A new approach to follow the formation of iron oxide nanoparticles synthesized by thermal decomposition
A novel way has been proposed to follow the formation of nanocrystalline magnetite. Iron oxide nanoparticles were synthesized by the thermal decomposition of Fe(acac)3 in the presence of oleic acid and oleylamine surfactants at high temperature. The species produced during the synthetic process are...
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| Veröffentlicht in: | Nanotechnology 2013-02, Vol.24 (5), p.055705-055705 |
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| container_issue | 5 |
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| container_title | Nanotechnology |
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| creator | Belaïd, Sarah Laurent, Sophie Vermeersch, Marjorie Elst, Luce Vander Perez-Morga, David Muller, Robert N |
| description | A novel way has been proposed to follow the formation of nanocrystalline magnetite. Iron oxide nanoparticles were synthesized by the thermal decomposition of Fe(acac)3 in the presence of oleic acid and oleylamine surfactants at high temperature. The species produced during the synthetic process are characterized through their effects on the proton nuclear magnetic relaxation of the reaction medium and their sizes. As shown by transmission electron microscopy, photon correlation spectroscopy and x-ray diffraction, the diameter of nano-objects increases when the time synthesis is longer. Magnetic properties evaluated by nuclear magnetic resonance (NMRD profiles, T1 and T2 measurements) were correlated with the size parameters. |
| doi_str_mv | 10.1088/0957-4484/24/5/055705 |
| format | Article |
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Iron oxide nanoparticles were synthesized by the thermal decomposition of Fe(acac)3 in the presence of oleic acid and oleylamine surfactants at high temperature. The species produced during the synthetic process are characterized through their effects on the proton nuclear magnetic relaxation of the reaction medium and their sizes. As shown by transmission electron microscopy, photon correlation spectroscopy and x-ray diffraction, the diameter of nano-objects increases when the time synthesis is longer. Magnetic properties evaluated by nuclear magnetic resonance (NMRD profiles, T1 and T2 measurements) were correlated with the size parameters.</description><identifier>ISSN: 0957-4484</identifier><identifier>EISSN: 1361-6528</identifier><identifier>DOI: 10.1088/0957-4484/24/5/055705</identifier><identifier>PMID: 23306107</identifier><identifier>CODEN: NNOTER</identifier><language>eng</language><publisher>Bristol: IOP Publishing</publisher><subject>Chemical synthesis methods ; Cross-disciplinary physics: materials science; rheology ; Diffraction ; Exact sciences and technology ; Ferric Compounds - chemical synthesis ; Ferric Compounds - chemistry ; Iron - analysis ; Iron oxides ; Magnetic properties ; Magnetic Resonance Spectroscopy ; Materials science ; Methods of nanofabrication ; Nanomaterials ; Nanoparticles ; Nanoparticles - chemistry ; Nanoparticles - ultrastructure ; Nanopowders ; Nanoscale materials and structures: fabrication and characterization ; Nanostructure ; Nanotechnology ; Nanotechnology - methods ; Particle Size ; Physics ; Solutions ; Temperature ; Thermal decomposition ; X-Ray Diffraction</subject><ispartof>Nanotechnology, 2013-02, Vol.24 (5), p.055705-055705</ispartof><rights>2013 IOP Publishing Ltd</rights><rights>2014 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c414t-2e36707bb32538c6079e3ffaaf58d9839bebed6861bccfa7f67d57e5387519843</citedby><cites>FETCH-LOGICAL-c414t-2e36707bb32538c6079e3ffaaf58d9839bebed6861bccfa7f67d57e5387519843</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://iopscience.iop.org/article/10.1088/0957-4484/24/5/055705/pdf$$EPDF$$P50$$Giop$$H</linktopdf><link.rule.ids>314,776,780,27901,27902,53821,53868</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=26875791$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/23306107$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Belaïd, Sarah</creatorcontrib><creatorcontrib>Laurent, Sophie</creatorcontrib><creatorcontrib>Vermeersch, Marjorie</creatorcontrib><creatorcontrib>Elst, Luce