In situ investigation of the tensile deformation of laser welded Ti{sub 2}AlNb joints
The tensile deformation behavior of laser welded Ti{sub 2}AlNb joints was investigated using in situ analysis methods. The fracture mode of the single-B2-phase fusion zone was quasi-cleavage at room temperature and intergranular at 650 °C, while that of base metal was microvoid coalescence at both r...
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creator | Zhang, Kezhao Ni, Longchang Lei, Zhenglong, E-ma |
description | The tensile deformation behavior of laser welded Ti{sub 2}AlNb joints was investigated using in situ analysis methods. The fracture mode of the single-B2-phase fusion zone was quasi-cleavage at room temperature and intergranular at 650 °C, while that of base metal was microvoid coalescence at both room temperature and 650 °C. Tensile deformation at room temperature was observed using in situ SEM tensile testing. In base metal, microcracks nucleated and propagated mainly within the O phase or along O/B2 phase boundaries. While both the cross- and multi-slips were found in the single-B2-phase fusion zone, a confocal laser scanning microscopy was used to observe the crack initiation and propagation process in situ at 650 °C. Cracks mainly formed along the B2/O phase boundaries in base metal, along the fragile grain boundaries of B2 phase in the fusion zone. The thermal simulation experiment and following TEM analysis indicated that the precipitation of continuous O-phase films along the B2 grain boundaries resulted in the high temperature brittleness of laser welded Ti{sub 2}AlNb joints. - Highlights: •Cracks formed within O phase or along B2/O boundaries in the base metal. •Cross- and multi-slips relieved stress in the fusion zone at room temperature. •Cracks mainly formed along the B2/O boundaries at 650 °C. •In the fusion zone, intergranular cracks were in situ observed at 650 °C. •O-phase films along B2 grain boundaries caused the high temperature brittleness. |
doi_str_mv | 10.1016/J.MATCHAR.2016.11.009 |
format | Article |
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The fracture mode of the single-B2-phase fusion zone was quasi-cleavage at room temperature and intergranular at 650 °C, while that of base metal was microvoid coalescence at both room temperature and 650 °C. Tensile deformation at room temperature was observed using in situ SEM tensile testing. In base metal, microcracks nucleated and propagated mainly within the O phase or along O/B2 phase boundaries. While both the cross- and multi-slips were found in the single-B2-phase fusion zone, a confocal laser scanning microscopy was used to observe the crack initiation and propagation process in situ at 650 °C. Cracks mainly formed along the B2/O phase boundaries in base metal, along the fragile grain boundaries of B2 phase in the fusion zone. The thermal simulation experiment and following TEM analysis indicated that the precipitation of continuous O-phase films along the B2 grain boundaries resulted in the high temperature brittleness of laser welded Ti{sub 2}AlNb joints. - Highlights: •Cracks formed within O phase or along B2/O boundaries in the base metal. •Cross- and multi-slips relieved stress in the fusion zone at room temperature. •Cracks mainly formed along the B2/O boundaries at 650 °C. •In the fusion zone, intergranular cracks were in situ observed at 650 °C. •O-phase films along B2 grain boundaries caused the high temperature brittleness.