Characterization of the carbides and the martensite phase in powder-metallurgy high-speed steel
A microstructural characterization of the powder-metallurgy high-speed-steel S390 Microclean was performed based on an elemental distribution of the carbide phase as well as crystallographic analyses. The results showed that there were two types of carbides present: vanadium-rich carbides, which wer...
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| Veröffentlicht in: | Materials characterization 2010-04, Vol.61 (4), p.452-458 |
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| creator | Godec, Matjaž Batič, Barbara Šetina Mandrino, Djordje Nagode, Aleš Leskovšek, Vojteh Škapin, Srečo D. Jenko, Monika |
| description | A microstructural characterization of the powder-metallurgy high-speed-steel S390 Microclean was performed based on an elemental distribution of the carbide phase as well as crystallographic analyses. The results showed that there were two types of carbides present: vanadium-rich carbides, which were not chemically homogeneous and exhibited a tungsten-enriched or tungsten-depleted central area; and chemically homogeneous tungsten-rich M
6C-type carbides. Despite the possibility of chemical inhomogenities, the crystallographic orientation of each of the carbides was shown to be uniform. Using electron backscatter diffraction the vanadium-rich carbides were determined to be either cubic VC or hexagonal V
6C
5, while the tungsten-rich carbides were M
6C. The electron backscatter diffraction results were also verified using X-ray diffraction. Several electron backscatter diffraction pattern maps were acquired in order to define the fraction of each carbide phase as well as the amount of martensite phase. The fraction of martensite was estimated using band-contrast images, while the fraction of carbides was calculated using the crystallographic data. |
| doi_str_mv | 10.1016/j.matchar.2010.02.003 |
| format | Article |
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6C-type carbides. Despite the possibility of chemical inhomogenities, the crystallographic orientation of each of the carbides was shown to be uniform. Using electron backscatter diffraction the vanadium-rich carbides were determined to be either cubic VC or hexagonal V
6C
5, while the tungsten-rich carbides were M
6C. The electron backscatter diffraction results were also verified using X-ray diffraction. Several electron backscatter diffraction pattern maps were acquired in order to define the fraction of each carbide phase as well as the amount of martensite phase. The fraction of martensite was estimated using band-contrast images, while the fraction of carbides was calculated using the crystallographic data.</description><identifier>ISSN: 1044-5803</identifier><identifier>EISSN: 1873-4189</identifier><identifier>DOI: 10.1016/j.matchar.2010.02.003</identifier><language>eng</language><publisher>New York, NY: Elsevier Inc</publisher><subject>AES ; AUGER ELECTRON SPECTROSCOPY ; BACKSCATTERING ; Carbides ; Cross-disciplinary physics: materials science; rheology ; Crystallography ; CUBIC LATTICES ; Diffraction ; EBSD ; EDS ; Electron back scatter diffraction ; ELECTRON DIFFRACTION ; Exact sciences and technology ; HEXAGONAL LATTICES ; Inhomogeneities ; MARTENSITE ; MATERIALS SCIENCE ; Mathematical analysis ; MICROSTRUCTURE ; Phase diagrams and microstructures developed by solidification and solid-solid phase transformations ; Physics ; POWDER METALLURGY ; Solidification ; STEELS ; Tool steel ; TUNGSTEN ; VANADIUM ; VANADIUM CARBIDES ; X-RAY DIFFRACTION ; XRD</subject><ispartof>Materials characterization, 2010-04, Vol.61 (4), p.452-458</ispartof><rights>2010 Elsevier Inc.</rights><rights>2015 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c497t-fb80cac217547e14da82b191345058739d7758753c1b1ad51fc4f390b88f88093</citedby><cites>FETCH-LOGICAL-c497t-fb80cac217547e14da82b191345058739d7758753c1b1ad51fc4f390b88f88093</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S1044580310000343$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>230,314,776,780,881,3537,27901,27902,65306</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=22615936$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.osti.gov/biblio/22066203$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Godec, Matjaž</creatorcontrib><creatorcontrib>Batič, Barbara Šetina</creatorcontrib><creatorcontrib>Mandrino, Djordje</creatorcontrib><creatorcontrib>Nagode, Aleš</creatorcontrib><creatorcontrib>Leskovšek, Vojteh</creatorcontrib><creatorcontrib>Škapin, Srečo D.