Simple Synthesis of Submicrometer Lead Titanate Powder by Precipitation of TiO2 Precursor on PbO Particulates

A simple way to prepare phase‐pure, submicrometer PbTiO3 powder was tried by precipitation. Precipitation was carried out in an aqueous PbO slurry using aqueous TiCl4 and dilute NH4OH at pH 9.5 ± 0.1. The TG/DSC curves of the PT precursor show weight loss of ∼7% and two exotherms at 492° and 522°C....

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Veröffentlicht in:Journal of the American Ceramic Society 2000-04, Vol.83 (4), p.971-973
Hauptverfasser: Han, Kyoung R., Koo, Hee Jin, Hong, Mee-Jeong, Lim, Chang Sup
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Sprache:eng
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