Hydrothermal synthesis and electrochemical performance of NiO microspheres with different nanoscale building blocks

NiO microspheres were successfully obtained by calcining the Ni(OH) 2 precursor, which were synthesized via the hydrothermal reaction of nickel chloride, glucose and ammonia. The products were characterized by TGA, XRD and SEM. The influences of glucose and reaction temperature on the morphologies o...

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Veröffentlicht in:	Journal of solid state chemistry 2010-11, Vol.183 (11), p.2576-2581
Hauptverfasser:	Wang, Ling, Hao, Yanjing, Zhao, Yan, Lai, Qiongyu, Xu, Xiaoyun
Format:	Artikel
Sprache:	eng
Schlagworte:	ALDEHYDES AMMONIA CARBOHYDRATES CHALCOGENIDES Charge CHEMICAL ANALYSIS CHEMISTRY CHLORIDES CHLORINE COMPOUNDS COHERENT SCATTERING Cross-disciplinary physics: materials science rheology DIFFRACTION Electrochemical performance ELECTROCHEMISTRY Electrode materials Electrodes: preparations and properties ELECTRON MICROSCOPY Exact sciences and technology General and physical chemistry GLUCOSE GRAVIMETRIC ANALYSIS Growth mechanism HALIDES HALOGEN COMPOUNDS HEXOSES HYDRIDES HYDROGEN COMPOUNDS HYDROTHERMAL SYNTHESIS HYDROXIDES INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY Materials science Methods of crystal growth physics of crystal growth MICROSCOPY MICROSPHERES MONOSACCHARIDES MORPHOLOGY Nanoscale materials and structures: fabrication and characterization Nanostructure NANOSTRUCTURES NICKEL CHLORIDES NICKEL COMPOUNDS NICKEL HYDROXIDES NICKEL OXIDES NiO microsphere NITROGEN COMPOUNDS NITROGEN HYDRIDES ORGANIC COMPOUNDS Other topics in nanoscale materials and structures OXIDES OXYGEN COMPOUNDS Physics PRECURSOR QUANTITATIVE CHEMICAL ANALYSIS Roasting SACCHARIDES SCANNING ELECTRON MICROSCOPY SCATTERING SYNTHESIS Theory and models of crystal growth physics of crystal growth, crystal morphology and orientation THERMAL ANALYSIS THERMAL GRAVIMETRIC ANALYSIS TRANSITION ELEMENT COMPOUNDS X-RAY DIFFRACTION
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