Synthesis and structure of zinc iodide complex with thiocarbamide, [Zn(CH4N2S)2I2]
A complex compound of zinc iodide with thiocarbamide [Zn(CH 4 N 2 S) 2 I 2 ] is obtained and its structure is studied by X-ray diffraction. Crystals are monoclinic, a = 10.494(2) Å, b = 7.473(2) Å, c = 14.871(4) Å, β = 91.354(18)°, V = 1165.9(5) Å 3 , space group P 2 1 / c , Z = 4. The structural un...
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| Veröffentlicht in: | Crystallography reports 2013-01, Vol.58 (1), p.65-67 |
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| creator | Albov, D. V. Buravlev, E. A. Savinkina, E. V. Zamilatskov, I. A. |
| description | A complex compound of zinc iodide with thiocarbamide [Zn(CH
4
N
2
S)
2
I
2
] is obtained and its structure is studied by X-ray diffraction. Crystals are monoclinic,
a
= 10.494(2) Å,
b
= 7.473(2) Å,
c
= 14.871(4) Å, β = 91.354(18)°,
V
= 1165.9(5) Å
3
, space group
P
2
1
/
c
,
Z
= 4. The structural unit of the crystal is molecular complex [Zn(CH
4
N
2
S)
2
I
2
], in which the zinc atom is coordinated by sulfur atoms of two thiocarbamide molecules and two iodine atoms. |
| doi_str_mv | 10.1134/S1063774513010033 |
| format | Article |
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4
N
2
S)
2
I
2
] is obtained and its structure is studied by X-ray diffraction. Crystals are monoclinic,
a
= 10.494(2) Å,
b
= 7.473(2) Å,
c
= 14.871(4) Å, β = 91.354(18)°,
V
= 1165.9(5) Å
3
, space group
P
2
1
/
c
,
Z
= 4. The structural unit of the crystal is molecular complex [Zn(CH
4
N
2
S)
2
I
2
], in which the zinc atom is coordinated by sulfur atoms of two thiocarbamide molecules and two iodine atoms.</description><identifier>ISSN: 1063-7745</identifier><identifier>EISSN: 1562-689X</identifier><identifier>DOI: 10.1134/S1063774513010033</identifier><language>eng</language><publisher>Dordrecht: SP MAIK Nauka/Interperiodica</publisher><subject>CARBON 14 ; Crystallography and Scattering Methods ; CRYSTALS ; IODINE ; MATERIALS SCIENCE ; MONOCLINIC LATTICES ; Physics ; Physics and Astronomy ; SPACE GROUPS ; Structure of Inorganic Compounds ; SYNTHESIS ; X-RAY DIFFRACTION ; ZINC ; ZINC IODIDES</subject><ispartof>Crystallography reports, 2013-01, Vol.58 (1), p.65-67</ispartof><rights>Pleiades Publishing, Ltd. 2013</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c316t-e3688093006fbbb0ac891cc77bce5dce961cde4ba9f322c281910e107b34945c3</citedby><cites>FETCH-LOGICAL-c316t-e3688093006fbbb0ac891cc77bce5dce961cde4ba9f322c281910e107b34945c3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S1063774513010033$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S1063774513010033$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>230,314,778,782,883,27911,27912,41475,42544,51306</link.rule.ids><backlink>$$Uhttps://www.osti.gov/biblio/22156472$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Albov, D. V.</creatorcontrib><creatorcontrib>Buravlev, E. A.</creatorcontrib><creatorcontrib>Savinkina, E. V.</creatorcontrib><creatorcontrib>Zamilatskov, I. A.</creatorcontrib><title>Synthesis and structure of zinc iodide complex with thiocarbamide, [Zn(CH4N2S)2I2]</title><title>Crystallography reports</title><addtitle>Crystallogr. Rep</addtitle><description>A complex compound of zinc iodide with thiocarbamide [Zn(CH
4
N
2
S)
2
I
2
] is obtained and its structure is studied by X-ray diffraction. Crystals are monoclinic,
a
= 10.494(2) Å,
b
= 7.473(2) Å,
c
= 14.871(4) Å, β = 91.354(18)°,
V
= 1165.9(5) Å
3
, space group
P
2
1
/
c
,
Z
= 4. The structural unit of the crystal is molecular complex [Zn(CH
4
N
2
S)
2
I
2
