Syntheses, structures and properties of silver(I) complexes with flexible 1,3,5-tris(pyridylmethoxyl)benzene ligands
Five new silver(I) complexes [Ag 2(L 2) 2](BF 4) 2·CH 3CN·CH 3OH ( 1), [Ag(L 2)(CF 3SO 3)] ( 2), [Ag(L 3)]ClO 4·CH 3OH ( 3), [Ag 2(L 3) 2](CF 3SO 3) 2·CH 3CN·CH 3OH·H 2O ( 4) and [Ag(L 3)]PF 6·2CH 3CN ( 5) [L 2=1,3,5-tris(2-pyridylmethoxyl)benzene, L 3=1,3,5-tris(3-pyridylmethoxyl)benzene] were synt...
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| creator | Wu, Gang Wang, Xiao-Feng Okamura, Taka-aki Chen, Min Sun, Wei-Yin Ueyama, Norikazu |
| description | Five new silver(I) complexes [Ag
2(L
2)
2](BF
4)
2·CH
3CN·CH
3OH (
1), [Ag(L
2)(CF
3SO
3)] (
2), [Ag(L
3)]ClO
4·CH
3OH (
3), [Ag
2(L
3)
2](CF
3SO
3)
2·CH
3CN·CH
3OH·H
2O (
4) and [Ag(L
3)]PF
6·2CH
3CN (
5) [L
2=1,3,5-tris(2-pyridylmethoxyl)benzene, L
3=1,3,5-tris(3-pyridylmethoxyl)benzene] were synthesized and characterized by single crystal X-ray diffraction analyses. In complexes
1–
5, ligands L
2 and L
3 show different conformations and act as three-connectors, while the Ag(I) atom serves as three-connecting node to result in the formation of 2D and 3D frameworks. Complexes
1 and
2 with different counteranions have similar 2D network structure with the same (4,8
2) topology. Complex
3 has a 3D structure with (10,3)-a topology while complexes
4 and
5 have the same 2D (6,3) topological structure. The results showed that the structure of organic ligands and counteranions play subtle but important role in determining the structure of the complexes. In addition, the photoluminescence and anion-exchange properties of the complexes were investigated in the solid state at room temperature.
Five new silver(I) coordination frameworks with different topology were obtained and their structures were determined by single crystal X-ray diffraction studies. The influence of counteranion and ligand on the structure of complexes was discussed, the photoluminescence and anion-exchange properties were reported.
[Display omitted] |
| doi_str_mv | 10.1016/j.jssc.2010.07.036 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_osti_</sourceid><recordid>TN_cdi_osti_scitechconnect_21432484</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><els_id>S002245961000318X</els_id><sourcerecordid>849477715</sourcerecordid><originalsourceid>FETCH-LOGICAL-c390t-a3ca6295cf6a4d67f0ab3ad26853937badcba1f276422ee84cb9231d99179e563</originalsourceid><addsrcrecordid>eNp9kU2LFDEQhhtRcFz9A54aRNyF6TFfnXTAiyx-LCx4UMFbSKernQyZTpvKrNv-etPM4tFTkpen3qrKW1UvKdlRQuXbw-6A6HaMFIGoHeHyUbWhRLeNYvLH42pDCGONaLV8Wj1DPBBCaduJTZW_LlPeAwJua8zp5PIpAdZ2Guo5xRlS9uUZxxp9uIN0eXNVu3icA9wX-bfP-3osd98HqOmWb9smJ4-X85L8sIQj5H28X8JVD9MfmKAO_mdxxufVk9EGhBcP50X1_eOHb9efm9svn26u3982jmuSG8udlUy3bpRWDFKNxPbcDkx2Lddc9XZwvaUjU1IwBtAJ12vG6aA1VRpayS-qV2ffiNkbdD6D27s4TeCyYVRwJjpRqDdnqiz86wSYzdGjgxDsBPGEphNaKKVoW0h2Jl2KiAlGMyd_tGkxlJg1B3Mwaw5mzcEQZUoOpej1g71FZ8OY7OQ8_qtknGnWMl24d2cOyo_ceUjrwDA5GHxa5x2i_1-bvzyQn6Y</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>849477715</pqid></control><display><type>article</type><title>Syntheses, structures and properties of silver(I) complexes with flexible 1,3,5-tris(pyridylmethoxyl)benzene ligands</title><source>Access via ScienceDirect (Elsevier)</source><creator>Wu, Gang ; Wang, Xiao-Feng ; Okamura, Taka-aki ; Chen, Min ; Sun, Wei-Yin ; Ueyama, Norikazu</creator><creatorcontrib>Wu, Gang ; Wang, Xiao-Feng ; Okamura, Taka-aki ; Chen, Min ; Sun, Wei-Yin ; Ueyama, Norikazu</creatorcontrib><description>Five new silver(I) complexes [Ag
