Nanocrystalline zinc oxide: Pyrolytic synthesis and spectroscopic characteristics

Nanocrystalline and microcrystalline ZnO powders are synthesized by the pyrolysis of organic zinc salts in the presence of a reducing catalyst represented by a porous cellulose carrier. The specimens obtained are characterized by X-ray powder diffraction, energy dispersive analysis, scanning electro...

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Veröffentlicht in:Crystallography reports 2010-01, Vol.55 (1), p.142-148
Hauptverfasser: Demyanets, L. N., Li, L. E., Lavrikov, A. S., Nikitin, S. V.
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Li, L. E.
Lavrikov, A. S.
Nikitin, S. V.
description Nanocrystalline and microcrystalline ZnO powders are synthesized by the pyrolysis of organic zinc salts in the presence of a reducing catalyst represented by a porous cellulose carrier. The specimens obtained are characterized by X-ray powder diffraction, energy dispersive analysis, scanning electron microscopy, and pulse cathodoluminescence. Lasing characteristics of the specimens are studied. The synthesis conditions, under which specimens with the crystallite morphology optimal for a low-threshold lasing are obtained, are found.
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subjects CARRIERS
CATALYSTS
CATHODOLUMINESCENCE
CELLULOSE
CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY
Crystallography and Scattering Methods
CRYSTALS
MORPHOLOGY
Nanomaterials
NANOSTRUCTURES
Physics
Physics and Astronomy
POROUS MATERIALS
POWDERS
PYROLYSIS
SCANNING ELECTRON MICROSCOPY
SYNTHESIS
X-RAY DIFFRACTION
ZINC OXIDES
title Nanocrystalline zinc oxide: Pyrolytic synthesis and spectroscopic characteristics
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