], in which the zinc atom is coordinated by sulfur atoms of two thiocarbamide molecules and two iodine atoms.</description><subject>CARBON 14</subject><subject>Crystallography and Scattering Methods</subject><subject>CRYSTALS</subject><subject>IODINE</subject><subject>MATERIALS SCIENCE</subject><subject>MONOCLINIC LATTICES</subject><subject>Physics</subject><subject>Physics and Astronomy</subject><subject>SPACE GROUPS</subject><subject>Structure of Inorganic Compounds</subject><subject>SYNTHESIS</subject><subject>X-RAY DIFFRACTION</subject><subject>ZINC</subject><subject>ZINC IODIDES</subject><issn>1063-7745</issn><issn>1562-689X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><recordid>eNp9kE9LAzEUxIMoWKsfwFvAi4KreUn231GK2kJRsAqiyLL7NuumtElJUrR-eiP1Jnh6A7-ZBzOEHAO7ABDycgYsE3kuUxAMGBNihwwgzXiSFeXzbtQRJz98nxx4P2eMFQXIAXmYbUzoldee1qalPrg1hrVT1Hb0Sxuk2ra6VRTtcrVQn_RDh56GXlusXVMvIzqnry_mdDSWd3x2xif87ZDsdfXCq6PfOyRPN9ePo3Eyvb-djK6mCQrIQqJEVhSsFIxlXdM0rMaiBMQ8b1ClLaoyA2yVbOqyE5wjL6AEpoDljZClTFEMycn2r_VBVx51UNijNUZhqDiP7WXOowu2LnTWe6e6auX0snabClj1M131Z7qY4duMj17zrlw1t2tnYpl_Qt-6k26y</recordid><startdate>20130101</startdate><enddate>20130101</enddate><creator>Albov, D. V.</creator><creator>Buravlev, E. A.</creator><creator>Savinkina, E. V.</creator><creator>Zamilatskov, I. A.</creator><general>SP MAIK Nauka/Interperiodica</general><scope>AAYXX</scope><scope>CITATION</scope><scope>OTOTI</scope></search><sort><creationdate>20130101</creationdate><title>Synthesis and structure of zinc iodide complex with thiocarbamide, [Zn(CH4N2S)2I2]</title><author>Albov, D. V. ; Buravlev, E. A. ; Savinkina, E. V. ; Zamilatskov, I. A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c316t-e3688093006fbbb0ac891cc77bce5dce961cde4ba9f322c281910e107b34945c3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>CARBON 14</topic><topic>Crystallography and Scattering Methods</topic><topic>CRYSTALS</topic><topic>IODINE</topic><topic>MATERIALS SCIENCE</topic><topic>MONOCLINIC LATTICES</topic><topic>Physics</topic><topic>Physics and Astronomy</topic><topic>SPACE GROUPS</topic><topic>Structure of Inorganic Compounds</topic><topic>SYNTHESIS</topic><topic>X-RAY DIFFRACTION</topic><topic>ZINC</topic><topic>ZINC IODIDES</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Albov, D. V.</creatorcontrib><creatorcontrib>Buravlev, E. A.</creatorcontrib><creatorcontrib>Savinkina, E. V.</creatorcontrib><creatorcontrib>Zamilatskov, I. A.</creatorcontrib><collection>CrossRef</collection><collection>OSTI.GOV</collection><jtitle>Crystallography reports</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Albov, D. V.</au><au>Buravlev, E. A.</au><au>Savinkina, E. V.</au><au>Zamilatskov, I. A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and structure of zinc iodide complex with thiocarbamide, [Zn(CH4N2S)2I2]</atitle><jtitle>Crystallography reports</jtitle><stitle>Crystallogr. Rep</stitle><date>2013-01-01</date><risdate>2013</risdate><volume>58</volume><issue>1</issue><spage>65</spage><epage>67</epage><pages>65-67</pages><issn>1063-7745</issn><eissn>1562-689X</eissn><abstract>A complex compound of zinc iodide with thiocarbamide [Zn(CH
4
N
2
S)
2
I
2
] is obtained and its structure is studied by X-ray diffraction. Crystals are monoclinic,
a
= 10.494(2) Å,
b
= 7.473(2) Å,
c
= 14.871(4) Å, β = 91.354(18)°,
V
= 1165.9(5) Å
3
, space group
P
2
1
/
c
,
Z
= 4. The structural unit of the crystal is molecular complex [Zn(CH
4
N
2
S)
2
I
2
], in which the zinc atom is coordinated by sulfur atoms of two thiocarbamide molecules and two iodine atoms.</abstract><cop>Dordrecht</cop><pub>SP MAIK Nauka/Interperiodica</pub><doi>10.1134/S1063774513010033</doi><tpages>3</tpages></addata></record> |
| fulltext | fulltext |
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| ispartof | Crystallography reports, 2013-01, Vol.58 (1), p.65-67 |
| issn | 1063-7745 1562-689X |
| language | eng |
| recordid | cdi_osti_scitechconnect_22156472 |
| source | Springer Nature - Complete Springer Journals |
| subjects | CARBON 14 Crystallography and Scattering Methods CRYSTALS IODINE MATERIALS SCIENCE MONOCLINIC LATTICES Physics Physics and Astronomy SPACE GROUPS Structure of Inorganic Compounds SYNTHESIS X-RAY DIFFRACTION ZINC ZINC IODIDES |
| title | Synthesis and structure of zinc iodide complex with thiocarbamide, [Zn(CH4N2S)2I2] |
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