Vander</creatorcontrib><creatorcontrib>Perez-Morga, David</creatorcontrib><creatorcontrib>Muller, Robert N</creatorcontrib><title>A new approach to follow the formation of iron oxide nanoparticles synthesized by thermal decomposition</title><title>Nanotechnology</title><addtitle>Nano</addtitle><addtitle>Nanotechnology</addtitle><description>A novel way has been proposed to follow the formation of nanocrystalline magnetite. Iron oxide nanoparticles were synthesized by the thermal decomposition of Fe(acac)3 in the presence of oleic acid and oleylamine surfactants at high temperature. The species produced during the synthetic process are characterized through their effects on the proton nuclear magnetic relaxation of the reaction medium and their sizes. As shown by transmission electron microscopy, photon correlation spectroscopy and x-ray diffraction, the diameter of nano-objects increases when the time synthesis is longer. Magnetic properties evaluated by nuclear magnetic resonance (NMRD profiles, T1 and T2 measurements) were correlated with the size parameters.</description><subject>Chemical synthesis methods</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Diffraction</subject><subject>Exact sciences and technology</subject><subject>Ferric Compounds - chemical synthesis</subject><subject>Ferric Compounds - chemistry</subject><subject>Iron - analysis</subject><subject>Iron oxides</subject><subject>Magnetic properties</subject><subject>Magnetic Resonance Spectroscopy</subject><subject>Materials science</subject><subject>Methods of nanofabrication</subject><subject>Nanomaterials</subject><subject>Nanoparticles</subject><subject>Nanoparticles - chemistry</subject><subject>Nanoparticles - ultrastructure</subject><subject>Nanopowders</subject><subject>Nanoscale materials and structures: fabrication and characterization</subject><subject>Nanostructure</subject><subject>Nanotechnology</subject><subject>Nanotechnology - methods</subject><subject>Particle Size</subject><subject>Physics</subject><subject>Solutions</subject><subject>Temperature</subject><subject>Thermal decomposition</subject><subject>X-Ray Diffraction</subject><issn>0957-4484</issn><issn>1361-6528</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqFkU1P3DAQhi3UCra0PwHkS6Ve0vW3nSNC9ENC6qU9W44zBqMkDnZWsP31dbRbOKI5zByedz7eQeiCkq-UGLMlrdSNEEZsmdjKLZFSE3mCNpQr2ijJzDu0eWHO0IdSHgih1DB6is4Y50RRojfo7gpP8ITdPOfk_D1eEg5pGNITXu6hlnl0S0wTTgHHvObn2AOe3JRml5foByi47KcKl_gXetztV2FVDbgHn8Y5lbg2-IjeBzcU-HTM5-jPt5vf1z-a21_ff15f3TZeULE0DLjSRHcdZ5Ibr4hugYfgXJCmbw1vO-igV0bRzvvgdFC6lxoqqyVtjeDn6Muhb73ncQdlsWMsHobBTZB2xVLOahAh6Nso01xxwrisqDygPqdSMgQ75zi6vLeU2PUddrXarlZbJqy0h3dU3eVxxK4boX9R_fe_Ap-PgCveDSG7ycfyyql6l27XXemBi2m2D2mXp2riG8P_AXVZod8</recordid><startdate>20130208</startdate><enddate>20130208</enddate><creator>Belaïd, Sarah</creator><creator>Laurent, Sophie</creator><creator>Vermeersch, Marjorie</creator><creator>Elst, Luce Vander</creator><creator>Perez-Morga, David</creator><creator>Muller, Robert N</creator><general>IOP Publishing</general><general>Institute of Physics</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>F28</scope><scope>FR3</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20130208</creationdate><title>A new approach to follow the formation of iron oxide nanoparticles synthesized by thermal decomposition</title><author>Belaïd, Sarah ; Laurent, Sophie ; Vermeersch, Marjorie ; Elst, Luce Vander ; Perez-Morga, David ; Muller, Robert N</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c414t-2e36707bb32538c6079e3ffaaf58d9839bebed6861bccfa7f67d57e5387519843</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>Chemical