Nanocrystalline zinc oxide: Pyrolytic synthesis and spectroscopic characteristics
Nanocrystalline and microcrystalline ZnO powders are synthesized by the pyrolysis of organic zinc salts in the presence of a reducing catalyst represented by a porous cellulose carrier. The specimens obtained are characterized by X-ray powder diffraction, energy dispersive analysis, scanning electro...
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Veröffentlicht in: | Crystallography reports 2010-01, Vol.55 (1), p.142-148 |
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description | Nanocrystalline and microcrystalline ZnO powders are synthesized by the pyrolysis of organic zinc salts in the presence of a reducing catalyst represented by a porous cellulose carrier. The specimens obtained are characterized by X-ray powder diffraction, energy dispersive analysis, scanning electron microscopy, and pulse cathodoluminescence. Lasing characteristics of the specimens are studied. The synthesis conditions, under which specimens with the crystallite morphology optimal for a low-threshold lasing are obtained, are found. |
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The synthesis conditions, under which specimens with the crystallite morphology optimal for a low-threshold lasing are obtained, are found.</description><identifier>ISSN: 1063-7745</identifier><identifier>EISSN: 1562-689X</identifier><identifier>DOI: 10.1134/S1063774510010219</identifier><language>eng</language><publisher>Dordrecht: SP MAIK Nauka/Interperiodica</publisher><subject>CARRIERS ; CATALYSTS ; CATHODOLUMINESCENCE ; CELLULOSE ; CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY ; Crystallography and Scattering Methods ; CRYSTALS ; MORPHOLOGY ; Nanomaterials ; NANOSTRUCTURES ; Physics ; Physics and Astronomy ; POROUS MATERIALS ; POWDERS ; PYROLYSIS ; SCANNING ELECTRON MICROSCOPY ; SYNTHESIS ; X-RAY DIFFRACTION ; ZINC OXIDES</subject><ispartof>Crystallography reports, 2010-01, Vol.55 (1), p.142-148</ispartof><rights>Pleiades Publishing, Ltd. 2010</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c316t-76e7e15ee17b4529df7ef5f838108440dace95b46897b65ed65840c34086ae073</citedby><cites>FETCH-LOGICAL-c316t-76e7e15ee17b4529df7ef5f838108440dace95b46897b65ed65840c34086ae073</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S1063774510010219$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S1063774510010219$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>230,314,780,784,885,27924,27925,41488,42557,51319</link.rule.ids><backlink>$$Uhttps://www.osti.gov/biblio/22051236$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Demyanets, L. N.</creatorcontrib><creatorcontrib>Li, L. E.</creatorcontrib><creatorcontrib>Lavrikov, A. S.</creatorcontrib><creatorcontrib>Nikitin, S. V.</creatorcontrib><title>Nanocrystalline zinc oxide: Pyrolytic synthesis and spectroscopic characteristics</title><title>Crystallography reports</title><addtitle>Crystallogr. Rep</addtitle><description>Nanocrystalline and microcrystalline ZnO powders are synthesized by the pyrolysis of organic zinc salts in the presence of a reducing catalyst represented by a porous cellulose carrier. The specimens obtained are characterized by X-ray powder diffraction, energy dispersive analysis, scanning electron microscopy, and pulse cathodoluminescence. Lasing characteristics of the specimens are studied. The synthesis conditions, under which specimens with the crystallite morphology optimal for a low-threshold lasing are obtained, are found.</description><subject>CARRIERS</subject><subject>CATALYSTS</subject><subject>CATHODOLUMINESCENCE</subject><subject>CELLULOSE</subject><subject>CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY</subject><subject>Crystallography and Scattering Methods</subject><subject>CRYSTALS</subject><subject>MORPHOLOGY</subject><subject>Nanomaterials</subject><subject>NANOSTRUCTURES</subject><subject>Physics</subject><subject>Physics and Astronomy</subject><subject>POROUS MATERIALS</subject><subject>POWDERS</subject><subject>PYROLYSIS</subject><subject>SCANNING ELECTRON MICROSCOPY</subject><subject>SYNTHESIS</subject><subject>X-RAY DIFFRACTION</subject><subject>ZINC OXIDES</subject><issn>1063-7745</issn><issn>1562-689X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2010</creationdate><recordtype>article</recordtype><recordid>eNp9kFtLxDAQhYMouK7-AN8KPldn2tzWNxFvsHhBBd9KNp26WWqyJBWsv94s65vg0wyc78ycGcaOEU4Ra372jCBrpbhAAIQKZztsgkJWpdSzt93cZ7nc6PvsIKUVAGiNfMKe7o0PNo5pMH3vPBXfztsifLmWzovHMYZ-HJwt0uiHJSWXCuPbIq3JDjEkG9ZZs0sTjR0oupTRdMj2OtMnOvqtU_Z6ffVyeVvOH27uLi_mpa1RDqWSpAgFEaoFF9Ws7RR1otO1RtCcQ2sszcSC5_xqIQW1UmgOtuagpSFQ9ZSdbOeGvLZJ1g1klzZ4n7M1VQUCq1pmCreUzXlTpK5ZR_dh4tggNJvPNX8-lz3V1pMy698pNqvwGX0-5h_TD8GRcKI</recordid><startdate>20100101</startdate><enddate>20100101</enddate><creator>Demyanets, L. 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N.</creatorcontrib><creatorcontrib>Li, L. E.</creatorcontrib><creatorcontrib>Lavrikov, A. S.</creatorcontrib><creatorcontrib>Nikitin, S. V.</creatorcontrib><collection>CrossRef</collection><collection>OSTI.GOV</collection><jtitle>Crystallography reports</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Demyanets, L. N.</au><au>Li, L. E.</au><au>Lavrikov, A. S.</au><au>Nikitin, S. V.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Nanocrystalline zinc oxide: Pyrolytic synthesis and spectroscopic characteristics</atitle><jtitle>Crystallography reports</jtitle><stitle>Crystallogr. Rep</stitle><date>2010-01-01</date><risdate>2010</risdate><volume>55</volume><issue>1</issue><spage>142</spage><epage>148</epage><pages>142-148</pages><issn>1063-7745</issn><eissn>1562-689X</eissn><abstract>Nanocrystalline and microcrystalline ZnO powders are synthesized by the pyrolysis of organic zinc salts in the presence of a reducing catalyst represented by a porous cellulose carrier. The specimens obtained are characterized by X-ray powder diffraction, energy dispersive analysis, scanning electron microscopy, and pulse cathodoluminescence. Lasing characteristics of the specimens are studied. The synthesis conditions, under which specimens with the crystallite morphology optimal for a low-threshold lasing are obtained, are found.</abstract><cop>Dordrecht</cop><pub>SP MAIK Nauka/Interperiodica</pub><doi>10.1134/S1063774510010219</doi><tpages>7</tpages></addata></record> |
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subjects | CARRIERS CATALYSTS CATHODOLUMINESCENCE CELLULOSE CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY Crystallography and Scattering Methods CRYSTALS MORPHOLOGY Nanomaterials NANOSTRUCTURES Physics Physics and Astronomy POROUS MATERIALS POWDERS PYROLYSIS SCANNING ELECTRON MICROSCOPY SYNTHESIS X-RAY DIFFRACTION ZINC OXIDES |
title | Nanocrystalline zinc oxide: Pyrolytic synthesis and spectroscopic characteristics |
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