</creatorcontrib><creatorcontrib>Jenko, Monika</creatorcontrib><title>Characterization of the carbides and the martensite phase in powder-metallurgy high-speed steel</title><title>Materials characterization</title><description>A microstructural characterization of the powder-metallurgy high-speed-steel S390 Microclean was performed based on an elemental distribution of the carbide phase as well as crystallographic analyses. The results showed that there were two types of carbides present: vanadium-rich carbides, which were not chemically homogeneous and exhibited a tungsten-enriched or tungsten-depleted central area; and chemically homogeneous tungsten-rich M
6C-type carbides. Despite the possibility of chemical inhomogenities, the crystallographic orientation of each of the carbides was shown to be uniform. Using electron backscatter diffraction the vanadium-rich carbides were determined to be either cubic VC or hexagonal V
6C
5, while the tungsten-rich carbides were M
6C. The electron backscatter diffraction results were also verified using X-ray diffraction. Several electron backscatter diffraction pattern maps were acquired in order to define the fraction of each carbide phase as well as the amount of martensite phase. The fraction of martensite was estimated using band-contrast images, while the fraction of carbides was calculated using the crystallographic data.</description><subject>AES</subject><subject>AUGER ELECTRON SPECTROSCOPY</subject><subject>BACKSCATTERING</subject><subject>Carbides</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Crystallography</subject><subject>CUBIC LATTICES</subject><subject>Diffraction</subject><subject>EBSD</subject><subject>EDS</subject><subject>Electron back scatter diffraction</subject><subject>ELECTRON DIFFRACTION</subject><subject>Exact sciences and technology</subject><subject>HEXAGONAL LATTICES</subject><subject>Inhomogeneities</subject><subject>MARTENSITE</subject><subject>MATERIALS SCIENCE</subject><subject>Mathematical analysis</subject><subject>MICROSTRUCTURE</subject><subject>Phase diagrams and microstructures developed by solidification and solid-solid phase transformations</subject><subject>Physics</subject><subject>POWDER METALLURGY</subject><subject>Solidification</subject><subject>STEELS</subject><subject>Tool steel</subject><subject>TUNGSTEN</subject><subject>VANADIUM</subject><subject>VANADIUM CARBIDES</subject><subject>X-RAY DIFFRACTION</subject><subject>XRD</subject><issn>1044-5803</issn><issn>1873-4189</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2010</creationdate><recordtype>article</recordtype><recordid>eNqFkUFr3DAQhU1poWnSn1AQlNKTNyPJsuRTKUuTFgK5pGchS-NYi1dyJW1L-uurzS695jRi-Ebz3rym-UBhQ4H217vN3hQ7m7RhUHvANgD8VXNBleRtR9Xwur6h61qhgL9t3uW8A4BeUXnR6G2dM7Zg8n9N8TGQOJEyI7Emjd5hJia458bepIIh-4JknU1G4gNZ4x-Hqd1jMctySI9PZPaPc5tXREdyQVyumjeTWTK-P9fL5ufNt4ft9_bu_vbH9utda7tBlnYaFVhjGZWik0g7ZxQb6UB5J0BUG4OTslbBLR2pcYJOtpv4AKNSk1Iw8Mvm4-nfmIvX2VaZdrYxBLRFMwZ9z4BX6vOJWlP8dcBc9N5ni8tiAsZD1kqIXgomuhfJKkVyAaAqKU6kTTHnhJNek6_HetIU9DEfvdPnfPQxHw1Mw7OWT-cNJluzTMkE6_P_YcZ6KgbeV-7LicN6vt8e09EdBovOp6M5F_0Lm_4Bs76nsQ</recordid><startdate>20100401</startdate><enddate>20100401</enddate><creator>Godec, Matjaž</creator><creator>Batič, Barbara Šetina</creator><creator>Mandrino, Djordje</creator><creator>Nagode, Aleš</creator><creator>Leskovšek, Vojteh</creator><creator>Škapin, Srečo D.