2(L
2)
2](BF
4)
2·CH
3CN·CH
3OH (
1), [Ag(L
2)(CF
3SO
3)] (
2), [Ag(L
3)]ClO
4·CH
3OH (
3), [Ag
2(L
3)
2](CF
3SO
3)
2·CH
3CN·CH
3OH·H
2O (
4) and [Ag(L
3)]PF
6·2CH
3CN (
5) [L
2=1,3,5-tris(2-pyridylmethoxyl)benzene, L
3=1,3,5-tris(3-pyridylmethoxyl)benzene] were synthesized and characterized by single crystal X-ray diffraction analyses. In complexes
1–
5, ligands L
2 and L
3 show different conformations and act as three-connectors, while the Ag(I) atom serves as three-connecting node to result in the formation of 2D and 3D frameworks. Complexes
1 and
2 with different counteranions have similar 2D network structure with the same (4,8
2) topology. Complex
3 has a 3D structure with (10,3)-a topology while complexes
4 and
5 have the same 2D (6,3) topological structure. The results showed that the structure of organic ligands and counteranions play subtle but important role in determining the structure of the complexes. In addition, the photoluminescence and anion-exchange properties of the complexes were investigated in the solid state at room temperature.
Five new silver(I) coordination frameworks with different topology were obtained and their structures were determined by single crystal X-ray diffraction studies. The influence of counteranion and ligand on the structure of complexes was discussed, the photoluminescence and anion-exchange properties were reported.
[Display omitted]</description><identifier>ISSN: 0022-4596</identifier><identifier>EISSN: 1095-726X</identifier><identifier>DOI: 10.1016/j.jssc.2010.07.036</identifier><identifier>CODEN: JSSCBI</identifier><language>eng</language><publisher>Amsterdam: Elsevier Inc</publisher><subject>ACETONITRILE ; ALCOHOLS ; Anion-exchange properties ; AROMATICS ; BENZENE ; COHERENT SCATTERING ; COMPLEXES ; Condensed matter: electronic structure, electrical, magnetic, and optical properties ; Condensed matter: structure, mechanical and thermal properties ; CRYSTAL STRUCTURE ; CRYSTALS ; DIFFRACTION ; EMISSION ; Exact sciences and technology ; HYDROCARBONS ; HYDROXY COMPOUNDS ; INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY ; ION EXCHANGE ; LIGANDS ; LUMINESCENCE ; MATHEMATICS ; METHANOL ; MONOCRYSTALS ; Networks ; NITRILES ; Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation ; ORGANIC COMPOUNDS ; ORGANIC NITROGEN COMPOUNDS ; PHOTOLUMINESCENCE ; PHOTON EMISSION ; Physics ; SCATTERING ; SILVER COMPLEXES ; Silver(I) complex ; Solid state ; Structure of solids and liquids; crystallography ; Structure of specific crystalline solids ; SYNTHESIS ; TEMPERATURE RANGE ; TEMPERATURE RANGE 0273-0400 K ; Three dimensional ; TOPOLOGY ; TRANSITION ELEMENT COMPLEXES ; Two dimensional ; X-RAY DIFFRACTION ; X-rays</subject><ispartof>Journal of solid state chemistry, 2010-09, Vol.183 (9), p.2174-2182</ispartof><rights>2010 Elsevier Inc.</rights><rights>2015 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c390t-a3ca6295cf6a4d67f0ab3ad26853937badcba1f276422ee84cb9231d99179e563</citedby><cites>FETCH-LOGICAL-c390t-a3ca6295cf6a4d67f0ab3ad26853937badcba1f276422ee84cb9231d99179e563</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.jssc.2010.07.036$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>230,314,780,784,885,3550,27924,27925,45995</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=23292529$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.osti.gov/biblio/21432484$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Wu, Gang</creatorcontrib><creatorcontrib>Wang, Xiao-Feng</creatorcontrib><creatorcontrib>Okamura, Taka-aki</creatorcontrib><creatorcontrib>Chen, Min</creatorcontrib><creatorcontrib>Sun, Wei-Yin</creatorcontrib><creatorcontrib>Ueyama, Norikazu</creatorcontrib><title>Syntheses, structures and properties of silver(I) complexes with flexible 1,3,5-tris(pyridylmethoxyl)benzene ligands</title><title>Journal of solid state chemistry</title><description>Five new silver(I) complexes [Ag
