A 31 T split-pair pulsed magnet for single crystal x-ray diffraction at low temperature

We have developed a pulsed magnet system with panoramic access for synchrotron x-ray diffraction in magnetic fields up to 31 T and at low temperature down to 1.5 K. The apparatus consists of a split-pair magnet, a liquid nitrogen bath to cool the pulsed coil, and a helium cryostat allowing sample te...

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Veröffentlicht in:Review of scientific instruments 2014-05, Vol.85 (5), p.053905-053905
Hauptverfasser: Duc, F, Fabrèges, X, Roth, T, Detlefs, C, Frings, P, Nardone, M, Billette, J, Lesourd, M, Zhang, L, Zitouni, A, Delescluse, P, Béard, J, Nicolin, J P, Rikken, G L J A
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Sprache:eng
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Zusammenfassung:We have developed a pulsed magnet system with panoramic access for synchrotron x-ray diffraction in magnetic fields up to 31 T and at low temperature down to 1.5 K. The apparatus consists of a split-pair magnet, a liquid nitrogen bath to cool the pulsed coil, and a helium cryostat allowing sample temperatures from 1.5 up to 250 K. Using a 1.15 MJ mobile generator, magnetic field pulses of 60 ms length were generated in the magnet, with a rise time of 16.5 ms and a repetition rate of 2 pulses/h at 31 T. The setup was validated for single crystal diffraction on the ESRF beamline ID06.
ISSN:0034-6748
1089-7623
DOI:10.1063/1.4878915