Hydrothermal synthesis of nanostructured zinc oxide and study of their optical properties
[Display omitted] ► Nanostructured ZnO were successfully obtained by a hydrothermal route. ► Inorganic precursor and molar ratio are key factors for morphology and particle size. ► Optical properties were also studied. Nanostructured ZnO (nanorods, nanoshuttles) have been synthesized by hydrothermal...
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| Veröffentlicht in: | Materials research bulletin 2012-03, Vol.47 (3), p.667-671 |
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| container_title | Materials research bulletin |
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| creator | Moulahi, A. Sediri, F. Gharbi, N. |
| description | [Display omitted]
► Nanostructured ZnO were successfully obtained by a hydrothermal route. ► Inorganic precursor and molar ratio are key factors for morphology and particle size. ► Optical properties were also studied.
Nanostructured ZnO (nanorods, nanoshuttles) have been synthesized by hydrothermal approach using ZnCl2 or Zn(NO3)2·6H2O as zinc sources and cetyltrimethylammonium bromide as structure-directing agent. Techniques X-ray powder diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), UV–visible absorption, Fourier transform infrared spectroscopy (FTIR) and Raman spectroscopy have been used to characterize the structure, morphology and composition of the nanostructured zinc oxide. The optical properties of the as-obtained materials were also studied and showing that it is possible to apply the ZnO nanoshuttles and nanorods on the UV filter, photocatalysis, and special optical devices. |
| doi_str_mv | 10.1016/j.materresbull.2011.12.027 |
| format | Article |
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► Nanostructured ZnO were successfully obtained by a hydrothermal route. ► Inorganic precursor and molar ratio are key factors for morphology and particle size. ► Optical properties were also studied.
Nanostructured ZnO (nanorods, nanoshuttles) have been synthesized by hydrothermal approach using ZnCl2 or Zn(NO3)2·6H2O as zinc sources and cetyltrimethylammonium bromide as structure-directing agent. Techniques X-ray powder diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), UV–visible absorption, Fourier transform infrared spectroscopy (FTIR) and Raman spectroscopy have been used to characterize the structure, morphology and composition of the nanostructured zinc oxide. The optical properties of the as-obtained materials were also studied and showing that it is possible to apply the ZnO nanoshuttles and nanorods on the UV filter, photocatalysis, and special optical devices.</description><identifier>ISSN: 0025-5408</identifier><identifier>EISSN: 1873-4227</identifier><identifier>DOI: 10.1016/j.materresbull.2011.12.027</identifier><language>eng</language><publisher>United States: Elsevier Ltd</publisher><subject>A. Inorganic compounds ; ABSORPTION ; B. Chemical synthesis ; C. Raman spectroscopy ; C. X-ray diffraction ; FOURIER TRANSFORM SPECTROMETERS ; FOURIER TRANSFORMATION ; HYDROTHERMAL SYNTHESIS ; INFRARED SPECTRA ; INORGANIC COMPOUNDS ; INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY ; MATERIALS SCIENCE ; NANOSCIENCE AND NANOTECHNOLOGY ; NANOSTRUCTURES ; OPTICAL PROPERTIES ; PARTICLE SIZE ; RAMAN SPECTROSCOPY ; SCANNING ELECTRON MICROSCOPY ; TRANSMISSION ELECTRON MICROSCOPY ; X-RAY DIFFRACTION ; ZINC ; ZINC CHLORIDES ; ZINC OXIDES</subject><ispartof>Materials research bulletin, 2012-03, Vol.47 (3), p.667-671</ispartof><rights>2011 Elsevier Ltd</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c352t-5b81e3011bb8652027d290e6a5f1ca9dd294105311c06c0d37f967708d838f1d3</citedby><cites>FETCH-LOGICAL-c352t-5b81e3011bb8652027d290e6a5f1ca9dd294105311c06c0d37f967708d838f1d3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0025540811006350$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>230,314,776,780,881,3537,27901,27902,65306</link.rule.ids><backlink>$$Uhttps://www.osti.gov/biblio/22212453$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Moulahi, A.</creatorcontrib><creatorcontrib>Sediri, F.</creatorcontrib><creatorcontrib>Gharbi, N.</creatorcontrib><title>Hydrothermal synthesis of nanostructured zinc oxide and study of their optical properties</title><title>Materials research bulletin</title><description>[Display omitted]
► Nanostructured ZnO were successfully obtained by a hydrothermal route. ► Inorganic precursor and molar ratio are key factors for morphology and particle size. ► Optical properties were also studied.