2(L
2)
2](BF
4)
2·CH
3CN·CH
3OH (
1), [Ag(L
2)(CF
3SO
3)] (
2), [Ag(L
3)]ClO
4·CH
3OH (
3), [Ag
2(L
3)
2](CF
3SO
3)
2·CH
3CN·CH
3OH·H
2O (
4) and [Ag(L
3)]PF
6·2CH
3CN (
5) [L
2=1,3,5-tris(2-pyridylmethoxyl)benzene, L
3=1,3,5-tris(3-pyridylmethoxyl)benzene] were synthesized and characterized by single crystal X-ray diffraction analyses. In complexes
1–
5, ligands L
2 and L
3 show different conformations and act as three-connectors, while the Ag(I) atom serves as three-connecting node to result in the formation of 2D and 3D frameworks. Complexes
1 and
2 with different counteranions have similar 2D network structure with the same (4,8
2) topology. Complex
3 has a 3D structure with (10,3)-a topology while complexes
4 and
5 have the same 2D (6,3) topological structure. The results showed that the structure of organic ligands and counteranions play subtle but important role in determining the structure of the complexes. In addition, the photoluminescence and anion-exchange properties of the complexes were investigated in the solid state at room temperature.
Five new silver(I) coordination frameworks with different topology were obtained and their structures were determined by single crystal X-ray diffraction studies. The influence of counteranion and ligand on the structure of complexes was discussed, the photoluminescence and anion-exchange properties were reported.
[Display omitted]</description><subject>ACETONITRILE</subject><subject>ALCOHOLS</subject><subject>Anion-exchange properties</subject><subject>AROMATICS</subject><subject>BENZENE</subject><subject>COHERENT SCATTERING</subject><subject>COMPLEXES</subject><subject>Condensed matter: electronic structure, electrical, magnetic, and optical properties</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>CRYSTAL STRUCTURE</subject><subject>CRYSTALS</subject><subject>DIFFRACTION</subject><subject>EMISSION</subject><subject>Exact sciences and technology</subject><subject>HYDROCARBONS</subject><subject>HYDROXY COMPOUNDS</subject><subject>INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY</subject><subject>ION EXCHANGE</subject><subject>LIGANDS</subject><subject>LUMINESCENCE</subject><subject>MATHEMATICS</subject><subject>METHANOL</subject><subject>MONOCRYSTALS</subject><subject>Networks</subject><subject>NITRILES</subject><subject>Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation</subject><subject>ORGANIC COMPOUNDS</subject><subject>ORGANIC NITROGEN COMPOUNDS</subject><subject>PHOTOLUMINESCENCE</subject><subject>PHOTON EMISSION</subject><subject>Physics</subject><subject>SCATTERING</subject><subject>SILVER COMPLEXES</subject><subject>Silver(I) complex</subject><subject>Solid state</subject><subject>Structure of solids and liquids; crystallography</subject><subject>Structure of specific crystalline solids</subject><subject>SYNTHESIS</subject><subject>TEMPERATURE RANGE</subject><subject>TEMPERATURE RANGE 0273-0400 K</subject><subject>Three dimensional</subject><subject>TOPOLOGY</subject><subject>TRANSITION ELEMENT COMPLEXES</subject><subject>Two dimensional</subject><subject>X-RAY