Laser-Induced Plasma as a Method for the Metallic Materials Hardness Estimation: An Alternative Approach

The application of an alternative laser-induced breakdown spectroscopy (LIBS) method based on transversely excited atmospheric (TEA) CO 2 laser was investigated for the first time for estimating the hardness of metallic materials. The human eye-safe (TEA) CO 2 laser, operating at 10.6 µm, was used f...

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Veröffentlicht in:Plasma chemistry and plasma processing 2020-03, Vol.40 (2), p.499-510
Hauptverfasser: Momcilovic, Milos, Petrovic, Jelena, Ciganovic, Jovan, Cvijovic-Alagic, Ivana, Koldzic, Filip, Zivkovic, Sanja
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container_end_page 510
container_issue 2
container_start_page 499
container_title Plasma chemistry and plasma processing
container_volume 40
creator Momcilovic, Milos
Petrovic, Jelena
Ciganovic, Jovan
Cvijovic-Alagic, Ivana
Koldzic, Filip
Zivkovic, Sanja
description The application of an alternative laser-induced breakdown spectroscopy (LIBS) method based on transversely excited atmospheric (TEA) CO 2 laser was investigated for the first time for estimating the hardness of metallic materials. The human eye-safe (TEA) CO 2 laser, operating at 10.6 µm, was used for plasma generation. The LIBS spectra were recorded by employing a cost-effective CCD camera for the time-integrated and spatial resolved measurements. The cast iron and aluminum alloys samples with different hardness have been tested. The ratio between the magnesium ionic and neutral lines in LIBS spectra was applied for estimating the material hardness. In addition, the hardness of all samples included in this study was determined using the conventional method for material hardness determination, i.e. Vickers hardness test. The linear dependence of magnesium lines intensity ratio on the sample’s hardness was obtained for both kinds of materials. Profilometric measurements were used to verify that the newly-introduced method is almost nondestructive for the investigated metals. The results obtained in the present work confirmed the potential of using this original LIBS system not only for the fast elemental analysis but also for the direct estimation of the hardness of metals and alloys.
doi_str_mv 10.1007/s11090-020-10063-5
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subjects 60 APPLIED LIFE SCIENCES
Alloy cast iron
ALUMINIUM ALLOYS
Aluminum base alloys
Carbon dioxide
CARBON DIOXIDE LASERS
CAST IRON
CCD cameras
Characterization and Evaluation of Materials
CHARGE-COUPLED DEVICES
Chemistry
Chemistry and Materials Science
Classical Mechanics
Diamond pyramid hardness tests
Estimation
Inorganic Chemistry
Laser induced breakdown spectroscopy
Laser plasmas
Lasers
Line spectra
MAGNESIUM
MATERIALS
MATERIALS SCIENCE
Mechanical Engineering
Nondestructive testing
Original Paper
PLASMA
Spectrum analysis
VICKERS HARDNESS
title Laser-Induced Plasma as a Method for the Metallic Materials Hardness Estimation: An Alternative Approach
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