</description><identifier>ISSN: 1044-5803</identifier><identifier>EISSN: 1873-4189</identifier><identifier>DOI: 10.1016/J.MATCHAR.2016.11.009</identifier><language>eng</language><publisher>United States</publisher><subject>BRITTLENESS ; CLEAVAGE ; CRACK PROPAGATION ; CRACKS ; DEFORMATION ; FRACTURES ; GRAIN BOUNDARIES ; LASER WELDING ; MATERIALS SCIENCE ; METALS ; PHASE TRANSFORMATIONS ; PRECIPITATION ; SCANNING ELECTRON MICROSCOPY ; SLIP ; STRESSES ; TEMPERATURE RANGE 0273-0400 K ; TEMPERATURE RANGE 0400-1000 K ; TITANIUM BASE ALLOYS ; TRANSMISSION ELECTRON MICROSCOPY ; WELDED JOINTS</subject><ispartof>Materials characterization, 2017-01, Vol.123</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>230,314,777,781,882,27905,27906</link.rule.ids><backlink>$$Uhttps://www.osti.gov/biblio/22689681$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Zhang, Kezhao</creatorcontrib><creatorcontrib>Ni, Longchang</creatorcontrib><creatorcontrib>Lei, Zhenglong, E-ma</creatorcontrib><title>In situ investigation of the tensile deformation of laser welded Ti{sub 2}AlNb joints</title><title>Materials characterization</title><description>The tensile deformation behavior of laser welded Ti{sub 2}AlNb joints was investigated using in situ analysis methods. The fracture mode of the single-B2-phase fusion zone was quasi-cleavage at room temperature and intergranular at 650 °C, while that of base metal was microvoid coalescence at both room temperature and 650 °C. Tensile deformation at room temperature was observed using in situ SEM tensile testing. In base metal, microcracks nucleated and propagated mainly within the O phase or along O/B2 phase boundaries. While both the cross- and multi-slips were found in the single-B2-phase fusion zone, a confocal laser scanning microscopy was used to observe the crack initiation and propagation process in situ at 650 °C. Cracks mainly formed along the B2/O phase boundaries in base metal, along the fragile grain boundaries of B2 phase in the fusion zone. The thermal simulation experiment and following TEM analysis indicated that the precipitation of continuous O-phase films along the B2 grain boundaries resulted in the high temperature brittleness of laser welded Ti{sub 2}AlNb joints. - Highlights: •Cracks formed within O phase or along B2/O boundaries in the base metal. •Cross- and multi-slips relieved stress in the fusion zone at room temperature. •Cracks mainly formed along the B2/O boundaries at 650 °C. •In the fusion zone, intergranular cracks were in situ observed at 650 °C. •O-phase films along B2 grain boundaries caused the high temperature brittleness.</description><subject>BRITTLENESS</subject><subject>CLEAVAGE</subject><subject>CRACK PROPAGATION</subject><subject>CRACKS</subject><subject>DEFORMATION</subject><subject>FRACTURES</subject><subject>GRAIN BOUNDARIES</subject><subject>LASER WELDING</subject><subject>MATERIALS SCIENCE</subject><subject>METALS</subject><subject>PHASE TRANSFORMATIONS</subject><subject>PRECIPITATION</subject><subject>SCANNING ELECTRON MICROSCOPY</subject><subject>SLIP</subject><subject>STRESSES</subject><subject>TEMPERATURE RANGE 0273-0400 K</subject><subject>TEMPERATURE RANGE 0400-1000 K</subject><subject>TITANIUM BASE ALLOYS</subject><subject>TRANSMISSION ELECTRON MICROSCOPY</subject><subject>WELDED JOINTS</subject><issn>1044-5803</issn><issn>1873-4189</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><recordid>eNqNjk9rwkAUxJdSof7pRxAe9Jzt2ySNm2MoFVuoB4lnicmLrmx3wbe2B_G7uwfx3NPMMAPzE2KqUCpUxeuX_K7q90W1kmmMUimJWD6IodKzLMmVLh-jxzxP3jRmT2LEfEDEQqvZUKw_HbAJJzDulziYXROMd-B7CHuCQI6NJeio98efe2UbpiP8ke2og9qc-bSF9FLZ5RYO3rjAEzHoG8v0fNOxeJl_RMTEx4sNtyZQu2-9c9SGTZoWuow02f9WV7tYSP0</recordid><startdate>20170115</startdate><enddate>20170115</enddate><creator>Zhang, Kezhao</creator><creator>Ni, Longchang</creator><creator>Lei, Zhenglong, E-ma</creator><scope>OTOTI</scope></search><sort><creationdate>20170115</creationdate><title>In