Structural and Magnetic Properties Study of Fe{sub 50}Si{sub 50} Powders with Different Microparticle Sizes
The structural properties and magnetic behavior of the Fe{sub 50}Si{sub 50} system were determined using X-ray diffraction (XRD), Mössbauer spectrometry (MS), vibration sample magnetometry (VSM), and scanning electron microscopy (SEM). Samples of Fe{sub 50}Si{sub 50} were melted using an arc furnace...
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| Veröffentlicht in: | Journal of superconductivity and novel magnetism 2019-05, Vol.32 (5) |
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| container_title | Journal of superconductivity and novel magnetism |
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| creator | Perdomo, J. F. González Hernandez, J. S. Trujillo Lozano, D. Oyola Martínez, Y. A. Rojas Alcázar, G. A. Pérez Rodriguez, H. Bustos |
| description | The structural properties and magnetic behavior of the Fe{sub 50}Si{sub 50} system were determined using X-ray diffraction (XRD), Mössbauer spectrometry (MS), vibration sample magnetometry (VSM), and scanning electron microscopy (SEM). Samples of Fe{sub 50}Si{sub 50} were melted using an arc furnace, then powder was obtained through a diamond file, and this was passed through different sieves. Finally, nanoparticles of this system were produced by means of surfactant-assisted mechanical alloying. XRD confirmed the presence of the FeSi (CS) and Fe{sub 5}Si{sub 3} structural phases. By transmission MS, it was observed that at room temperature the spectrum is formed by three general components, a doublet associated with the FeSi (CS) phase and two sextets associated with the Fe{sub 5}Si{sub 3} phase; this gives the idea of the distribution of the sizes of particles present in the sample. By VSM, the soft magnetic behavior of the system was ratified and it was determined that the biggest saturation magnetization corresponds to the smallest particles. |
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By transmission MS, it was observed that at room temperature the spectrum is formed by three general components, a doublet associated with the FeSi (CS) phase and two sextets associated with the Fe{sub 5}Si{sub 3} phase; this gives the idea of the distribution of the sizes of particles present in the sample. 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XRD confirmed the presence of the FeSi (CS) and Fe{sub 5}Si{sub 3} structural phases. By transmission MS, it was observed that at room temperature the spectrum is formed by three general components, a doublet associated with the FeSi (CS) phase and two sextets associated with the Fe{sub 5}Si{sub 3} phase; this gives the idea of the distribution of the sizes of particles present in the sample. 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By transmission MS, it was observed that at room temperature the spectrum is formed by three general components, a doublet associated with the FeSi (CS) phase and two sextets associated with the Fe{sub 5}Si{sub 3} phase; this gives the idea of the distribution of the sizes of particles present in the sample. By VSM, the soft magnetic behavior of the system was ratified and it was determined that the biggest saturation magnetization corresponds to the smallest particles.</abstract><cop>United States</cop></addata></record> |
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| subjects | IRON SILICIDES MAGNETIC MATERIALS MAGNETIC PROPERTIES MAGNETIZATION MOESSBAUER SPECTROMETERS NANOPARTICLES NANOSCIENCE AND NANOTECHNOLOGY SATURATION SCANNING ELECTRON MICROSCOPY SPECTRA SPECTROSCOPY VIBRATING SAMPLE MAGNETOMETERS X-RAY DIFFRACTION |
| title | Structural and Magnetic Properties Study of Fe{sub 50}Si{sub 50} Powders with Different Microparticle Sizes |
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