DIFFRACTION</subject><subject>X-rays</subject><issn>0022-4596</issn><issn>1095-726X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2010</creationdate><recordtype>article</recordtype><recordid>eNp9kU2LFDEQhhtRcFz9A54aRNyF6TFfnXTAiyx-LCx4UMFbSKernQyZTpvKrNv-etPM4tFTkpen3qrKW1UvKdlRQuXbw-6A6HaMFIGoHeHyUbWhRLeNYvLH42pDCGONaLV8Wj1DPBBCaduJTZW_LlPeAwJua8zp5PIpAdZ2Guo5xRlS9uUZxxp9uIN0eXNVu3icA9wX-bfP-3osd98HqOmWb9smJ4-X85L8sIQj5H28X8JVD9MfmKAO_mdxxufVk9EGhBcP50X1_eOHb9efm9svn26u3982jmuSG8udlUy3bpRWDFKNxPbcDkx2Lddc9XZwvaUjU1IwBtAJ12vG6aA1VRpayS-qV2ffiNkbdD6D27s4TeCyYVRwJjpRqDdnqiz86wSYzdGjgxDsBPGEphNaKKVoW0h2Jl2KiAlGMyd_tGkxlJg1B3Mwaw5mzcEQZUoOpej1g71FZ8OY7OQ8_qtknGnWMl24d2cOyo_ceUjrwDA5GHxa5x2i_1-bvzyQn6Y</recordid><startdate>20100901</startdate><enddate>20100901</enddate><creator>Wu, Gang</creator><creator>Wang, Xiao-Feng</creator><creator>Okamura, Taka-aki</creator><creator>Chen, Min</creator><creator>Sun, Wei-Yin</creator><creator>Ueyama, Norikazu</creator><general>Elsevier Inc</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope><scope>OTOTI</scope></search><sort><creationdate>20100901</creationdate><title>Syntheses, structures and properties of silver(I) complexes with flexible 1,3,5-tris(pyridylmethoxyl)benzene ligands</title><author>Wu, Gang ; Wang, Xiao-Feng ; Okamura, Taka-aki ; Chen, Min ; Sun, Wei-Yin ; Ueyama, Norikazu</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c390t-a3ca6295cf6a4d67f0ab3ad26853937badcba1f276422ee84cb9231d99179e563</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2010</creationdate><topic>ACETONITRILE</topic><topic>ALCOHOLS</topic><topic>Anion-exchange properties</topic><topic>AROMATICS</topic><topic>BENZENE</topic><topic>COHERENT SCATTERING</topic><topic>COMPLEXES</topic><topic>Condensed matter: electronic structure, electrical, magnetic, and optical properties</topic><topic>Condensed matter: structure, mechanical and thermal properties</topic><topic>CRYSTAL STRUCTURE</topic><topic>CRYSTALS</topic><topic>DIFFRACTION</topic><topic>EMISSION</topic><topic>Exact sciences and technology</topic><topic>HYDROCARBONS</topic><topic>HYDROXY COMPOUNDS</topic><topic>INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY</topic><topic>ION EXCHANGE</topic><topic>LIGANDS</topic><topic>LUMINESCENCE</topic><topic>MATHEMATICS</topic><topic>METHANOL</topic><topic>MONOCRYSTALS</topic><topic>Networks</topic><topic>NITRILES</topic><topic>Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation</topic><topic>ORGANIC COMPOUNDS</topic><topic>ORGANIC NITROGEN COMPOUNDS</topic><topic>PHOTOLUMINESCENCE</topic><topic>PHOTON EMISSION</topic><topic>Physics</topic><topic>SCATTERING</topic><topic>SILVER COMPLEXES</topic><topic>Silver(I) complex</topic><topic>Solid state</topic><topic>Structure of solids and liquids; crystallography</topic><topic>Structure of specific crystalline solids</topic><topic>SYNTHESIS</topic><topic>TEMPERATURE RANGE</topic><topic>TEMPERATURE RANGE 0273-0400 K</topic><topic>Three dimensional</topic><topic>TOPOLOGY</topic><topic>TRANSITION ELEMENT COMPLEXES</topic><topic>Two dimensional</topic><topic>X-RAY DIFFRACTION</topic><topic>X-rays</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Wu, Gang</creatorcontrib><creatorcontrib>Wang, Xiao-Feng</creatorcontrib><creatorcontrib>Okamura, Taka-aki</creatorcontrib><creatorcontrib>Chen, Min</creatorcontrib><creatorcontrib>Sun, Wei-Yin</creatorcontrib><creatorcontrib>Ueyama, Norikazu</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>OSTI.GOV</collection><jtitle>Journal of solid state chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Wu, Gang</au><au>Wang, Xiao-Feng</au><au>Okamura, Taka-aki</au><au>Chen, Min</au><au>Sun, Wei-Yin</au><au>Ueyama, Norikazu</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Syntheses, structures and properties of silver(I) complexes with flexible 1,3,5-tris(pyridylmethoxyl)benzene ligands</atitle><jtitle>Journal of solid state chemistry</jtitle><date>2010-09-01</date><risdate>2010</risdate><volume>183</volume><issue>9</issue><spage>2174</spage><epage>2182</epage><pages>2174-2182</pages><issn>0022-4596</issn><eissn>1095-726X</eissn><coden>JSSCBI</coden><abstract>Five new silver(I) complexes [Ag
2(L
2)
2](BF
4)
2·CH
3CN·CH
3OH (
1), [Ag(L
2)(CF
3SO
3)] (
2), [Ag(L
3)]ClO
4·CH
3OH (
3), [Ag
2(L
3)
2](CF
3SO
3)
2·CH
3CN·CH
3OH·H
2O (
4) and [Ag(L
3)]PF
6·2CH
3CN (
5) [L
2=1,3,5-tris(2-pyridylmethoxyl)benzene, L
3=1,3,5-tris(3-pyridylmethoxyl)benzene] were synthesized and characterized by single crystal X-ray diffraction analyses. In complexes
1–
5, ligands L
2 and L
3 show different conformations and act as three-connectors, while the Ag(I) atom serves as three-connecting node to result in the formation of 2D and 3D frameworks. Complexes
1 and
2 with different counteranions have similar 2D network structure with the same (4,8
2) topology. Complex
3 has a 3D structure with (10,3)-a topology while complexes
4 and
5 have the same 2D (6,3) topological structure. The results showed that the structure of organic ligands and counteranions play subtle but important role in determining the structure of the complexes. In addition, the photoluminescence and anion-exchange properties of the complexes were investigated in the solid state at room temperature.
Five new silver(I) coordination frameworks with different topology were obtained and their structures were determined by single crystal X-ray diffraction studies. The influence of counteranion and ligand on the structure of complexes was discussed, the photoluminescence and anion-exchange properties were reported.
[Display omitted]</abstract><cop>Amsterdam</cop><pub>Elsevier Inc</pub><doi>10.1016/j.jssc.2010.07.036</doi><tpages>9</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0022-4596 |
| ispartof | Journal of solid state chemistry, 2010-09, Vol.183 (9), p.2174-2182 |
| issn | 0022-4596 1095-726X |
| language | eng |
| recordid | cdi_osti_scitechconnect_21432484 |
| source | Access via ScienceDirect (Elsevier) |
| subjects | ACETONITRILE ALCOHOLS Anion-exchange properties AROMATICS BENZENE COHERENT SCATTERING COMPLEXES Condensed matter: electronic structure, electrical, magnetic, and optical properties Condensed matter: structure, mechanical and thermal properties CRYSTAL STRUCTURE CRYSTALS DIFFRACTION EMISSION Exact sciences and technology HYDROCARBONS HYDROXY COMPOUNDS INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY ION EXCHANGE LIGANDS LUMINESCENCE MATHEMATICS METHANOL MONOCRYSTALS Networks NITRILES Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation ORGANIC COMPOUNDS ORGANIC NITROGEN COMPOUNDS PHOTOLUMINESCENCE PHOTON EMISSION Physics SCATTERING SILVER COMPLEXES Silver(I) complex Solid state Structure of solids and liquids crystallography Structure of specific crystalline solids SYNTHESIS TEMPERATURE RANGE TEMPERATURE RANGE 0273-0400 K Three dimensional TOPOLOGY TRANSITION ELEMENT COMPLEXES Two dimensional X-RAY DIFFRACTION X-rays |
| title | Syntheses, structures and properties of silver(I) complexes with flexible 1,3,5-tris(pyridylmethoxyl)benzene ligands |
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