Surface Interrogation Scanning Electrochemical Microscopy (SI-SECM) of Photoelectrochemistry at a W/Mo-BiVO4 Semiconductor Electrode: Quantification of Hydroxyl Radicals during Water Oxidation

Reaction kinetics and surface coverage of water oxidation intermediates at a W/Mo-BiVO4 photoanode were studied using surface interrogation scanning electrochemical microscopy (SI-SECM). Adsorbed hydroxyl radicals (OH•) were produced during water oxidation at the semiconductor surface under UV–visib...

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Veröffentlicht in:Journal of physical chemistry. C 2013-06, Vol.117 (23), p.12093-12102
Hauptverfasser: Park, Hyun S, Leonard, Kevin C, Bard, Allen J
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Sprache:eng
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