Biomimetic synthesis of hierarchical crystalline hydroxyapatite fibers in large-scale
[Display omitted] ► Crystalline hierarchical hydroxyapatite (HAp) fibers are synthesized. ► We employ a biomimetic route by using cotton cloth as a natural bio-template. ► We study the effects of pH, ultrasonic cleaning time, and calcination temperature. ► We obtain an optimized reaction condition....
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| Veröffentlicht in: | Materials research bulletin 2012-06, Vol.47 (6), p.1572-1576 |
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| container_issue | 6 |
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| container_title | Materials research bulletin |
| container_volume | 47 |
| creator | Xing, Chaogang Ge, Suxiang Huang, Baojun Bo, Yingying Zhang, Di Zheng, Zhi |
| description | [Display omitted]
► Crystalline hierarchical hydroxyapatite (HAp) fibers are synthesized. ► We employ a biomimetic route by using cotton cloth as a natural bio-template. ► We study the effects of pH, ultrasonic cleaning time, and calcination temperature. ► We obtain an optimized reaction condition. ► This is a low cost method for production of hierarchical HAp fibers.
Crystalline hierarchical hydroxyapatite [Ca10(PO4)6(OH)2, HAp)] fibers were successfully synthesized via a biomimetic route by using cotton cloth as a natural bio-template. The effects of pH value, aging time, ultrasonic cleaning time, and calcination temperature on the purity and morphology of the resulting hydroxyapatite (HAp) were monitored by scanning election microscope (SEM), X-ray diffraction (XRD), and infrared spectrophotometer (IR) to obtain an optimized reaction condition, namely, pH 9, ultrasonic cleaning for 1min, aging for 24h, and calcination at 600°C for 4h. We found that the natural cellulose could not only control the morphology of HAp but also lower its phase transformation temperature. The impact of this method lies in its low cost and successful production of large-scale patterning of three-dimensional hierarchical HAp fibers. |
| doi_str_mv | 10.1016/j.materresbull.2012.02.018 |
| format | Article |
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► Crystalline hierarchical hydroxyapatite (HAp) fibers are synthesized. ► We employ a biomimetic route by using cotton cloth as a natural bio-template. ► We study the effects of pH, ultrasonic cleaning time, and calcination temperature. ► We obtain an optimized reaction condition. ► This is a low cost method for production of hierarchical HAp fibers.
Crystalline hierarchical hydroxyapatite [Ca10(PO4)6(OH)2, HAp)] fibers were successfully synthesized via a biomimetic route by using cotton cloth as a natural bio-template. The effects of pH value, aging time, ultrasonic cleaning time, and calcination temperature on the purity and morphology of the resulting hydroxyapatite (HAp) were monitored by scanning election microscope (SEM), X-ray diffraction (XRD), and infrared spectrophotometer (IR) to obtain an optimized reaction condition, namely, pH 9, ultrasonic cleaning for 1min, aging for 24h, and calcination at 600°C for 4h. We found that the natural cellulose could not only control the morphology of HAp but also lower its phase transformation temperature. The impact of this method lies in its low cost and successful production of large-scale patterning of three-dimensional hierarchical HAp fibers.</description><identifier>ISSN: 0025-5408</identifier><identifier>EISSN: 1873-4227</identifier><identifier>DOI: 10.1016/j.materresbull.2012.02.018</identifier><language>eng</language><publisher>United States: Elsevier Ltd</publisher><subject>A. Inorganic compounds ; A. Structural materials ; APATITES ; B. Crystal growth ; BUILDING MATERIALS ; C. X-ray diffraction ; CALCINATION ; CRYSTAL GROWTH ; D. Microstructure ; FIBERS ; INORGANIC COMPOUNDS ; MATERIALS SCIENCE ; MICROSTRUCTURE ; PHASE TRANSFORMATIONS ; SCANNING ELECTRON MICROSCOPY ; SYNTHESIS ; X-RAY DIFFRACTION</subject><ispartof>Materials research bulletin, 2012-06, Vol.47 (6), p.1572-1576</ispartof><rights>2012 Elsevier Ltd</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c352t-cc7c54417182110482e2cbae27fbc98e7bf2345179cedceedddffaa7699f298e3</citedby><cites>FETCH-LOGICAL-c352t-cc7c54417182110482e2cbae27fbc98e7bf2345179cedceedddffaa7699f298e3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0025540812000724$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>230,314,776,780,881,3537,27901,27902,65534</link.rule.ids><backlink>$$Uhttps://www.osti.gov/biblio/22215128$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Xing, Chaogang</creatorcontrib><creatorcontrib>Ge, Suxiang</creatorcontrib><creatorcontrib>Huang, Baojun</creatorcontrib><creatorcontrib>Bo, Yingying</creatorcontrib><creatorcontrib>Zhang, Di</creatorcontrib><creatorcontrib>Zheng, Zhi</creatorcontrib><title>Biomimetic synthesis of hierarchical crystalline hydroxyapatite fibers in large-scale</title><title>Materials research bulletin</title><description>[Display omitted]
► Crystalline hierarchical hydroxyapatite (HAp) fibers are synthesized. ► We employ a biomimetic route by using cotton cloth as a natural bio-template. ► We study the effects of pH, ultrasonic cleaning time, and calcination temperature. ► We obtain an optimized reaction condition. ► This is a low cost method for production of hierarchical HAp fibers.
