Quantitative assessment of alkali-reactive aggregate mineral content through XRD using polished sections as a supplementary tool to RILEM AAR-1 (petrographic method)
The mineral content of 5 aggregate samples from 4 different countries, including reactive and non-reactive aggregate types, was assessed quantitatively by X-ray diffraction (XRD) using polished sections. Additionally, electron probe microanalyzer (EPMA) mapping and cathodoluminescence (CL) were used...
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Veröffentlicht in: | Cement and concrete research 2012-11, Vol.42 (11), p.1428-1437 |
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creator | Castro, Nélia Sorensen, Bjørn E. Broekmans, Maarten A.T.M. |
description | The mineral content of 5 aggregate samples from 4 different countries, including reactive and non-reactive aggregate types, was assessed quantitatively by X-ray diffraction (XRD) using polished sections. Additionally, electron probe microanalyzer (EPMA) mapping and cathodoluminescence (CL) were used to characterize the opal-CT identified in one of the aggregate samples. Critical review of results from polished sections against traditionally powdered specimen has demonstrated that for fine-grained rocks without preferred orientation the assessment of mineral content by XRD using polished sections may represent an advantage over traditional powder specimens. Comparison of data on mineral content and silica speciation with expansion data from PARTNER project confirmed that the presence of opal-CT plays an important role in the reactivity of one of the studied aggregates. Used as a complementary tool to RILEM AAR-1, the methodology suggested in this paper has the potential to improve the strength of the petrographic method. |
doi_str_mv | 10.1016/j.cemconres.2012.08.004 |
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Additionally, electron probe microanalyzer (EPMA) mapping and cathodoluminescence (CL) were used to characterize the opal-CT identified in one of the aggregate samples. Critical review of results from polished sections against traditionally powdered specimen has demonstrated that for fine-grained rocks without preferred orientation the assessment of mineral content by XRD using polished sections may represent an advantage over traditional powder specimens. Comparison of data on mineral content and silica speciation with expansion data from PARTNER project confirmed that the presence of opal-CT plays an important role in the reactivity of one of the studied aggregates. 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Public works ; CATHODOLUMINESCENCE ; Cement concrete constituents ; ELECTRON MICROPROBE ANALYSIS ; ELECTRON PROBES ; Exact sciences and technology ; GRAIN ORIENTATION ; Materials ; MATERIALS SCIENCE ; Opaline silica ; OPALS ; PETROGRAPHY ; Petrography (B) ; REACTIVITY ; ROCKS ; X-RAY DIFFRACTION ; X-ray diffraction (B)</subject><ispartof>Cement and concrete research, 2012-11, Vol.42 (11), p.1428-1437</ispartof><rights>2012 Elsevier Ltd</rights><rights>2014 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c439t-4eb3dbe25347eb9df2973803be13024ceb9cf87fbf5fd596895f84bb0d1385763</citedby><cites>FETCH-LOGICAL-c439t-4eb3dbe25347eb9df2973803be13024ceb9cf87fbf5fd596895f84bb0d1385763</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.cemconres.2012.08.004$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>230,315,781,785,886,3551,27929,27930,46000</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=26617144$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.osti.gov/biblio/22149354$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Castro, Nélia</creatorcontrib><creatorcontrib>Sorensen, Bjørn E.</creatorcontrib><creatorcontrib>Broekmans, Maarten A.T.M.</creatorcontrib><title>Quantitative assessment of alkali-reactive aggregate mineral content through XRD using polished sections as a supplementary tool to RILEM AAR-1 (petrographic method)</title><title>Cement and concrete research</title><description>The mineral content of 5 aggregate samples from 4 different countries, including reactive and non-reactive aggregate types, was assessed quantitatively by X-ray diffraction (XRD) using polished sections. Additionally, electron probe microanalyzer (EPMA) mapping and cathodoluminescence (CL) were used to characterize the opal-CT identified in one of the aggregate samples. Critical review of results from polished sections against traditionally powdered specimen has demonstrated that for fine-grained rocks without preferred orientation the assessment of mineral content by XRD using polished sections may represent an advantage over traditional powder specimens. Comparison of data on mineral content and silica speciation with expansion data from PARTNER project confirmed that the presence of opal-CT plays an important role in the reactivity of one of the studied aggregates. Used as a complementary tool to RILEM AAR-1, the methodology suggested in this paper has the potential to improve the strength of the petrographic method.