YBCO Oxalate Coprecipitation in Alcoholic Solutions

A process for synthesis of ultrafine YBa2Cu3O7–x powder by oxalate coprecipitation from nearly saturated solutions of the metal acetates and a 2‐propanol solution of oxalic acid was developed. The coprecipitation was complete within 5 min in an ice bath at 0–2°C. The final stoichiometry was Y:Ba:Cu...

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Veröffentlicht in:	Journal of the American Ceramic Society 1994-06, Vol.77 (6), p.1436-1440
Hauptverfasser:	Shter, Gennady E., Grader, Gideon S.
Format:	Artikel
Sprache:	eng
Schlagworte:	360201 - Ceramics, Cermets, & Refractories- Preparation & Fabrication 400201 - Chemical & Physicochemical Properties ALKALINE EARTH METAL COMPOUNDS BARIUM COMPOUNDS BARIUM OXIDES CARBOXYLIC ACID SALTS CHALCOGENIDES COPPER COMPOUNDS COPPER OXIDES COPRECIPITATION DATA EXPERIMENTAL DATA HIGH-TC SUPERCONDUCTORS INFORMATION INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY MATERIALS SCIENCE NUMERICAL DATA OXALATES OXIDES OXYGEN COMPOUNDS PRECIPITATION SEPARATION PROCESSES SUPERCONDUCTORS SYNTHESIS TRANSITION ELEMENT COMPOUNDS YTTRIUM COMPOUNDS YTTRIUM OXIDES
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