Crystalline hierarchical hydroxyapatite [Ca10(PO4)6(OH)2, HAp)] fibers were successfully synthesized via a biomimetic route by using cotton cloth as a natural bio-template. The effects of pH value, aging time, ultrasonic cleaning time, and calcination temperature on the purity and morphology of the resulting hydroxyapatite (HAp) were monitored by scanning election microscope (SEM), X-ray diffraction (XRD), and infrared spectrophotometer (IR) to obtain an optimized reaction condition, namely, pH 9, ultrasonic cleaning for 1min, aging for 24h, and calcination at 600°C for 4h. We found that the natural cellulose could not only control the morphology of HAp but also lower its phase transformation temperature. The impact of this method lies in its low cost and successful production of large-scale patterning of three-dimensional hierarchical HAp fibers.</description><subject>A. Inorganic compounds</subject><subject>A. Structural materials</subject><subject>APATITES</subject><subject>B. Crystal growth</subject><subject>BUILDING MATERIALS</subject><subject>C. X-ray diffraction</subject><subject>CALCINATION</subject><subject>CRYSTAL GROWTH</subject><subject>D. Microstructure</subject><subject>FIBERS</subject><subject>INORGANIC COMPOUNDS</subject><subject>MATERIALS SCIENCE</subject><subject>MICROSTRUCTURE</subject><subject>PHASE TRANSFORMATIONS</subject><subject>SCANNING ELECTRON MICROSCOPY</subject><subject>SYNTHESIS</subject><subject>X-RAY DIFFRACTION</subject><issn>0025-5408</issn><issn>1873-4227</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><recordid>eNqNUEtLxDAQDqLguvofip67JtN203rzrbDgxT2HdDqxWfpYkij235uyHjwKA3OY7zUfY5eCrwQX6-vdqteBnCNff3bdCriAFY8jyiO2EKXM0hxAHrMF51CkRc7LU3bm_Y5znpdSLtj2zo697SlYTPw0hJa89cloktaS0w5bi7pL0E0-6K6zAyXt1Ljxe9J7HWygxNianE_skHTafVDqI57O2YnRnaeL371k26fH9_uXdPP2_Hp_u0kxKyCkiBKLPBdSlCBETAQEWGsCaWqsSpK1gSwvhKyQGiRqmsYYreW6qgzEe7ZkVwfd0QerPMZA2OI4DIRBAYAoBJQRdXNAoRu9d2TU3tleu0kJruYa1U79rVHNNSoeR8zkhwOZ4h9fsZTZhoYYyLrZpRntf2R-AH2ohXY</recordid><startdate>20120601</startdate><enddate>20120601</enddate><creator>Xing, Chaogang</creator><creator>Ge, Suxiang</creator><creator>Huang, Baojun</creator><creator>Bo, Yingying</creator><creator>Zhang, Di</creator><creator>Zheng, Zhi</creator><general>Elsevier Ltd</general><scope>AAYXX</scope><scope>CITATION</scope><scope>OTOTI</scope></search><sort><creationdate>20120601</creationdate><title>Biomimetic synthesis of hierarchical crystalline hydroxyapatite fibers in large-scale</title><author>Xing, Chaogang ; Ge, Suxiang ; Huang, Baojun ; Bo, Yingying ; Zhang, Di ; Zheng, Zhi</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c352t-cc7c54417182110482e2cbae27fbc98e7bf2345179cedceedddffaa7699f298e3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>A. Inorganic compounds</topic><topic>A. Structural materials</topic><topic>APATITES</topic><topic>B. Crystal growth</topic><topic>BUILDING MATERIALS</topic><topic>C. X-ray diffraction</topic><topic>CALCINATION</topic><topic>CRYSTAL GROWTH</topic><topic>D. Microstructure</topic><topic>FIBERS</topic><topic>INORGANIC