Nanostructured ZnO (nanorods, nanoshuttles) have been synthesized by hydrothermal approach using ZnCl2 or Zn(NO3)2·6H2O as zinc sources and cetyltrimethylammonium bromide as structure-directing agent. Techniques X-ray powder diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), UV–visible absorption, Fourier transform infrared spectroscopy (FTIR) and Raman spectroscopy have been used to characterize the structure, morphology and composition of the nanostructured zinc oxide. The optical properties of the as-obtained materials were also studied and showing that it is possible to apply the ZnO nanoshuttles and nanorods on the UV filter, photocatalysis, and special optical devices.</description><subject>A. Inorganic compounds</subject><subject>ABSORPTION</subject><subject>B. Chemical synthesis</subject><subject>C. Raman spectroscopy</subject><subject>C. X-ray diffraction</subject><subject>FOURIER TRANSFORM SPECTROMETERS</subject><subject>FOURIER TRANSFORMATION</subject><subject>HYDROTHERMAL SYNTHESIS</subject><subject>INFRARED SPECTRA</subject><subject>INORGANIC COMPOUNDS</subject><subject>INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY</subject><subject>MATERIALS SCIENCE</subject><subject>NANOSCIENCE AND NANOTECHNOLOGY</subject><subject>NANOSTRUCTURES</subject><subject>OPTICAL PROPERTIES</subject><subject>PARTICLE SIZE</subject><subject>RAMAN SPECTROSCOPY</subject><subject>SCANNING ELECTRON MICROSCOPY</subject><subject>TRANSMISSION ELECTRON MICROSCOPY</subject><subject>X-RAY DIFFRACTION</subject><subject>ZINC</subject><subject>ZINC CHLORIDES</subject><subject>ZINC OXIDES</subject><issn>0025-5408</issn><issn>1873-4227</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><recordid>eNqNUDtPwzAQthBIlMJ_iGBO8DkPu2yoPIpUiQUGJiuxL6qrNI5sBxF-PY7KwMh0d9L3uo-Qa6AZUKhu99mhDugc-mbsuoxRgAxYRhk_IQsQPE8LxvgpWVDKyrQsqDgnF97vKaWF4HxBPjaTdjbs0B3qLvFTH1dvfGLbpK9764MbVRgd6uTb9CqxX0ZjUvc68WHU0wyLBOMSOwSjosLg7IAuGPSX5KytO49Xv3NJ3p8e39abdPv6_LK-36YqL1lIy0YA5jF304iqZDG5ZiuKVV22oOqVjlcBtMwBFK0U1TlvVxXnVGiRixZ0viQ3R90Y1kivTEC1U7bvUQXJGANWlHlE3R1RylnvHbZycOZQu0kClXOVci__VinnKiUwGQNF8sORjPGPT4NutsFeoTZudtHW_EfmB4TUhRI</recordid><startdate>20120301</startdate><enddate>20120301</enddate><creator>Moulahi, A.</creator><creator>Sediri, F.</creator><creator>Gharbi, N.</creator><general>Elsevier Ltd</general><scope>AAYXX</scope><scope>CITATION</scope><scope>OTOTI</scope></search><sort><creationdate>20120301</creationdate><title>Hydrothermal synthesis of nanostructured zinc oxide and study of their optical properties</title><author>Moulahi, A. ; Sediri, F. ; Gharbi, N.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c352t-5b81e3011bb8652027d290e6a5f1ca9dd294105311c06c0d37f967708d838f1d3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>A. Inorganic compounds</topic><topic>ABSORPTION</topic><topic>B. Chemical synthesis</topic><topic>C. Raman spectroscopy</topic><topic>C. X-ray diffraction</topic><topic>FOURIER TRANSFORM SPECTROMETERS</topic><topic>FOURIER TRANSFORMATION</topic><topic>HYDROTHERMAL SYNTHESIS</topic><topic>INFRARED SPECTRA</topic><topic>INORGANIC COMPOUNDS</topic><topic>INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY</topic><topic>MATERIALS SCIENCE</topic><topic>NANOSCIENCE AND NANOTECHNOLOGY</topic><topic>NANOSTRUCTURES</topic><topic>OPTICAL PROPERTIES</topic><topic>PARTICLE SIZE</topic><topic>RAMAN SPECTROSCOPY</topic><topic>SCANNING ELECTRON MICROSCOPY</topic><topic>TRANSMISSION ELECTRON MICROSCOPY</topic><topic>X-RAY DIFFRACTION</topic><topic>ZINC</topic><topic>ZINC CHLORIDES</topic><topic>ZINC OXIDES</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Moulahi, A.