Lamellar Fe/Al{sub 2}O{sub 3} catalyst for high-yield production of multi-walled carbon nanotubes bundles

The lamellar Fe/Al{sub 2}O{sub 3} catalysts were prepared by sol-gel method, and then with these prepared catalysts, carbon nanotubes (CNTs) were synthesized by catalytic chemical vapor deposition (CCVD) method using C{sub 2}H{sub 2} as precursor. The as-prepared CNTs and Fe/Al{sub 2}O{sub 3} cataly...

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Veröffentlicht in:Materials research bulletin 2009-02, Vol.44 (2)
Hauptverfasser: Wang Xinqing, Li Liang, Chu Ningjie, Liu Yapi, Jin Hongxiao, Ge Hongliang
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Li Liang
Chu Ningjie
Liu Yapi
Jin Hongxiao
Ge Hongliang
description The lamellar Fe/Al{sub 2}O{sub 3} catalysts were prepared by sol-gel method, and then with these prepared catalysts, carbon nanotubes (CNTs) were synthesized by catalytic chemical vapor deposition (CCVD) method using C{sub 2}H{sub 2} as precursor. The as-prepared CNTs and Fe/Al{sub 2}O{sub 3} catalysts were characterized by X-ray diffraction, field emission scanning electron microscopy, transmission electron microscopy, high-resolution transmission electron microscopy and Raman spectrum. The results proved that the as-prepared CNTs actually existed in bundles. And the growth of CNTs bundles should be attributed to the lamellar catalysts, which supported the bottom growth mechanism of CNTs. The transition metal of Mo was not introduced in catalysts to produce CNTs bundles, which was different with others' results.
doi_str_mv 10.1016/j.materresbull.2008.04.022
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subjects ALUMINIUM OXIDES
CARBON
CATALYSTS
CHEMICAL VAPOR DEPOSITION
IRON
MATERIALS SCIENCE
MICROSTRUCTURE
NANOTUBES
RAMAN SPECTRA
SCANNING ELECTRON MICROSCOPY
SOL-GEL PROCESS
SYNTHESIS
TRANSMISSION ELECTRON MICROSCOPY
X-RAY DIFFRACTION
title Lamellar Fe/Al{sub 2}O{sub 3} catalyst for high-yield production of multi-walled carbon nanotubes bundles
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