synthesis methods</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Diffraction</topic><topic>Exact sciences and technology</topic><topic>Ferric Compounds - chemical synthesis</topic><topic>Ferric Compounds - chemistry</topic><topic>Iron - analysis</topic><topic>Iron oxides</topic><topic>Magnetic properties</topic><topic>Magnetic Resonance Spectroscopy</topic><topic>Materials science</topic><topic>Methods of nanofabrication</topic><topic>Nanomaterials</topic><topic>Nanoparticles</topic><topic>Nanoparticles - chemistry</topic><topic>Nanoparticles - ultrastructure</topic><topic>Nanopowders</topic><topic>Nanoscale materials and structures: fabrication and characterization</topic><topic>Nanostructure</topic><topic>Nanotechnology</topic><topic>Nanotechnology - methods</topic><topic>Particle Size</topic><topic>Physics</topic><topic>Solutions</topic><topic>Temperature</topic><topic>Thermal decomposition</topic><topic>X-Ray Diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Belaïd, Sarah</creatorcontrib><creatorcontrib>Laurent, Sophie</creatorcontrib><creatorcontrib>Vermeersch, Marjorie</creatorcontrib><creatorcontrib>Elst, Luce Vander</creatorcontrib><creatorcontrib>Perez-Morga, David</creatorcontrib><creatorcontrib>Muller, Robert N</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Nanotechnology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Belaïd, Sarah</au><au>Laurent, Sophie</au><au>Vermeersch, Marjorie</au><au>Elst, Luce Vander</au><au>Perez-Morga, David</au><au>Muller, Robert N</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A new approach to follow the formation of iron oxide nanoparticles synthesized by thermal decomposition</atitle><jtitle>Nanotechnology</jtitle><stitle>Nano</stitle><addtitle>Nanotechnology</addtitle><date>2013-02-08</date><risdate>2013</risdate><volume>24</volume><issue>5</issue><spage>055705</spage><epage>055705</epage><pages>055705-055705</pages><issn>0957-4484</issn><eissn>1361-6528</eissn><coden>NNOTER</coden><abstract>A novel way has been proposed to follow the formation of nanocrystalline magnetite. Iron oxide nanoparticles were synthesized by the thermal decomposition of Fe(acac)3 in the presence of oleic acid and oleylamine surfactants at high temperature. The species produced during the synthetic process are characterized through their effects on the proton nuclear magnetic relaxation of the reaction medium and their sizes. As shown by transmission electron microscopy, photon correlation spectroscopy and x-ray diffraction, the diameter of nano-objects increases when the time synthesis is longer. Magnetic properties evaluated by nuclear magnetic resonance (NMRD profiles, T1 and T2 measurements) were correlated with the size parameters.</abstract><cop>Bristol</cop><pub>IOP Publishing</pub><pmid>23306107</pmid><doi>10.1088/0957-4484/24/5/055705</doi><tpages>8</tpages></addata></record> |
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| source | MEDLINE; IOP Publishing Journals; Institute of Physics (IOP) Journals - HEAL-Link |
| subjects | Chemical synthesis methods Cross-disciplinary physics: materials science rheology Diffraction Exact sciences and technology Ferric Compounds - chemical synthesis Ferric Compounds - chemistry Iron - analysis Iron oxides Magnetic properties Magnetic Resonance Spectroscopy Materials science Methods of nanofabrication Nanomaterials Nanoparticles Nanoparticles - chemistry Nanoparticles - ultrastructure Nanopowders Nanoscale materials and structures: fabrication and characterization Nanostructure Nanotechnology Nanotechnology - methods Particle Size Physics Solutions Temperature Thermal decomposition X-Ray Diffraction |
| title | A new approach to follow the formation of iron oxide nanoparticles synthesized by thermal decomposition |
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