Effect of borides on hot deformation behavior and microstructure evolution of powder metallurgy high borated stainless steel

To investigate borides effect on the hot deformation behavior and microstructure evolution of powder metallurgy high borated stainless steel, hot compression tests at the temperatures of 950–1150°C and the strain rates of 0.01–10s−1 were performed. Flow stress curves indicated that borides increased...

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Veröffentlicht in:Materials characterization 2017-02, Vol.124, p.182-191
Hauptverfasser: Zhou, Xuan, Wang, Mingjia, Fu, Yifeng, Wang, Zixi, Li, Yanmei, Yang, Shunkai, Zhao, Hongchang, Li, Hangbo
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container_end_page 191
container_issue
container_start_page 182
container_title Materials characterization
container_volume 124
creator Zhou, Xuan
Wang, Mingjia
Fu, Yifeng
Wang, Zixi
Li, Yanmei
Yang, Shunkai
Zhao, Hongchang
Li, Hangbo
description To investigate borides effect on the hot deformation behavior and microstructure evolution of powder metallurgy high borated stainless steel, hot compression tests at the temperatures of 950–1150°C and the strain rates of 0.01–10s−1 were performed. Flow stress curves indicated that borides increased the material's stress level at low temperature but the strength was sacrificed at temperatures above 1100°C. A hyperbolic-sine equation was used to characterize the dependence of the flow stress on the deformation temperature and strain rate. The hot deformation activation energy and stress exponent were determined to be 355kJ/mol and 3.2, respectively. The main factors leading to activation energy and stress exponent of studied steel lower than those of commercial 304 stainless steel were discussed. Processing maps at the strains of 0.1, 0.3, 0.5, and 0.7 showed that flow instability mainly concentrated at 950–1150°C and strain rate higher than 0.6s−1. Results of microstructure illustrated that dynamic recrystallization was fully completed at both high temperature-low strain rate and low temperature-high strain rate. In the instability region cracks were generated in addition to cavities. Interestingly, borides maintained a preferential orientation resulting from particle rotation during compression. [Display omitted] •The decrement of activation energy was affected by boride and boron solution.•The decrease of stress exponent was influenced by composition and Cottrell atmosphere.•Boride represented a preferential orientation caused by particle rotation.
doi_str_mv 10.1016/j.matchar.2017.01.001
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Flow stress curves indicated that borides increased the material's stress level at low temperature but the strength was sacrificed at temperatures above 1100°C. A hyperbolic-sine equation was used to characterize the dependence of the flow stress on the deformation temperature and strain rate. The hot deformation activation energy and stress exponent were determined to be 355kJ/mol and 3.2, respectively. The main factors leading to activation energy and stress exponent of studied steel lower than those of commercial 304 stainless steel were discussed. Processing maps at the strains of 0.1, 0.3, 0.5, and 0.7 showed that flow instability mainly concentrated at 950–1150°C and strain rate higher than 0.6s−1. Results of microstructure illustrated that dynamic recrystallization was fully completed at both high temperature-low strain rate and low temperature-high strain rate. In the instability region cracks were generated in addition to cavities. Interestingly, borides maintained a preferential orientation resulting from particle rotation during compression. 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Flow stress curves indicated that borides increased the material's stress level at low temperature but the strength was sacrificed at temperatures above 1100°C. A hyperbolic-sine equation was used to characterize the dependence of the flow stress on the deformation temperature and strain rate. The hot deformation activation energy and stress exponent were determined to be 355kJ/mol and 3.2, respectively. The main factors leading to activation energy and stress exponent of studied steel lower than those of commercial 304 stainless steel were discussed. Processing maps at the strains of 0.1, 0.3, 0.5, and 0.7 showed that flow instability mainly concentrated at 950–1150°C and strain rate higher than 0.6s−1. Results of microstructure illustrated that dynamic recrystallization was fully completed at both high temperature-low strain rate and low temperature-high strain rate. In the instability region cracks were generated in addition to cavities. Interestingly, borides maintained a preferential orientation resulting from particle rotation during compression. 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Interestingly, borides maintained a preferential orientation resulting from particle rotation during compression. [Display omitted] •The decrement of activation energy was affected by boride and boron solution.•The decrease of stress exponent was influenced by composition and Cottrell atmosphere.•Boride represented a preferential orientation caused by particle rotation.</abstract><cop>United States</cop><pub>Elsevier Inc</pub><doi>10.1016/j.matchar.2017.01.001</doi><tpages>10</tpages><orcidid>https://orcid.org/0000-0002-9353-0689</orcidid></addata></record>
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subjects ACTIVATION ENERGY
Borated stainless steel
BORATES
Boride
BORIDES
BORON
COMPRESSION
DEFORMATION
Deformation behavior
DIAGRAMS
FLOW STRESS
MATERIALS SCIENCE
MICROSTRUCTURE
POWDER METALLURGY
POWDERS
RECRYSTALLIZATION
ROTATION
STAINLESS STEEL-304
STRAIN RATE
STRAINS
TEMPERATURE RANGE 0400-1000 K
TEMPERATURE RANGE 1000-4000 K
title Effect of borides on hot deformation behavior and microstructure evolution of powder metallurgy high borated stainless steel
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