</creatorcontrib><creatorcontrib>Sediri, F.</creatorcontrib><creatorcontrib>Gharbi, N.</creatorcontrib><collection>CrossRef</collection><collection>OSTI.GOV</collection><jtitle>Materials research bulletin</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Moulahi, A.</au><au>Sediri, F.</au><au>Gharbi, N.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Hydrothermal synthesis of nanostructured zinc oxide and study of their optical properties</atitle><jtitle>Materials research bulletin</jtitle><date>2012-03-01</date><risdate>2012</risdate><volume>47</volume><issue>3</issue><spage>667</spage><epage>671</epage><pages>667-671</pages><issn>0025-5408</issn><eissn>1873-4227</eissn><abstract>[Display omitted]
► Nanostructured ZnO were successfully obtained by a hydrothermal route. ► Inorganic precursor and molar ratio are key factors for morphology and particle size. ► Optical properties were also studied.
Nanostructured ZnO (nanorods, nanoshuttles) have been synthesized by hydrothermal approach using ZnCl2 or Zn(NO3)2·6H2O as zinc sources and cetyltrimethylammonium bromide as structure-directing agent. Techniques X-ray powder diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), UV–visible absorption, Fourier transform infrared spectroscopy (FTIR) and Raman spectroscopy have been used to characterize the structure, morphology and composition of the nanostructured zinc oxide. The optical properties of the as-obtained materials were also studied and showing that it is possible to apply the ZnO nanoshuttles and nanorods on the UV filter, photocatalysis, and special optical devices.</abstract><cop>United States</cop><pub>Elsevier Ltd</pub><doi>10.1016/j.materresbull.2011.12.027</doi><tpages>5</tpages></addata></record> |
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| ispartof | Materials research bulletin, 2012-03, Vol.47 (3), p.667-671 |
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| language | eng |
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| source | Elsevier ScienceDirect Journals |
| subjects | A. Inorganic compounds ABSORPTION B. Chemical synthesis C. Raman spectroscopy C. X-ray diffraction FOURIER TRANSFORM SPECTROMETERS FOURIER TRANSFORMATION HYDROTHERMAL SYNTHESIS INFRARED SPECTRA INORGANIC COMPOUNDS INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY MATERIALS SCIENCE NANOSCIENCE AND NANOTECHNOLOGY NANOSTRUCTURES OPTICAL PROPERTIES PARTICLE SIZE RAMAN SPECTROSCOPY SCANNING ELECTRON MICROSCOPY TRANSMISSION ELECTRON MICROSCOPY X-RAY DIFFRACTION ZINC ZINC CHLORIDES ZINC OXIDES |
| title | Hydrothermal synthesis of nanostructured zinc oxide and study of their optical properties |
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