</description><subject>Aggregate (D)</subject><subject>Aggregates and other concrete constituents</subject><subject>Alkali-aggregate reaction (C)</subject><subject>Applied sciences</subject><subject>Buildings. Public works</subject><subject>CATHODOLUMINESCENCE</subject><subject>Cement concrete constituents</subject><subject>ELECTRON MICROPROBE ANALYSIS</subject><subject>ELECTRON PROBES</subject><subject>Exact sciences and technology</subject><subject>GRAIN ORIENTATION</subject><subject>Materials</subject><subject>MATERIALS SCIENCE</subject><subject>Opaline silica</subject><subject>OPALS</subject><subject>PETROGRAPHY</subject><subject>Petrography (B)</subject><subject>REACTIVITY</subject><subject>ROCKS</subject><subject>X-RAY DIFFRACTION</subject><subject>X-ray diffraction (B)</subject><issn>0008-8846</issn><issn>1873-3948</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><recordid>eNqFUdGK1DAULaLguPoNBkTQh45Jk7bp47C7ugsj4qDgW0jTmzZj25TczIIf5H-a0mVffbnh3pxzzz2cLHvL6J5RVn067w1Mxs8BcF9QVuyp3FMqnmU7Jmue80bI59mOUipzKUX1MnuFeE5tVXC5y_5-v-g5uqijewCiEQFxgjkSb4kef-vR5QG02X77PkCvI5DJzRD0SJJsXMFxCP7SD-TX6YZc0M09WfzocICOICSynzHtJprgZVlGWAV0-EOi92Mq5HR_vP1KDodTzsiHBWLwfdDL4AyZIA6--_g6e2H1iPDm8b3Kfn6-_XF9lx-_fbm_PhxzI3gTcwEt71ooSi5qaJvOFk3NJeUtME4LYdLMWFnb1pa2K5tKNqWVom1px7gs64pfZe-2vR6jU2hcBDMkk3MyoYqCiYaXIqHqDWWCRwxg1RLclAwpRtWaiTqrp0zUmomiUqVMEvP9xlw0Gj3aoGfj8IleVBWrmVhxhw0HyeyDg7DeArOBzoX1lM67_2r9A3FRqd4</recordid><startdate>20121101</startdate><enddate>20121101</enddate><creator>Castro, Nélia</creator><creator>Sorensen, Bjørn E.</creator><creator>Broekmans, Maarten A.T.M.</creator><general>Elsevier Ltd</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>OTOTI</scope></search><sort><creationdate>20121101</creationdate><title>Quantitative assessment of alkali-reactive aggregate mineral content through XRD using polished sections as a supplementary tool to RILEM AAR-1 (petrographic method)</title><author>Castro, Nélia ; Sorensen, Bjørn E. ; Broekmans, Maarten A.T.M.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c439t-4eb3dbe25347eb9df2973803be13024ceb9cf87fbf5fd596895f84bb0d1385763</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>Aggregate (D)</topic><topic>Aggregates and other concrete constituents</topic><topic>Alkali-aggregate reaction (C)</topic><topic>Applied sciences</topic><topic>Buildings. Public works</topic><topic>CATHODOLUMINESCENCE</topic><topic>Cement concrete constituents</topic><topic>ELECTRON MICROPROBE ANALYSIS</topic><topic>ELECTRON PROBES</topic><topic>Exact sciences and technology</topic><topic>GRAIN ORIENTATION</topic><topic>Materials</topic><topic>MATERIALS SCIENCE</topic><topic>Opaline silica</topic><topic>OPALS</topic><topic>PETROGRAPHY</topic><topic>Petrography (B)</topic><topic>REACTIVITY</topic><topic>ROCKS</topic><topic>X-RAY DIFFRACTION</topic><topic>X-ray diffraction (B)</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Castro, Nélia</creatorcontrib><creatorcontrib>Sorensen, Bjørn E.</creatorcontrib><creatorcontrib>Broekmans, Maarten A.T.M.</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>OSTI.GOV</collection><jtitle>Cement and concrete research</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Castro, Nélia</au><au>Sorensen, Bjørn E.</au><au>Broekmans, Maarten A.T.M.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Quantitative assessment of alkali-reactive aggregate mineral content through XRD using polished sections as a supplementary tool to RILEM AAR-1 (petrographic method)</atitle><jtitle>Cement and concrete research</jtitle><date>2012-11-01</date><risdate>2012</risdate><volume>42</volume><issue>11</issue><spage>1428</spage><epage>1437</epage><pages>1428-1437</pages><issn>0008-8846</issn><eissn>1873-3948</eissn><coden>CCNRAI</coden><abstract>The mineral content of 5 aggregate samples from 4 different countries, including reactive and non-reactive aggregate types, was assessed quantitatively by X-ray diffraction (XRD) using polished sections. Additionally, electron probe microanalyzer (EPMA) mapping and cathodoluminescence (CL) were used to characterize the opal-CT identified in one of the aggregate samples. Critical review of results from polished sections against traditionally powdered specimen has demonstrated that for fine-grained rocks without preferred orientation the assessment of mineral content by XRD using polished sections may represent an advantage over traditional powder specimens. Comparison of data on mineral content and silica speciation with expansion data from PARTNER project confirmed that the presence of opal-CT plays an important role in the reactivity of one of the studied aggregates. Used as a complementary tool to RILEM AAR-1, the methodology suggested in this paper has the potential to improve the strength of the petrographic method.</abstract><cop>Kidlington</cop><pub>Elsevier Ltd</pub><doi>10.1016/j.cemconres.2012.08.004</doi><tpages>10</tpages></addata></record> |
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subjects | Aggregate (D) Aggregates and other concrete constituents Alkali-aggregate reaction (C) Applied sciences Buildings. Public works CATHODOLUMINESCENCE Cement concrete constituents ELECTRON MICROPROBE ANALYSIS ELECTRON PROBES Exact sciences and technology GRAIN ORIENTATION Materials MATERIALS SCIENCE Opaline silica OPALS PETROGRAPHY Petrography (B) REACTIVITY ROCKS X-RAY DIFFRACTION X-ray diffraction (B) |
title | Quantitative assessment of alkali-reactive aggregate mineral content through XRD using polished sections as a supplementary tool to RILEM AAR-1 (petrographic method) |
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