X-ray microdiffraction: local stress distributions in polycrystalline and epitaxial thin films

When investigated by X-ray microdiffraction, the stress states in thin metal films are found to be more complex than as assumed by the simple models that have been formulated to describe their behavior. In this paper, the local differences in stress have been measured in a polycrystalline Al(0.5 wt%...

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Veröffentlicht in:Microelectronic engineering 2004-07, Vol.75 (1), p.117-126
Hauptverfasser: Phillips, M.A, Spolenak, R, Tamura, N, Brown, W.L, MacDowell, A.A, Celestre, R.S, Padmore, H.A, Batterman, B.W, Arzt, E, Patel, J.R
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container_end_page 126
container_issue 1
container_start_page 117
container_title Microelectronic engineering
container_volume 75
creator Phillips, M.A
Spolenak, R
Tamura, N
Brown, W.L
MacDowell, A.A
Celestre, R.S
Padmore, H.A
Batterman, B.W
Arzt, E
Patel, J.R
description When investigated by X-ray microdiffraction, the stress states in thin metal films are found to be more complex than as assumed by the simple models that have been formulated to describe their behavior. In this paper, the local differences in stress have been measured in a polycrystalline Al(0.5 wt% Cu) film on Si and an epitaxial Cu film on Al 2O 3. Significant differences in stress state are apparent between grains, but also within grains. While both types of film display a local variation in residual stress state, the width of the distribution is much broader in the polycrystalline film. The reasons for this are discussed in terms of grain size distribution and dislocation nucleation.
doi_str_mv 10.1016/j.mee.2003.12.053
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source Elsevier ScienceDirect Journals
subjects Al–Cu
Applied sciences
DISLOCATIONS
DISTRIBUTION
Electronics
Exact sciences and technology
GRAIN SIZE
Materials
MATERIALS SCIENCE
Microdiffraction
Microelectronic fabrication (materials and surfaces technology)
NUCLEATION
Plasticity
Semiconductor electronics. Microelectronics. Optoelectronics. Solid state devices
Size effects
Stress measurement
Synchrotron
Testing, measurement, noise and reliability
THIN FILMS
X-RAY MICRODIFFRACTION STRESS ANALYSIS THIN FILM
title X-ray microdiffraction: local stress distributions in polycrystalline and epitaxial thin films
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