com/doi/pdf/10.1080/10826079408013445$$EPDF$$P50$$Ginformaworld$$H</linktopdf><linktohtml>$$Uhttps://www.tandfonline.com/doi/full/10.1080/10826079408013445$$EHTML$$P50$$Ginformaworld$$H</linktohtml><link.rule.ids>314,776,780,4009,27902,27903,27904,59623,60412</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=4071388$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Yamaguchi, M.</creatorcontrib><creatorcontrib>Ishida, J.</creatorcontrib><creatorcontrib>Xuan, Z. X.</creatorcontrib><creatorcontrib>Nakamura, A.</creatorcontrib><creatorcontrib>Yoshitake, T.</creatorcontrib><title>Determination of Glyoxal, Methylglyoxal, Diacethyl, and 2, 3-Pentanedione in Fermented Foods by High-Performance Liquid Chromatography with Fluorescence Detection</title><title>Journal of liquid chromatography</title><description>A highly sensitive and rapid high-performance liquid chromatographic method for the determination of glyoxal, methylglyoxaJ. diacethyl, and 2, 3-pentanedione in fermented foods is described. After extraction of the compounds with methanol, the compounds in the extract are converted into the corresponding fluorescent derivatives by reaction with 1.2-diamino-4.5-methylenedioxybenzene. a fluorogenic reagent for α-dicarbonyl compounds. The derivatives are separated on a reversed-phase column (L-column ODS) with isocratic elution using acetonitrile −0.5M ammonium acetate, and are detected fluorimetrically. The detection limits are 11.6-13.8 fmol per 10-μl injection for all the compounds at a signal to noise ratio of 3.</description><subject>Biological and medical sciences</subject><subject>Fermented food industries</subject><subject>Food industries</subject><subject>Fundamental and applied biological sciences. Psychology</subject><subject>Other fermented food industries</subject><issn>0148-3919</issn><issn>2331-0413</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1994</creationdate><recordtype>article</recordtype><recordid>eNp1kL9OwzAQxi0EEhX0Adg8MDZgx07sSCyoJS1SEQwwR67_NEZpXOxUJa_Dk-K2lAVxg093-n535w-AK4xuMOLoNj5pjlhBY4EJpdkJGKSE4ARRTE7BAGHKE1Lg4hwMQ3hHMTLKaM4H4GuiO-1XthWddS10Bk6b3n2KZgSfdFf3zfJYTqyQ-84IilbBdARJ8qLbTrRaRVRD28IyjootrWDpnApw0cOZXdZR543zK9FKDef2Y2MVHNferUTnll6s6x5ubVfDstk4r4PUO93uMLk76hKcGdEEPfzJF-CtfHgdz5L58_RxfD9PJEmzLpEFIqZAGVoU0mCGc04JKbRi2BjGdEo5YxKlDFOcpSpXMueEqAXPFkWa5xkmFwAf5krvQvDaVGtvV8L3FUbVzufqj8-RuT4waxGkaIyPX7ThF6SIYcJ5lN0dZLbd-7B1vlFVJ_rG-SND_t_yDXvfkIM</recordid><startdate>19940101</startdate><enddate>19940101</enddate><creator>Yamaguchi, M.</creator><creator>Ishida, J.</creator><creator>Xuan, Z. X.</creator><creator>Nakamura, A.</creator><creator>Yoshitake, T.</creator><general>Taylor & Francis Group</general><general>Dekker</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>19940101</creationdate><title>Determination of Glyoxal, Methylglyoxal, Diacethyl, and 2, 3-Pentanedione in Fermented Foods by High-Performance Liquid Chromatography with Fluorescence Detection</title><author>Yamaguchi, M. ; Ishida, J. ; Xuan, Z. X. ; Nakamura, A. ; Yoshitake, T.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c325t-c903f9050b9cf171684339ed71ff77e24877c02714152d6dc6833db85b9266513</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1994</creationdate><topic>Biological and medical sciences</topic><topic>Fermented food industries</topic><topic>Food industries</topic><topic>Fundamental and applied biological sciences. Psychology</topic><topic>Other fermented food industries</topic><toplevel>online_resources</toplevel><creatorcontrib>Yamaguchi, M.</creatorcontrib><creatorcontrib>Ishida, J.</creatorcontrib><creatorcontrib>Xuan, Z. X.</creatorcontrib><creatorcontrib>Nakamura, A.</creatorcontrib><creatorcontrib>Yoshitake, T.</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><jtitle>Journal of liquid chromatography</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Yamaguchi, M.</au><au>Ishida, J.</au><au>Xuan, Z. X.</au><au>Nakamura, A.</au><au>Yoshitake, T.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Determination of Glyoxal, Methylglyoxal, Diacethyl, and 2, 3-Pentanedione in Fermented Foods by High-Performance Liquid Chromatography with Fluorescence Detection</atitle><jtitle>Journal of liquid chromatography</jtitle><date>1994-01-01</date><risdate>1994</risdate><volume>17</volume><issue>1</issue><spage>203</spage><epage>211</epage><pages>203-211</pages><issn>0148-3919</issn><eissn>2331-0413</eissn><coden>JLCHD8</coden><abstract>A highly sensitive and rapid high-performance liquid chromatographic method for the determination of glyoxal, methylglyoxaJ. diacethyl, and 2, 3-pentanedione in fermented foods is described. After extraction of the compounds with methanol, the compounds in the extract are converted into the corresponding fluorescent derivatives by reaction with 1.2-diamino-4.5-methylenedioxybenzene. a fluorogenic reagent for α-dicarbonyl compounds. The derivatives are separated on a reversed-phase column (L-column ODS) with isocratic elution using acetonitrile −0.5M ammonium acetate, and are detected fluorimetrically. The detection limits are 11.6-13.8 fmol per 10-μl injection for all the compounds at a signal to noise ratio of 3.</abstract><cop>New York, NY</cop><pub>Taylor & Francis Group</pub><doi>10.1080/10826079408013445</doi><tpages>9</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0148-3919 |
| ispartof | Journal of liquid chromatography, 1994-01, Vol.17 (1), p.203-211 |
| issn | 0148-3919 2331-0413 |
| language | eng |
| recordid | cdi_pascalfrancis_primary_4071388 |
| source | Taylor & Francis Journals Complete |
| subjects | Biological and medical sciences Fermented food industries Food industries Fundamental and applied biological sciences. Psychology Other fermented food industries |
| title | Determination of Glyoxal, Methylglyoxal, Diacethyl, and 2, 3-Pentanedione in Fermented Foods by High-Performance Liquid Chromatography with Fluorescence Detection |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-25T09%3A09%3A39IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-pascalfrancis_infor&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Determination%20of%20Glyoxal,%20Methylglyoxal,%20Diacethyl,%20and%202,%203-Pentanedione%20in%20Fermented%20Foods%20by%20High-Performance%20Liquid%20Chromatography%20with%20Fluorescence%20Detection&rft.jtitle=Journal%20of%20liquid%20chromatography&rft.au=Yamaguchi,%20M.&rft.date=1994-01-01&rft.volume=17&rft.issue=1&rft.spage=203&rft.epage=211&rft.pages=203-211&rft.issn=0148-3919&rft.eissn=2331-0413&rft.coden=JLCHD8&rft_id=info:doi/10.1080/10826079408013445&rft_dat=%3Cpascalfrancis_infor%3E4071388%3C/pascalfrancis_infor%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_id=info:pmid/&rfr_iscdi=true |