situ investigation of the tensile deformation of laser welded Ti{sub 2}AlNb joints</title><author>Zhang, Kezhao ; Ni, Longchang ; Lei, Zhenglong, E-ma</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-osti_scitechconnect_226896813</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>BRITTLENESS</topic><topic>CLEAVAGE</topic><topic>CRACK PROPAGATION</topic><topic>CRACKS</topic><topic>DEFORMATION</topic><topic>FRACTURES</topic><topic>GRAIN BOUNDARIES</topic><topic>LASER WELDING</topic><topic>MATERIALS SCIENCE</topic><topic>METALS</topic><topic>PHASE TRANSFORMATIONS</topic><topic>PRECIPITATION</topic><topic>SCANNING ELECTRON MICROSCOPY</topic><topic>SLIP</topic><topic>STRESSES</topic><topic>TEMPERATURE RANGE 0273-0400 K</topic><topic>TEMPERATURE RANGE 0400-1000 K</topic><topic>TITANIUM BASE ALLOYS</topic><topic>TRANSMISSION ELECTRON MICROSCOPY</topic><topic>WELDED JOINTS</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Zhang, Kezhao</creatorcontrib><creatorcontrib>Ni, Longchang</creatorcontrib><creatorcontrib>Lei, Zhenglong, E-ma</creatorcontrib><collection>OSTI.GOV</collection><jtitle>Materials characterization</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Zhang, Kezhao</au><au>Ni, Longchang</au><au>Lei, Zhenglong, E-ma</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>In situ investigation of the tensile deformation of laser welded Ti{sub 2}AlNb joints</atitle><jtitle>Materials characterization</jtitle><date>2017-01-15</date><risdate>2017</risdate><volume>123</volume><issn>1044-5803</issn><eissn>1873-4189</eissn><abstract>The tensile deformation behavior of laser welded Ti{sub 2}AlNb joints was investigated using in situ analysis methods. The fracture mode of the single-B2-phase fusion zone was quasi-cleavage at room temperature and intergranular at 650 °C, while that of base metal was microvoid coalescence at both room temperature and 650 °C. Tensile deformation at room temperature was observed using in situ SEM tensile testing. In base metal, microcracks nucleated and propagated mainly within the O phase or along O/B2 phase boundaries. While both the cross- and multi-slips were found in the single-B2-phase fusion zone, a confocal laser scanning microscopy was used to observe the crack initiation and propagation process in situ at 650 °C. Cracks mainly formed along the B2/O phase boundaries in base metal, along the fragile grain boundaries of B2 phase in the fusion zone. The thermal simulation experiment and following TEM analysis indicated that the precipitation of continuous O-phase films along the B2 grain boundaries resulted in the high temperature brittleness of laser welded Ti{sub 2}AlNb joints. - Highlights: •Cracks formed within O phase or along B2/O boundaries in the base metal. •Cross- and multi-slips relieved stress in the fusion zone at room temperature. •Cracks mainly formed along the B2/O boundaries at 650 °C. •In the fusion zone, intergranular cracks were in situ observed at 650 °C. •O-phase films along B2 grain boundaries caused the high temperature brittleness.</abstract><cop>United States</cop><doi>10.1016/J.MATCHAR.2016.11.009</doi></addata></record> |
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subjects | BRITTLENESS CLEAVAGE CRACK PROPAGATION CRACKS DEFORMATION FRACTURES GRAIN BOUNDARIES LASER WELDING MATERIALS SCIENCE METALS PHASE TRANSFORMATIONS PRECIPITATION SCANNING ELECTRON MICROSCOPY SLIP STRESSES TEMPERATURE RANGE 0273-0400 K TEMPERATURE RANGE 0400-1000 K TITANIUM BASE ALLOYS TRANSMISSION ELECTRON MICROSCOPY WELDED JOINTS |
title | In situ investigation of the tensile deformation of laser welded Ti{sub 2}AlNb joints |
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