COMPOUNDS</topic><topic>MATERIALS SCIENCE</topic><topic>MICROSTRUCTURE</topic><topic>PHASE TRANSFORMATIONS</topic><topic>SCANNING ELECTRON MICROSCOPY</topic><topic>SYNTHESIS</topic><topic>X-RAY DIFFRACTION</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Xing, Chaogang</creatorcontrib><creatorcontrib>Ge, Suxiang</creatorcontrib><creatorcontrib>Huang, Baojun</creatorcontrib><creatorcontrib>Bo, Yingying</creatorcontrib><creatorcontrib>Zhang, Di</creatorcontrib><creatorcontrib>Zheng, Zhi</creatorcontrib><collection>CrossRef</collection><collection>OSTI.GOV</collection><jtitle>Materials research bulletin</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Xing, Chaogang</au><au>Ge, Suxiang</au><au>Huang, Baojun</au><au>Bo, Yingying</au><au>Zhang, Di</au><au>Zheng, Zhi</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Biomimetic synthesis of hierarchical crystalline hydroxyapatite fibers in large-scale</atitle><jtitle>Materials research bulletin</jtitle><date>2012-06-01</date><risdate>2012</risdate><volume>47</volume><issue>6</issue><spage>1572</spage><epage>1576</epage><pages>1572-1576</pages><issn>0025-5408</issn><eissn>1873-4227</eissn><abstract>[Display omitted]
► Crystalline hierarchical hydroxyapatite (HAp) fibers are synthesized. ► We employ a biomimetic route by using cotton cloth as a natural bio-template. ► We study the effects of pH, ultrasonic cleaning time, and calcination temperature. ► We obtain an optimized reaction condition. ► This is a low cost method for production of hierarchical HAp fibers.
Crystalline hierarchical hydroxyapatite [Ca10(PO4)6(OH)2, HAp)] fibers were successfully synthesized via a biomimetic route by using cotton cloth as a natural bio-template. The effects of pH value, aging time, ultrasonic cleaning time, and calcination temperature on the purity and morphology of the resulting hydroxyapatite (HAp) were monitored by scanning election microscope (SEM), X-ray diffraction (XRD), and infrared spectrophotometer (IR) to obtain an optimized reaction condition, namely, pH 9, ultrasonic cleaning for 1min, aging for 24h, and calcination at 600°C for 4h. We found that the natural cellulose could not only control the morphology of HAp but also lower its phase transformation temperature. The impact of this method lies in its low cost and successful production of large-scale patterning of three-dimensional hierarchical HAp fibers.</abstract><cop>United States</cop><pub>Elsevier Ltd</pub><doi>10.1016/j.materresbull.2012.02.018</doi><tpages>5</tpages></addata></record> |
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| subjects | A. Inorganic compounds A. Structural materials APATITES B. Crystal growth BUILDING MATERIALS C. X-ray diffraction CALCINATION CRYSTAL GROWTH D. Microstructure FIBERS INORGANIC COMPOUNDS MATERIALS SCIENCE MICROSTRUCTURE PHASE TRANSFORMATIONS SCANNING ELECTRON MICROSCOPY SYNTHESIS X-RAY DIFFRACTION |
| title | Biomimetic synthesis of hierarchical crystalline hydroxyapatite fibers in large-scale |
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