</creator><creator>Jenko, Monika</creator><general>Elsevier Inc</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>OTOTI</scope></search><sort><creationdate>20100401</creationdate><title>Characterization of the carbides and the martensite phase in powder-metallurgy high-speed steel</title><author>Godec, Matjaž ; Batič, Barbara Šetina ; Mandrino, Djordje ; Nagode, Aleš ; Leskovšek, Vojteh ; Škapin, Srečo D. ; Jenko, Monika</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c497t-fb80cac217547e14da82b191345058739d7758753c1b1ad51fc4f390b88f88093</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2010</creationdate><topic>AES</topic><topic>AUGER ELECTRON SPECTROSCOPY</topic><topic>BACKSCATTERING</topic><topic>Carbides</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Crystallography</topic><topic>CUBIC LATTICES</topic><topic>Diffraction</topic><topic>EBSD</topic><topic>EDS</topic><topic>Electron back scatter diffraction</topic><topic>ELECTRON DIFFRACTION</topic><topic>Exact sciences and technology</topic><topic>HEXAGONAL LATTICES</topic><topic>Inhomogeneities</topic><topic>MARTENSITE</topic><topic>MATERIALS SCIENCE</topic><topic>Mathematical analysis</topic><topic>MICROSTRUCTURE</topic><topic>Phase diagrams and microstructures developed by solidification and solid-solid phase transformations</topic><topic>Physics</topic><topic>POWDER METALLURGY</topic><topic>Solidification</topic><topic>STEELS</topic><topic>Tool steel</topic><topic>TUNGSTEN</topic><topic>VANADIUM</topic><topic>VANADIUM CARBIDES</topic><topic>X-RAY DIFFRACTION</topic><topic>XRD</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Godec, Matjaž</creatorcontrib><creatorcontrib>Batič, Barbara Šetina</creatorcontrib><creatorcontrib>Mandrino, Djordje</creatorcontrib><creatorcontrib>Nagode, Aleš</creatorcontrib><creatorcontrib>Leskovšek, Vojteh</creatorcontrib><creatorcontrib>Škapin, Srečo D.</creatorcontrib><creatorcontrib>Jenko, Monika</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>OSTI.GOV</collection><jtitle>Materials characterization</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Godec, Matjaž</au><au>Batič, Barbara Šetina</au><au>Mandrino, Djordje</au><au>Nagode, Aleš</au><au>Leskovšek, Vojteh</au><au>Škapin, Srečo D.</au><au>Jenko, Monika</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Characterization of the carbides and the martensite phase in powder-metallurgy high-speed steel</atitle><jtitle>Materials characterization</jtitle><date>2010-04-01</date><risdate>2010</risdate><volume>61</volume><issue>4</issue><spage>452</spage><epage>458</epage><pages>452-458</pages><issn>1044-5803</issn><eissn>1873-4189</eissn><abstract>A microstructural characterization of the powder-metallurgy high-speed-steel S390 Microclean was performed based on an elemental distribution of the carbide phase as well as crystallographic analyses. The results showed that there were two types of carbides present: vanadium-rich carbides, which were not chemically homogeneous and exhibited a tungsten-enriched or tungsten-depleted central area; and chemically homogeneous tungsten-rich M
6C-type carbides. Despite the possibility of chemical inhomogenities, the crystallographic orientation of each of the carbides was shown to be uniform. Using electron backscatter diffraction the vanadium-rich carbides were determined to be either cubic VC or hexagonal V
6C
5, while the tungsten-rich carbides were M
6C. The electron backscatter diffraction results were also verified using X-ray diffraction. Several electron backscatter diffraction pattern maps were acquired in order to define the fraction of each carbide phase as well as the amount of martensite phase. The fraction of martensite was estimated using band-contrast images, while the fraction of carbides was calculated using the crystallographic data.</abstract><cop>New York, NY</cop><pub>Elsevier Inc</pub><doi>10.1016/j.matchar.2010.02.003</doi><tpages>7</tpages></addata></record> |
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| source | Elsevier ScienceDirect Journals |
| subjects | AES AUGER ELECTRON SPECTROSCOPY BACKSCATTERING Carbides Cross-disciplinary physics: materials science rheology Crystallography CUBIC LATTICES Diffraction EBSD EDS Electron back scatter diffraction ELECTRON DIFFRACTION Exact sciences and technology HEXAGONAL LATTICES Inhomogeneities MARTENSITE MATERIALS SCIENCE Mathematical analysis MICROSTRUCTURE Phase diagrams and microstructures developed by solidification and solid-solid phase transformations Physics POWDER METALLURGY Solidification STEELS Tool steel TUNGSTEN VANADIUM VANADIUM CARBIDES X-RAY DIFFRACTION XRD |
| title | Characterization of the carbides and the martensite phase in powder-metallurgy high-speed steel |
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